Physical Change During Preparation of Nanofluids 36 Summary 37

4 RESULT AND DISCUSSION 30 4.1 Introduction 30 4.2 Comparison of AC Breakdown Voltage Between Base Oil and Fe 3 O 4 Nanofluid 30 4.3 Results of Fe 3 O 4 Nanofluids AC Breakdown Voltage Under Moisture Effect 32 4.4 The Effect of Different Size of Probes During Ultrasonication Processes 35

4.5 Physical Change During Preparation of Nanofluids 36

4.6 Summary 37

5 CONCLUSION AND RECOMMENDATIONS 38 5.1 Conclusions 38 5.2 Recommendations 39 REFERENCES 40 APPENDICES 44 LIST OF TABLES TABLE TITLE PAGE 2.1 Analysis of transformer oil based nanofluids system in literacture 11 3.1 List of the probes made of Titanium 23 3.2 The list of the percentage mass fraction of water to the total concentration of nanofluid 26 4.1 The breakdown voltage result for base oil and Fe 3 O 4 nanofluid 30 4.2 Results of Fe 3 O 4 nanofluids AC breakdown voltage under moisture Effect 32 4.3 The differences motion of vibration produced by two types of probes in oil 35 4.4 The physical change during preparation of nanofluid 37 LIST OF FIGURES FIGURE TITLE PAGE 2.1 Material of nanoparticles in transformer oil 5 2.2 Insulating oil in an electrical power transformer 7 2.3 BDV testing instrument 8 2.4 Solid nanoparticles 10 2.5 Magnetic stirrer 13 2.6 OPG-100A insulating oil tester 14 2.7 Comparison AC breakdown voltage of mineral oil and SiO 2 nanoflluids 15 3.1 Flowchart of the methodology 18 3.2 Flowchart of a preparation procedure for mineral oil based Nanofluids 21 3.3 Iron Oxide Nanopowder, Fe 3 O 4 21 3.4 Weighing of nanopowder by using a Digital analytical balance 22 3.5 Mixing of Oleic acid with mineral oil 22 3.6 40mm probes made of Titanium 23 3.7 The ultra-sonication treatment process 24 3.8 The vacuum drying oven process 25 3.9 The process of dropping water into the nanofluids 25 3.10 Megger oil tester OTS60PB 27 3.11 A list of electrode shapes and gap spacing for standard testing specifications 27 3.12 The setting of the gap distance between the both electrodes 28 3.13 The placed of the sample in the test vessel 29 3.14 Figure 3.14: The selecting the IEC 156 at the options menu Display 29 4.1 Graph of Comparison of Average Breakdown Voltage between Base Oil and Fe 3 O 4 Nanofluid 30 4.2 Graph of breakdown voltage of Fe 3 O 4 nanofluids under moisture effect 33 4.3 The graph of comparison of Average AC breakdown voltage between base oil and the percentage of water presence in the Fe 3 O 4 nanofluid 34 LIST OF ABBREVIATIONS HV - High Voltage IEC - International Eletrotechnical Comission AC - Alternating Current DC - Direct Current EHV - Extra High Voltage nm - nanometer BDV - Breakdown voltage PVD - Physical Vapor Diposition g - gram kV - kilovolt mm - milimeter l - liter kPa - kilopascal MF - Mass fraction M - Mass PFAE - Palm Fatty Acid Easter LIST OF APPENDICES APPENDIX TITLE PAGE A Calculation of Mass Fraction of Water to the Total Concentration of Nanofluid 44 CHAPTER 1 INTRODUCTION

1.1 Introduction