Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  Perpustakaan Unika

7. LAMPIRAN Lampiran 1. Kurva Standar

  12 y = 0,8673x + 1,4165

  10 R² = 0,971

  8 Series1

  6 Linear (Series1)

  4

  2

  2

  4

  6

  8

  10

  12 Lampiran 2. Perhitungan

  2.1. Persetase Recovery Kadmium (Cd)

  2.2. Jumlah Logam Cd yang Terserap oleh Fraksi Terlarut y = 1,4165x + 0,8673

2 R = 0,971

2.2.1. Konsentrasi 10%

2.2.1.1. Ukuran Partikel 40 mesh Ulangan 1 Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.2.1.2. Ukuran Partikel 80 mesh Ulangan 1 Ulangan 2 Perpustakaan Unika

  Perpustakaan Unika

  2.2.1.3. Ukuran Partikel 100 mesh Ulangan 1 Ulangan 3 Ulangan 2 Ulangan 4 Ulangan 3 Ulangan 5 Ulangan 4

  Ulangan 5

2.2.2. Konsentrasi 15%

2.2.2.1. Ukuran Partikel 40 mesh Ulangan 1 Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.2.2.2. Ukuran Partikel 80 mesh Ulangan 1 Perpustakaan Unika

  Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.2.2.3. Ukuran Partikel 100 mesh Ulangan 1 Ulangan 2 Ulangan 3 Perpustakaan Unika

  Ulangan 4 Ulangan 5

2.2.3. Konsentrasi 20% Ulangan 1 Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.2.2.2. Ukuran Partikel 80 mesh Ulangan 1 Perpustakaan Unika

  Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.2.2.3. Ukuran Partikel 100 mesh Ulangan 1 Ulangan 2 Ulangan 3 Perpustakaan Unika

  Ulangan 4 Ulangan 5

2.2.4. Kontrol

2.2.4.1. Konsentrasi 10% Ulangan 1 Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.2.4.2. Konsentrasi 15% Ulangan 1 Perpustakaan Unika

  Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.2.4.3. Konsentrasi 20% Ulangan 1 Ulangan 2 Ulangan 3 Perpustakaan Unika

  Perpustakaan Unika Ulangan 4 Ulangan 5

2.3. Jumlah Logam Cd yang Terserap oleh Fraksi Tidak Tidak Terlarut

  y = 1,4165 + 0,8673x

2 R = 0,971

2.3.1. Konsentrasi 10%

2.3.1.1. Ukuran Partikel 40 mesh Ulangan 1

  Ulangan 2 Ulangan 3 Ulangan 4 Ulangan 5

  2.3.1.2. Ukuran Partikel 80 mesh Ulangan 1 Ulangan 2 Ulangan 3 Ulangan 4 Perpustakaan Unika

  × 0,86 × 5 Ulangan 5

  8,63 × 0,86 × 5 Ulangan 2 Ulangan 3

  Jumlah Ulangan 4 Ulangan 5

2.3.1.3. Ukuran Partikel 100 mesh Ulangan 1

  2.3.2. Konsentrasi 15%

  2.3.2.1. Ukuran Partikel 40 mesh Ulangan 1 Perpustakaan Unika

  Perpustakaan Unika Ulangan 2

  2.3.2.2. Ukuran Partikel 80 mesh Ulangan 1 Jumlah Ulangan 3 Ulangan 2 Ulangan 4 Ulangan 3 Ulangan 5

  Perpustakaan Unika Ulangan 4 Ulangan 3 Ulangan 5 Ulangan 4

2.3.2.3. Ukuran Partikel 100 mesh Ulangan 1 Ulangan 5

  × 1,23 × 5 Ulangan 2

  6,55 × 1,68 × 5 Ulangan 5

  2.3.3.2. Ukuran Partikel 80 mesh Ulangan 1 8,4 × 1,62 × 5 Ulangan 2

  Perpustakaan Unika

2.3.3. Konsentrasi 20%

2.3.3.1. Ukuran Partikel 40 mesh Ulangan 1 Ulangan 2 Ulangan 3 Ulangan 4

  = 67,79 Ulangan 4 Ulangan 5

  ,16 Ulangan 3 Ulangan 4 Ulangan 5

  Perpustakaan Unika

2.3.3.3. Ukuran Partikel 100 mesh Ulangan 1 Ulangan 2

  Perpustakaan Unika

2.3.4. Kontrol

2.3.4.2.1. Konsentrasi 10% Ulangan 1 Ulangan 5 Ulangan 2

  2.3.4.2.2. Konsentrasi 15% Ulangan 1 Ulangan 3 Ulangan 2 Ulangan 4

  Perpustakaan Unika Ulangan 3 Ulangan 2 Ulangan 4 Ulangan 3 Ulangan 5 Ulangan 4

2.3.4.2.3. Konsentrasi 20% Ulangan 5 Ulangan 1

  Perpustakaan Unika Lampiran 3. Hasil Normalitas Data

  3.1. Tabel Normalitas Fraksi Terlarut, Tidak Terlarut dan Total

Tests of Normal ity

a

  Kolmogorov -Smirnov Shapiro-Wilk Mesh Stat istic df Sig. Stat istic df Sig. Terlarut 40 mesh

  .199 15 .114 .872 15 .037 80 mesh .245 15 .015 .873 15 .037 100 mesh

  .114 15 .200* .975 15 .922 Tidak_Terlarut 40 mesh

  .386 15 .000 .708 15 .000 80 mesh .206 15 .087 .861 15 .025 100 mesh

  .211 15 .072 .867 15 .030 Total 40 mesh

  .246 15 .015 .896 15 .083 80 mesh .234 15 .027 .909 15 .130 100 mesh

  .180 15 .200* .917 15 .173 *. This is a lower bound of the true signif icance.

  a.

  Lillief ors Signif icance Correction

  Tests of Normali ty a

  Kolmogorov -Smirnov Shapiro-Wilk Konsentrasi Stat istic df Sig. Stat istic df Sig. Terlarut 10% .144 15 .200* .896 15 .084

  15% .260 15 .007 .855 15 .020

  20% .151 15 .200* .924 15 .224

  Tidak_Terlarut 10% .197 15 .123 .861 15 .025

  15% .293 15 .001 .707 15 .000

  20% .254 15 .010 .853 15 .019

  Total 10% .139 15 .200* .932 15 .291

  15% .226 15 .038 .898 15 .089 20%

  .104 15 .200* .964 15 .766 *. This is a lower bound of t he true signif icance.

  a.

  Lillief ors Signif icance Correct ion

• .

  5 15.6300 2.06222

  Mean Std. Dev iat ion N

  Konsentrasi 10% 15% 20% Total

  45 Mesh 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total

  15 22.9798 8.87682

  15 18.4393 6.16434

  15 20.7907 9.06020

  15 29.7093 7.19859

  5 16.8333 4.33758

  5 14.7780 3.50973

  5 14.5260 3.96706

  15 21.1960 1.43839

  5 21.5520 9.67596

  5 14.9620 4.00236

  15 34.0640 3.68816

  3.2. Tabel Normalitas Kontrol (Terlarut, Tidak Terlarut dan Total) Lampiran 4. Tabel Deskriptif Statistik

  5 30.5540 5.57527

  5 25.5780 3.01458

  5 32.2160 4.66843

  Dependent Variable: Terlarut 33.8680 5.45702

  Descriptive Statistics

  Lillief ors Signif icance Correct ion a.

  Shapiro-Wilk This is a lower bound of t he true signif icance.

  a

  Kolmogorov -Smirnov

  Terlarut Tidak_Terlarut Total Stat istic df Sig. Stat istic df Sig.

  Konsentrasi 10% 15% 20% 10% 15% 20% 10% 15% 20%

  .208 5 .200* .971 5 .882 .223 5 .200* .968 5 .864 .195 5 .200* .976 5 .910 .262 5 .200* .895 5 .384 .210 5 .200* .948 5 .723 .232 5 .200* .872 5 .275 .220 5 .200* .921 5 .537 .207 5 .200* .938 5 .652 .247 5 .200* .876 5 .292

  4.1. Tabel Deskriptif Statistik Fraksi Terlarut Tests of Normali ty

  Perpustakaan Unika

  4.2. Tabel Deskriptif Statistik Fraksi Tidak Terlarut

  15 72.3060 5.19208

  5 59.0420 4.60614

  5 60.5260 3.15597

  5 55.9320 7.19225

  15 47.6220 4.36525

  5 64.4820 2.73727

  5 67.0560 4.28571

  5 59.7200 9.61374

  5 83.2400 4.85226

  

Descriptive Statistics

  5 81.4920 5.03791

  5 79.0127 6.80606

  15 56.0520 12.85986

  15 68.9213 11.40388

  15 Mesh 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh

  Konsentrasi 10% 15% 20% Total

  Mean Std. Dev iat ion N

  Dependent Variable: Total 48.2280 6.10019

  Mean Std. Dev iat ion N

  4.3. Tabel Deskriptif Statistik Fraksi Total

Descriptive Statistics

  5 38.1660 18.19307

  Dependent Variable: Tidak_Terlarut 14.3600 1.70807

  5 26.8280 .78334

  5 34.9480 .60093

  5 25.3787 8.82767

  15 13.5560 1.37939

  5 48.8500 3.45913

  5 52.0920 1.55643

  15 51.1120 4.79178

  Konsentrasi 10% 15% 20% Total

  5 68.7120 2.24636

  5 66.7140 2.27570

  5 62.1793 8.70701

  15 26.3427 18.35005

  15 48.1300 17.84870

  15 51.2513 13.52206

  15 41.9080 19.80497

  45 Mesh 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total 40 mesh 80 mesh 100 mesh Total

  Perpustakaan Unika

  4.4. Tabel Deskriptif Statistik Kontrol (Fraksi Terlarut, Tidak Terlarut dan Total) Descriptives

  5 37.03900 .913540 .408548 35.90469 38.17331 35.832 38.002 5 13.23500 1.566150 .700404 11.29037 15.17963 10.564 14.574 5 7.76720 1.019355 .455869 6.50150 9.03290 6.334 8.820 15 19.34707 13.200600 3.408380 12.03682 26.65732 6.334 38.002 5 32.38040 .662887 .296452 31.55732 33.20348 31.425 33.224 5 57.93600 1.726478 .772105 55.79229 60.07971 56.232 60.400 5 79.01360 1.900449 .849907 76.65388 81.37332 76.463 81.410 15 56.44333 19.787218 5.109038 45.48554 67.40113 31.425 81.410 5 69.41960 1.305491 .583833 67.79862 71.04058 67.957 70.584 5 71.17080 1.773797 .793266 68.96834 73.37326 69.560 74.088 5 86.78060 2.670402 1.194240 83.46486 90.09634 82.797 89.289 15 75.79033 8.287203 2.139747 71.20103 80.37963 67.957 89.289

  10% 15% 20% Total 10% 15% 20% Total 10% 15% 20% Total

  Terlarut Tidak_Terlarut Total

  N Mean Std. Dev iat ion Std. Error Lower Bound Upper Bound 95% Conf idence Interv al f or

  Mean Minimum Maximum

  Perpustakaan Unika

  64 Perpustakaan Unika

  Lampiran 5. Tabel Anova

  5.1. Tabel Two-Way Anova Fraksi Terlarut a Levene's Test of Equali ty of Error Variances

  Dependent Variable: Terlarut F df 1 df 2 Sig.

  2.191

  8 36 .052 Tests the null hy pothesis that the error v ariance of t he dependent v ariable is equal across groups.

  a.

  Design: Intercept+Konsentrasi+Mesh+Konsentrasi * Mesh

  

Tests of Between-Subjects Effects

  Dependent Variable: Terlarut Ty pe I II Sum Source of Squares df Mean Square F Sig.

  a

  Corrected Model 2968.466 8 371.058 26.789 .000 Intercept

  23763.158 1 23763.158 1715.615 .000 Konsentrasi

  1457.793 2 728.896 52.624 .000 Mesh 1060.421 2 530.211 38.279 .000 Konsentrasi * Mesh

  450.253 4 112.563 8.127 .000 Error

  498.640 36 13.851 Total

  27230.264

  45 Corrected Total 3467.106

  44 a. R Squared = . 856 (Adjusted R Squared = .824)

  5.2. Tabel Two-Way Anova Fraksi Tidak Terlarut a Levene's Test of Equali ty of Error Variances

  Dependent Variable: Tidak_Terlarut F df 1 df 2 Sig.

  4.556

  8 36 .001 Tests the null hy pothesis that the error v ariance of t he dependent v ariable is equal across groups.

  a.

  Design: Intercept+Konsentrasi+Mesh+Konsentrasi * Mesh

  65

  Design: Intercept+Konsentrasi+Mesh+Konsentrasi * Mesh a.

  R Squared = . 896 (Adjusted R Squared = .873) a.

  Ty pe I II Sum of Squares df Mean Square F Sig.

  44 Source Corrected Model Intercept Konsentrasi Mesh Konsentrasi * Mesh Error Total Corrected Total

  45 7263.016

  196734.679

  148.682 4 37.171 1.768 .157 756.748 36 21.021

  4596.366 2 2298.183 109.329 .000 1761.220 2 880.610 41.892 .000

  8 813.284 38.689 .000 189471.662 1 189471.662 9013.538 .000

  a

  Dependent Variable: Total 6506.268

  Tests of Between-Subjects Effects

  8 36 .444 F df 1 df 2 Sig. Tests the null hy pothesis that the error v ariance of t he dependent v ariable is equal across groups.

  5.3. Tabel Two-Way Anova Total

Tests of Between-Subjects Effects

  Dependent Variable: Total 1.012

  Levene's Test of Equali ty of Error Variances a

  R Squared = . 988 (Adjusted R Squared = .985) a.

  Ty pe I II Sum of Squares df Mean Square F Sig.

  44 Source Corrected Model Intercept Konsentrasi Mesh Konsentrasi * Mesh Error Total Corrected Total

  45 17258.412

  213.477 36 5.930 96291.033

  5524.361 2 2762.181 465.805 .000 1048.348 4 262.087 44.198 .000

  8 2130.617 359.300 .000 79032.621 1 79032.621 13327.802 .000 10472.226 2 5236.113 883.001 .000

  a

  Dependent Variable: Tidak_Terlarut 17044.935

  Perpustakaan Unika

  66 Perpustakaan Unika

  5.4. Tabel One-Way Anova Kontrol

Test of Homogeneity of Variances

  Lev ene St at ist ic df 1 df 2 Sig. Terlarut

  .631

  2 12 .549 Tidak_Terlarut 1.554

  2 12 .251 Total

  5.078

  2 12 .025

  

ANOVA

  Sum of Squares df Mean Square F Sig. Terlarut Between Groups

  862.852 2 431.426 33.843 .000 Within Groups

  152.975 12 12.748 Total 1015.827

  14 Tidak_Terlarut Between Groups 5130.221 2 2565.111 258.057 .000

  Within Groups 119.281 12 9.940

  Total 5249.502

  14 Total Between Groups 1926.841 2 963.420 38.437 .000

  Within Groups 300.778 12 25.065

  Total 2227.619

  14 Lampiran 6. Tabel Post Hoc

  6.1. Tabel Post Hoc Fraksi Terlarut

Terl arut

a,b

  Duncan Subset

  Konsentrasi N

  1

  2

  3 20% 15 16.8333 15% 15 21.5520 10% 15 30.5540 Sig. 1.000 1.000 1.000 Means f or groups in homogeneous subset s are display ed.

  Based on Ty pe III Sum of Squares The error t erm is Mean Square(Error) = 13.851.

  a.

  Uses Harmonic Mean Sample Size = 15.000.

  b.

  Alpha = .05.

  67 Perpustakaan Unika

  Terl arut a,b

  Duncan Subset

  Mesh N

  1

  2 100 mesh 15 18.4393 80 mesh 15 20.7907 40 mesh 15 29.7093 Sig.

  .092 1.000 Means f or groups in homogeneous subset s are display ed. Based on Ty pe III Sum of Squares The error t erm is Mean Square(Error) = 13.851.

  a.

  Uses Harmonic Mean Sample Size = 15.000.

  b.

  Alpha = .05.

  6.2. Tabel Post Hoc Fraksi Tidak Terlarut

Tidak_Terlarut

a,b

  Duncan Subset

  Konsentrasi N

  1

  2

  3 10% 15 25.3787 15% 15 38.1660 20% 15 62.1793 Sig.

  1.000 1.000 1.000 Means f or groups in homogeneous subset s are display ed. Based on Ty pe III Sum of Squares The error t erm is Mean Square(Error) = 5.930.

  a.

  Uses Harmonic Mean Sample Size = 15.000.

  b.

  Alpha = .05.

  

Tidak_Terlarut

a,b

  Duncan Subset

  Mesh N

  1

  2

  3 40 mesh 15 26.3427 80 mesh 15 48.1300 100 mesh 15 51.2513 Sig.

  1.000 1.000 1.000 Means f or groups in homogeneous subsets are display ed. Based on Ty pe III Sum of Squares The error term is Mean Square(Error) = 5.930.

  68 Perpustakaan Unika

  6.3. Tabel Post Hoc Total

Total

a,b

  Duncan Subset

  Konsentrasi N

  1

  2

  3 10% 15 55.9320 15% 15 59.7200 20% 15 79.0127 Sig.

  1.000 1.000 1.000 Means f or groups in homogeneous subset s are display ed. Based on Ty pe III Sum of Squares The error t erm is Mean Square(Error) = 21.021.

  a.

  Uses Harmonic Mean Sample Size = 15.000.

  b.

  Alpha = .05.

  Total a,b

  Duncan Subset

  Mesh N

  1

  2 40 mesh 15 56.0520 80 mesh 15 68.9213 100 mesh 15 69.6913 Sig.

  1.000 .648 Means f or groups in homogeneous subset s are display ed. Based on Ty pe III Sum of Squares The error t erm is Mean Square(Error) = 21.021.

  a.

  Uses Harmonic Mean Sample Size = 15.000.

  b.

  Alpha = .05.

  6.4. Tabel Post Hoc Kontrol (Fraksi Terlarut)

Terl arut

a

  Duncan Subset f or alpha = .05

  Konsentrasi N

  1

  2

  3 20% 5 12.1620 15% 5 18.4320 10% 5 30.4420 Sig.

  1.000 1.000 1.000 Means f or groups in homogeneous subset s are display ed.

  69 Perpustakaan Unika

  6.5. Tabel Post Hoc Kontrol (Fraksi Tidak Terlarut)

Tidak_Terlarut

a

  Duncan Subset f or alpha = .05

  Konsentrasi N

  1

  2

  3 10% 5 33.2300 15% 5 52.6600 20% 5 78.3840 Sig. 1.000 1.000 1.000 Means f or groups in homogeneous subset s are display ed.

  a.

  Uses Harmonic Mean Sample Size = 5.000.

  6.6. Tabel Post Hoc Kontrol (Fraksi Total)

Total

a

  Duncan Subset f or alpha = .05

  Konsentrasi N

  1

  2

  3 10% 5 63.6740 15% 5 71.0860 20% 5 90.5500 Sig. 1.000 1.000 1.000 Means f or groups in homogeneous subset s are display ed.

  a.

  Uses Harmonic Mean Sample Size = 5.000.