LAMPIRAN A TABEL DATA PENGUJIAN TRUE DENSITY, POROSITAS, BULK DENSITY, FLUX DENSITY, DAN PERMEABILITAS
L-1 LAMPIRAN A TABEL DATA PENGUJIAN TRUE DENSITY, POROSITAS, BULK DENSITY, FLUX DENSITY, DAN PERMEABILITAS
Tabel L.1 Data true density serbuk Ba-ferrite digiling selama 0, 12,24, dan
48 jam, dan true density Ba-ferrite dengan penambahan B
2 O
3 sebanyak 0, 0.2, 0.5, 1.0, dan 2.0 % berat digiling selama 48 jam.
3 True Density (g/cm ) Waktu Milling (jam) 0 % 0.5 % 1.0 % 2.0 %
4.37
12
4.40
24
4.71
48
4.76
4.82
4.89
4.97 Tabel L.2 Nilai porositas dari bahan magnet Ba-ferrite dengan penambahan B O sebanyak 0, 0.5, 1.0, dan 2.0 % berat digiling selama 48
2
3 o jam yang disinter pada suhu: 1100, 1150, dan 1200 C porosity
B
2 O
3 o o o ( % berat) 1100 C 1150 C 1200 C
7.5
6.8
7.5
0.5
5.0
5.2
5.7
1
8.2
7.7
7.8
2
8.7
7.6
8.8 Tabel L.3 Nilai bulk density dari bahan magnet Ba-ferrite dengan penambahan B
2 O 3 sebanyak 0, 0.2, 0.5, 1.0, dan 2.0 % berat digiling selama 48 jam yang disinter pada suhu: 1100, 1150, dan o 1200 C.
3
- B
19
12 O
19
2 O
3 (0.5 % berat) 2.28
2.43
0.93 1,35 BaFe
12 O
2 O
2.85
3 (1.0 % berat) 1.87
2.8
0.66 1,90 BaFe
12 O
19
2 O
3 (2.0 % berat) 1.64
2.11
0.76 1,65 BaFe
2.18
0.77 1,63 dimana μ o = 1,256 G.cm/A
Br/H CB)
Tabel L.4 Data Flux density magnetic dari bahan magnet Ba-ferrite dengan penambahan B
2 O 3 sebanyak 0, 0.2, 0.5, 1.0, dan 2.0 % berat digiling selama 48 jam yang disinter pada suhu: 1100, 1150, dan 1200 o C, masing-masing ditahan selama 1 jam. B
2 O
3 ( % berat) Flux Density (Gauss)
1100 o C 1150 o C 1200 o C 798.5 603.2 714 0.5 832.5 618.3 723.1
1 699.6 598.1 622.8 2 604.2 463.9 439.9 Tabel L.5 Data perbandingan permeabilitas dan susespbilitas bahan Barium heksaferit. Komposisi
Br (kG)
H
CB(kOe) µ m (
BaFe
3 (0 % berat)
12 O
19
2.26
2.9
0.77 1,63 BaFe
12 O
19
2 O
- B
- B
- B
L-2 LAMPIRAN B HASIL PENGUJIAN MAGNETIK DENGAN MENGGUNAKAN
PERMAGRAPH
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
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L-2
LAMPIRAN C
HASIL PENGUJIAN MIKROSTRUKTUR MENGGUNAKAN
SCANNING ELECTRON MICROSCOPE (SEM)-EDX
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe
12 O
19 Keterangan Komersil CHINA (serbuk) Operator Dr. Toto Sudiro Pembesaran 4000 x
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe
12 O
19 Komersil CHINA milling 48 jam Keterangan (serbuk) Operator Dr. Toto Sudiro Pembesaran 4000 x
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe
12 O
19 Komersil CHINA + B O milling 48 jam
2
3 Keterangan (serbuk) Operator Dr. Toto Sudiro
Pembesaran 4000 x
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe
12 O
19 Keterangan Komersil CHINA (pelet) Operator Dr. Toto Sudiro Pembesaran 1000 x
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe
12 O
19 Komersil CHINA milling 48 jam Keterangan (pelet) Operator Dr. Toto Sudiro Pembesaran 4000 x
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe
12 O
19 Komersil CHINA + B O milling 48
2
3 Keterangan jam (pelet) Operator Dr. Toto Sudiro
Pembesaran 4000 x
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe
12 O
19 Keterangan EDX Komersil CHINA (Serbuk) Operator Dr. Toto Sudiro Pembesaran 4000 x
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe O
12
19 EDX Komersil CHINA milling 48 Keterangan jam (serbuk) Operator Dr. Toto Sudiro Pembesaran 4000 x
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
LEMBAGA ILMU PENGETAHUAN INDONESIA PUSAT PENELITIAN FISIKA
- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556 JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832 e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id Sampel BaFe O
12
19 EDX Komersil CHINA + B
2 O
3 Keterangan milling 48 jam (serbuk)
Operator Dr. Toto Sudiro Pembesaran 4000 x
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
KAWASAN PUSPITEK SERPONG TANGERANG 15314 Tel. (021) 7560570 = 750556
JALAN SANGKURIANG KOMPLEKS LIPI BANDUNG 40135 No telp (022) 2504832
e-mail : info@fisika.lipi.go.id http//www.fisika.lipi.go.id
LEMBAGA ILMU PENGETAHUAN INDONESIA
PUSAT PENELITIAN FISIKA
RESEARCH CENTER FOR PHISICS- – INDONESIA INSTITUTE OF SCIENCES
L-4 LAMPIRAN D HASIL PENGUJIAN
PARTICLE SIZE ANALYSIS (PSA)
Barium hexaferrite original sp4 Element Line App.
0,1193
Weight% sigma Atomic
Weight %
Conc k ratio Intensity corrn.
Element Line App.
Totals 100 Barium hexaferrite original milling 48 jam + B 2 O 3 Sp4
BaF2 1-Jun-1999 12:00 AM
7 0,9502 11,59 0,11 2,94
S 12,79
O K_SERIE
Ba L_SERIE
SrF2 1-Jun-1999 12:00 AM
2 0,6152 1,31 0,09 0,52
0,0087
S 0,94
Sr L_SERIE
Fe 1-Jun-1999 12:00 AM
% Standard
S 81,62
0,6500
0,0174
BaF2 1-Jun-1999 12:00 AM
9 0,941 8,59 0,09 2,01
0,1186
S 12,71
Ba L_SERIE
SrF2 1-Jun-1999 12:00 AM
4 0,6257 1,91 0,08 0,7
S 1,88
0,2929
Sr L_SERIE
Fe 1-Jun-1999 12:00 AM
3 0,9234 57,43 0,13 32,99
0,8337
S 83,37
Fe K_SERIE
SiO2 1-Jun-1999 12:00 AM
2 1,6195 32,06 0,11 64,3
9 0,9318 60,06 0,15 37,54
S 65,01
Conc k ratio
Fe K_SERIES
1 0.009
Sr L_SERIES
36.36 Fe 1-Jun-1999 12:00 AM
0.14
59.09
83 0.9296
69.98 0.699
60.24 SiO2 1-Jun-1999 12:00 AM
1.27
0.12
28.05
68 1.6118
57.58 0.206
O K_SERIES
Weight% sigma Atomic% Standard
Weight %
Intensity corrn.
27 0.6163
0.08
Fe K_SERIE
Weight %
SiO2 1-Jun-1999 12:00 AM
9 1,6015 27,04 0,13 58,99
0,1804
S 50,29
O K_SERIE
% Standard
Weight% sigma Atomic
Conc k ratio Intensity corrn.
0.5 SrF2 1-Jun-1999 12:00 AM
Sp8 Element Line App.
Totals 100 Barium hexaferrite original millig 48 jam
2.9 BaF2 1-Jun-1999 12:00 AM
0.1
11.59
65 0.9479
14 0.130
Ba L_SERIES
Totals 100
L-4 LAMPIRAN E HASIL PENGUJIAN
X-RAY DIFRACTION (XRD) DAN MATCH REPORT
Match! Phase Analysis Report Sample: C-cina_Theta_2-Theta
Sample Data
File name C-cina_Theta_2-Theta.rd File path D:/punya dol/TESIS DELOVITA USU 4-6-2014/DATA PENGUJIAN TESIS DELOVITA 20-5-2014/DATA XRD DELOVITA/CHINA ORIGIN Data collected Jul 7, 2014 02:15:40 Data range 9.930º - 79.930º Number of points 3501 Step size 0.020 Rietveld refinement converged No Alpha2 subtracted Yes Background subtr. Yes Data smoothed Yes 2theta correction -0.07º Radiation X-rays Wavelength 1.540598 Å
Matched Phases Index Amount (%) Name Formula sum
A 100.0 Barium dodecairon(III) oxide Ba Fe12 O19
103.5 Unidentified peak area
A: Barium dodecairon(III) oxide (100.0 %)
Formula sum Ba Fe12 O19 Entry number 96-100-9039 Figure-of-Merit (FoM) 0.742763 Total number of peaks 186 Peaks in range 185 Peaks matched
82 Intensity scale factor
1.02 Space group P 63/m m c Crystal system hexagonal Unit cell a= 5.8890 Å c= 23.1820 Å I/Icor
4.27 Calc. density 3.850 g/cm³ Reference Bertaut F, Deschamps A, Pauthenet R, "Etude de la substitution de Fe par Al, Ga et Cr dans l'hexaferrite de baryum, Ba O, (Fe2 O3)6",
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences (1884 - 1965) 246, 2594-2597 (1958)
Candidates
Name Formula Entry No. FoMBarium dodecairon(III) oxide Ba Fe12 O19 96-100-9039 0.7194
Search-Match
SettingsReference database used COD-Inorg REV107951 2014.03.25 Automatic zeropoint adaptation Yes Minimum figure-of-merit (FoM)
0.60 Parameter/influence 2theta
0.50 Parameter/influence intensities
0.50 Parameter multiple/single phase(s) 0.50
Selection Criteria
16 16.73 5.2936 253.21 0.9200
61 24.57 3.6202 414.40 0.9200
49 22.19 4.0021 388.16 0.9200
50 22.30 3.9827 386.49 0.9200
51 22.47 3.9536 479.16 0.9200
52 22.58 3.9338 452.22 0.9200
53 22.99 3.8659 654.10 0.9200 A
54 23.34 3.8085 453.14 0.9200 A
55 23.52 3.7801 398.16 0.9200
56 23.71 3.7499 407.05 0.9200
57 23.86 3.7267 389.34 0.9200
58 24.06 3.6961 350.97 0.9200
59 24.23 3.6703 377.01 0.9200
60 24.39 3.6463 322.24 0.9200
62 24.76 3.5924 374.76 0.9200
47 21.92 4.0518 395.65 0.9200
63 24.87 3.5769 375.21 0.9200
64 25.17 3.5352 366.29 0.9200
65 25.39 3.5058 340.45 0.9200
66 25.60 3.4764 378.00 0.9200
67 25.78 3.4524 368.38 0.9200
68 25.92 3.4352 319.81 0.9200 A
69 26.11 3.4101 279.22 0.9200
70 26.22 3.3961 324.45 0.9200
71 26.37 3.3765 295.74 0.9200
72 26.51 3.3593 305.02 0.9200
73 26.72 3.3341 316.78 0.9200
74 26.92 3.3099 325.71 0.9200
75 27.14 3.2828 321.51 0.9200
48 22.02 4.0330 354.78 0.9200
46 21.73 4.0866 390.59 0.9200
17 16.92 5.2366 315.71 0.9200
30 18.94 4.6817 447.43 0.9200 A
18 17.07 5.1911 337.24 0.9200
19 17.19 5.1544 327.31 0.9200
20 17.40 5.0933 378.83 0.9200 A
21 17.57 5.0433 363.08 0.9200
22 17.67 5.0148 358.96 0.9200
23 17.83 4.9715 353.42 0.9200 A
24 17.95 4.9389 354.90 0.9200
25 18.16 4.8824 312.34 0.9200
26 18.31 4.8424 324.57 0.9200
27 18.41 4.8162 352.94 0.9200
28 18.61 4.7637 385.33 0.9200
29 18.72 4.7375 414.36 0.9200
31 19.14 4.6325 371.35 0.9200
45 21.63 4.1057 380.02 0.9200
32 19.35 4.5827 415.42 0.9200
33 19.55 4.5375 395.78 0.9200
34 19.69 4.5044 440.09 0.9200
35 19.81 4.4782 378.72 0.9200
36 20.00 4.4354 434.53 0.9200
37 20.15 4.4033 432.99 0.9200
38 20.35 4.3614 478.00 0.9200
39 20.49 4.3309 433.39 0.9200
40 20.69 4.2895 486.36 0.9200
41 20.89 4.2483 423.05 0.9200 A
42 21.08 4.2116 381.46 0.9200
43 21.28 4.1711 400.85 0.9200
44 21.47 4.1347 428.54 0.9200
76 27.44 3.2483 294.37 0.9200
107 33.55 2.6693 284.46 0.9200
108 33.71 2.6569 286.28 0.9200
109 34.11 2.6268 741.28 0.9200 A
110 34.53 2.5954 272.56 0.9200
111 34.71 2.5822 254.89 0.9200 112 35.01 2.5609 317.40 0.9200 113 35.21 2.5465 339.85 0.9200 A 114 35.44 2.5305 287.36 0.9200 A 115 35.63 2.5181 272.47 0.9200 A 116 35.83 2.5039 255.46 0.9200 117 35.93 2.4971 262.06 0.9200 A 118 36.74 2.4445 232.03 0.9200 119 36.89 2.4344 271.01 0.9200 120 37.10 2.4210 423.72 0.9200 A 121 37.30 2.4090 261.89 0.9200 122 38.00 2.3661 231.92 0.9200 123 38.36 2.3446 262.78 0.9200 A 124 38.78 2.3202 252.67 0.9200 A 125 39.04 2.3051 229.44 0.9200 A 126 39.66 2.2708 280.47 0.9200 127 40.19 2.2420 245.67 0.9200 128 40.39 2.2314 293.59 0.9200 A 129 41.79 2.1596 255.69 0.9200 130 42.05 2.1471 226.22 0.9200 131 42.25 2.1372 243.40 0.9200 132 42.44 2.1282 296.31 0.9200 A 133 47.07 1.9292 240.37 0.9200 A 134 47.52 1.9119 235.75 0.9200 A 135 49.35 1.8450 234.82 0.9200 A 136 50.09 1.8196 243.87 0.9200 A 137 54.74 1.6756 248.17 0.9200 A 138 55.02 1.6675 369.10 0.9200 A 139 55.30 1.6598 312.14 0.9200 A 140 55.45 1.6556 245.93 0.9200 A 141 56.30 1.6328 270.34 0.9200 A 142 56.45 1.6288 304.97 0.9200 143 56.63 1.6239 401.42 0.9200 A 144 56.82 1.6190 257.16 0.9200 A 145 57.23 1.6084 247.46 0.9200 A 146 57.51 1.6012 255.32 0.9200 A 147 62.66 1.4815 233.15 0.9200 A 148 62.90 1.4764 245.57 0.9200 149 63.03 1.4736 266.54 0.9200 150 63.15 1.4711 237.57 0.9200 A 151 65.54 1.4232 236.45 0.9200 A 152 72.49 1.3029 227.90 0.9200 A 153 72.81 1.2979 234.64 0.9200 A
Rietveld Refinement using FullProf Calculation was not run or did not converge. Integrated Profile Areas Based on calculated profile Profile area Counts Amount
Overall diffraction profile 122222 100.00% Background radiation 36071 29.51% Diffraction peaks 86151 70.49% Peak area belonging to selected phases 86151 70.49%
Match! Phase Analysis Report Sample: BaFeO-milled 48 h
20.1 Unidentified peak area
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences (1884 - 1965) 246, 2594-2597 (1958)
(1925)
3.58 Calc. density 5.291 g/cm³ Reference Pauling L., Hendricks S. B., "Crystal structures of hematite and corundum", Journal of the American Chemical Society 47, 781-790
0.83 Space group R -3 c Crystal system rhombohedral Unit cell a= 5.4200 Å α= 55.280º I/Icor
14 Intensity scale factor
19 Peaks matched
33 Peaks in range
Formula sum Fe2 O3 Entry number 96-900-9783 Figure-of-Merit (FoM) 0.661775 Total number of peaks
4.27 Calc. density 3.850 g/cm³ Reference Bertaut F, Deschamps A, Pauthenet R, "Etude de la substitution de Fe par Al, Ga et Cr dans l'hexaferrite de baryum, Ba O, (Fe2 O3)6",
Sample Data
1.39 Space group P 63/m m c Crystal system hexagonal Unit cell a= 5.8890 Å c= 23.1820 Å I/Icor
61 Intensity scale factor
Formula sum Ba Fe12 O19 Entry number 96-100-9039 Figure-of-Merit (FoM) 0.776425 Total number of peaks 186 Peaks in range 114 Peaks matched
A: Barium dodecairon(III) oxide (58.0 %)
42.0 Hematite Fe2 O3
58.0 Barium dodecairon(III) oxide Ba Fe12 O19 B
A
Matched Phases Index Amount (%) Name Formula sum
File name BaFeO-milled 48 h.ras File path G:/TESIS DELOVITA USU 4-6-2014/DATA PENGUJIAN TESIS DELOVITA 20-5-2014/DATA XRD DELOVITA/CHINA MILLING 48 JAM HEM Data collected Jun 4, 2014 13:49:46 Data range 10.120º - 80.085º Number of points 3501 Step size 0.020 Rietveld refinement converged No Alpha2 subtracted Yes Background subtr. No Data smoothed Yes 2theta correction 0.12º Radiation X-rays Wavelength 1.540598 Å
B: Hematite (42.0 %)
Fe2 O3 96-210-1168 0.6919 Fe2 O3 96-210-1169 0.6919 Fe2 O3 96-210-1170 0.6919 iron oxide Fe3 O4 96-151-3305 0.6891
2 13.36 6.6218 305.96 0.1600
11 15.08 5.8688 442.25 0.1600
10 14.87 5.9517 358.03 0.1600
9 14.68 6.0292 364.16 0.1600
8 14.60 6.0632 326.97 0.1600
7 14.41 6.1413 401.03 0.1600
6 14.23 6.2200 342.89 0.1600
5 14.11 6.2709 388.69 0.1600
4 14.02 6.3098 331.46 0.1600
3 13.81 6.4093 309.31 0.1600
1 12.98 6.8130 298.60 0.1600
Fe3 O4 96-210-1927 0.6883 Magnetite Fe3 O4 96-900-2324 0.6876 Magnetite Fe3 O4 96-900-5839 0.6876 Magnetite Fe3 O4 96-900-7707 0.6873 Magnetite Fe3 O4 96-900-6190 0.6872 Magnetite Fe3 O4 96-900-6195 0.6872 Magnetite Fe3 O4 96-900-6200 0.6872 Magnetite Fe3 O4 96-900-6185 0.6871 Magnetite Fe3 O4 96-900-6243 0.6871 Magnetite Fe3 O4 96-900-6253 0.6871 Magnetite Fe3 O4 96-900-6266 0.6871 Magnetite Fe3 O4 96-901-3530 0.6870 Magnetite Fe3 O4 96-900-2317 0.6868 Magnetite Fe3 O4 96-900-0927 0.6855 Iron(III) oxide (Hematite) Fe2 O3 96-101-1241 0.6853 Magnetite Fe3 O4 96-901-0940 0.6846 Magnetite Fe3 O4 96-900-5837 0.6844 Magnetite Fe3 O4 96-900-7645 0.6838 Magnetite Fe3 O4 96-900-6921 0.6837 Magnetite Fe3 O4 96-900-5841 0.6832 Magnetite Fe3 O4 96-900-5814 0.6824 and 26 others...
No. 2theta [º] d [Å] I/I0 FWHM Matched
present: Peak List
All elements not mentioned above
Selection Criteria Elements: Elements that must be present: O, Fe Elements that must NOT be
0.50 Parameter multiple/single phase(s) 0.50
0.50 Parameter/influence intensities
0.60 Parameter/influence 2theta
Reference database used COD-Inorg REV107951 2014.03.25 Automatic zeropoint adaptation Yes Minimum figure-of-merit (FoM)
Search-Match Settings
12 15.22 5.8158 434.46 0.1600 A
43 20.37 4.3558 811.80 0.1600
85 27.75 3.2117 590.29 0.1600
74 25.61 3.4760 630.98 0.1600
75 25.81 3.4486 777.18 0.1600
76 26.00 3.4239 600.19 0.1600 A
77 26.14 3.4067 694.61 0.1600
78 26.33 3.3816 706.90 0.1600
79 26.52 3.3586 714.56 0.1600
80 26.75 3.3294 649.08 0.1600
81 27.02 3.2974 680.98 0.1600
82 27.15 3.2816 675.53 0.1600
83 27.35 3.2579 675.47 0.1600
84 27.57 3.2331 617.91 0.1600
86 27.89 3.1964 695.20 0.1600
72 25.19 3.5326 735.40 0.1600
87 28.00 3.1837 645.24 0.1600
88 28.17 3.1656 569.65 0.1600
89 28.31 3.1500 591.73 0.1600
90 28.51 3.1278 610.35 0.1600
91 28.69 3.1087 630.31 0.1600
92 28.90 3.0865 623.02 0.1600 A
93 29.19 3.0573 678.06 0.1600
94 29.35 3.0409 552.26 0.1600
95 29.54 3.0220 654.81 0.1600
96 29.73 3.0030 631.89 0.1600
97 29.97 2.9793 642.40 0.1600
98 30.15 2.9621 665.22 0.1600
73 25.42 3.5015 795.55 0.1600
71 24.99 3.5602 728.99 0.1600
44 20.59 4.3105 825.78 0.1600
56 22.53 3.9437 724.86 0.1600
45 20.75 4.2781 804.29 0.1600 A
46 21.05 4.2171 835.05 0.1600
47 21.18 4.1920 755.15 0.1600
48 21.30 4.1690 805.57 0.1600
49 21.46 4.1379 803.18 0.1600
50 21.58 4.1153 813.37 0.1600
51 21.71 4.0896 830.37 0.1600
52 21.81 4.0710 818.91 0.1600
53 22.03 4.0309 805.31 0.1600
54 22.22 3.9971 824.34 0.1600
55 22.34 3.9772 802.86 0.1600
57 22.65 3.9218 807.47 0.1600
70 24.88 3.5758 700.54 0.1600
58 22.88 3.8843 755.14 0.1600
59 22.99 3.8653 827.83 0.1600 A
60 23.16 3.8370 744.30 0.1600 A
61 23.32 3.8112 778.60 0.1600
62 23.45 3.7908 710.89 0.1600
63 23.60 3.7674 751.39 0.1600
64 23.83 3.7316 709.07 0.1600
65 23.93 3.7150 706.56 0.1600
66 24.12 3.6873 776.17 0.1600 B
67 24.29 3.6616 714.02 0.1600
68 24.49 3.6315 754.90 0.1600
69 24.71 3.6005 772.85 0.1600
99 30.26 2.9510 794.44 0.1600 A 100 30.44 2.9342 757.12 0.1600 101 30.63 2.9162 732.07 0.1600 102 30.84 2.8969 694.75 0.1600 A 103 30.96 2.8859 701.00 0.1600
134 37.20 2.4153 691.88 0.1600
135 37.45 2.3997 447.61 0.1600
136 37.70 2.3842 472.55 0.1600
137 37.89 2.3723 390.64 0.1600
138 38.13 2.3584 471.21 0.1600 139 38.37 2.3442 456.55 0.1600 A 140 38.54 2.3342 433.93 0.1600 A 141 38.75 2.3219 361.42 0.1600 A 142 38.94 2.3113 482.98 0.1600 143 39.13 2.3002 406.67 0.1600 A 144 39.33 2.2892 410.79 0.1600 B 145 39.52 2.2783 409.94 0.1600 146 39.69 2.2691 375.32 0.1600 147 39.89 2.2581 401.07 0.1600 148 40.02 2.2513 374.86 0.1600 149 40.34 2.2340 512.86 0.1600 A 150 40.56 2.2226 434.00 0.1600 151 40.86 2.2070 418.78 0.1600 B 152 41.11 2.1937 431.88 0.1600 153 41.37 2.1809 422.30 0.1600 154 41.58 2.1704 459.78 0.1600 155 41.79 2.1596 361.24 0.1600 156 42.00 2.1493 358.70 0.1600 157 42.18 2.1407 312.37 0.1600 158 42.35 2.1324 466.88 0.1600 A 159 42.54 2.1233 367.04 0.1600 160 42.73 2.1145 369.97 0.1600 161 42.86 2.1082 337.21 0.1600 A 162 43.02 2.1010 381.62 0.1600 163 43.18 2.0932 321.09 0.1600 164 43.53 2.0773 416.66 0.1600 B 165 43.75 2.0674 390.58 0.1600 A 166 44.11 2.0513 329.46 0.1600 167 44.41 2.0383 331.88 0.1600 168 44.69 2.0262 302.20 0.1600 169 44.93 2.0160 326.77 0.1600 170 45.16 2.0062 391.74 0.1600 171 45.41 1.9957 374.59 0.1600 172 45.64 1.9860 334.24 0.1600 173 46.37 1.9565 361.61 0.1600 174 46.74 1.9421 379.22 0.1600 A 175 46.99 1.9322 357.86 0.1600 A 176 47.68 1.9060 316.79 0.1600 A 177 49.71 1.8327 304.34 0.1600 A,B 178 49.95 1.8242 358.71 0.1600 A 179 50.15 1.8175 302.94 0.1600 180 50.41 1.8087 314.00 0.1600 A 181 50.67 1.8001 301.41 0.1600 182 51.27 1.7803 293.14 0.1600 A 183 52.30 1.7479 317.18 0.1600 184 52.50 1.7418 300.50 0.1600 185 53.26 1.7184 403.74 0.1600 A 186 53.99 1.6970 400.60 0.1600 A 187 54.29 1.6883 376.81 0.1600 B 188 54.60 1.6795 318.12 0.1600 A 189 54.82 1.6732 361.83 0.1600 190 55.13 1.6646 414.67 0.1600 A 191 55.38 1.6576 357.62 0.1600 A 192 55.89 1.6439 300.82 0.1600 193 56.10 1.6381 357.86 0.1600 B
Match! Phase Analysis Report Sample: BAFe-0,5%
20.6 Unidentified peak area
66 Intensity scale factor
34 Peaks in range
W", Journal of Magnetism and Magnetic Materials 62, 57-67 (1986)
Formula sum
Fe2 O3
Entry number
96-901-5066
Figure-of-Merit (FoM)
0.739597
Total number of peaks
13 Intensity scale factor
19 Peaks matched
2.88 Calc. density
1.04 Space group R -3 c
Crystal system
trigonal (hexagonal axes)
Unit cell
a= 5.0249 Å c= 13.7163 Å
I/Icor
4.01
5.363 g/cm³
Reference Collomb A, Wolfers P, Obradors X, "Neutron diffraction studies of some hexagonal ferrites: BaFe~12~O~19~, BaMg~2~-W and BaCo~2~-
I/Icor
Sample Data
Entry number
File name BAFe-0,5%.ras File path G:/tesis/PENGUJIAN DAN KARAKTERISASI/DATA XRD DELOVITA/delovita Data collected Jun 16, 2014 09:09:57 Data range 10.000º - 79.965º Number of points 3501 Step size 0.020 Rietveld refinement converged No Alpha2 subtracted No Background subtr. No Data smoothed Yes 2theta correction 0.11º Radiation X-rays Wavelength 1.540598 Å
Matched Phases Index Amount (%) Name Formula sum
A
48.9 Barium dodecairon(III) oxide Ba Fe12 O19 B
26.8 Hematite Fe2 O3 C
24.3 B2 Ba O4
A: Barium dodecairon(III) oxide (48.9 %)
Formula sum
Ba Fe12 O19
96-100-8329
a= 5.8650 Å c= 23.0990 Å
Figure-of-Merit (FoM)
0.776402
Total number of peaks 186 Peaks in range
107
Peaks matched
1.35 Space group P 63/m m c
Crystal system
hexagonal
Unit cell
B: Hematite (26.8 %)
Search-Match Settings
COD-Inorg REV107951 2014.03.25
Reference database used Automatic zeropoint adaptation Yes Minimum figure-of-merit (FoM) 0.60
0.50 Parameter/influence 2theta
Parameter/influence intensities 0.50 Parameter multiple/single phase(s) 0.50
Selection Crit
Elements: Elements that must be present: O, Fe Elements that must NOT be
38 27.74 3.2134 570.89 0.1600
27 26.01 3.4225 528.76 0.1600 A
28 26.14 3.4058 483.69 0.1600
29 26.34 3.3815 553.55 0.1600
30 26.47 3.3640 566.77 0.1600
31 26.58 3.3514 499.81 0.1600
32 26.68 3.3383 506.84 0.1600
33 26.86 3.3168 563.89 0.1600
34 27.02 3.2968 639.32 0.1600
35 27.22 3.2732 555.68 0.1600
36 27.39 3.2534 562.77 0.1600
37 27.63 3.2263 604.93 0.1600
39 27.91 3.1944 513.34 0.1600
25 25.60 3.4763 516.01 0.1600
40 28.12 3.1708 554.27 0.1600
41 28.23 3.1589 615.01 0.1600
42 28.42 3.1376 542.04 0.1600 C
43 28.56 3.1232 531.05 0.1600
44 28.70 3.1076 590.88 0.1600
45 28.87 3.0905 554.57 0.1600
46 29.12 3.0636 627.95 0.1600 A
47 29.28 3.0481 585.11 0.1600 C
48 29.68 3.0077 586.02 0.1600
49 29.88 2.9884 614.87 0.1600
50 30.05 2.9717 645.40 0.1600
26 25.83 3.4459 602.06 0.1600 C
24 25.50 3.4897 493.06 0.1600 C
All elements not mentioned above
10 23.10 3.8473 557.19 0.1600 A
present: Peak List
No. 2theta [º] d [Å] I/I0 FWHM Matched
1 21.52 4.1259 437.85 0.1600 C
2 21.79 4.0760 505.07 0.1600
3 21.97 4.0433 440.14 0.1600
4 22.14 4.0120 516.14 0.1600
5 22.33 3.9787 462.32 0.1600
6 22.50 3.9492 462.18 0.1600
7 22.61 3.9294 462.94 0.1600
8 22.79 3.8993 494.54 0.1600 C
9 22.91 3.8782 561.78 0.1600
11 23.34 3.8084 625.46 0.1600 A
23 25.29 3.5183 466.51 0.1600
12 23.44 3.7920 515.60 0.1600
13 23.67 3.7560 504.52 0.1600
14 23.85 3.7285 456.93 0.1600
15 23.98 3.7073 495.01 0.1600
16 24.09 3.6914 485.89 0.1600
17 24.26 3.6657 493.14 0.1600 B
18 24.56 3.6217 526.07 0.1600 C
19 24.75 3.5941 536.02 0.1600
20 24.88 3.5762 518.02 0.1600
21 25.06 3.5508 509.09 0.1600
22 25.17 3.5354 570.27 0.1600
51 30.22 2.9549 612.50 0.1600
82 36.25 2.4760 735.23 0.1600 A
92 38.16 2.3567 748.33 0.1600
98 39.30 2.2906 884.68 0.1600 A,B
97 39.15 2.2990 741.07 0.1600
96 38.97 2.3094 908.97 0.1600 A
95 38.80 2.3191 802.59 0.1600 A,C
94 38.54 2.3340 836.69 0.1600 A
93 38.28 2.3493 668.47 0.1600
91 37.99 2.3667 682.94 0.1600 C
83 36.44 2.4635 713.03 0.1600
90 37.86 2.3745 662.81 0.1600
89 37.73 2.3824 737.61 0.1600
88 37.54 2.3939 693.04 0.1600
87 37.25 2.4118 715.78 0.1600 A
86 37.03 2.4259 713.28 0.1600
85 36.92 2.4330 705.65 0.1600
84 36.65 2.4502 735.41 0.1600 C
99 39.53 2.2781 822.62 0.1600 100 39.69 2.2691 892.88 0.1600 101 39.85 2.2603 936.81 0.1600 102 40.07 2.2485 807.02 0.1600 103 40.32 2.2351 761.81 0.1600 104 40.45 2.2282 871.46 0.1600 A 105 40.64 2.2184 929.68 0.1600 106 40.85 2.2074 726.23 0.1600 107 40.98 2.2006 726.54 0.1600 B 108 41.24 2.1871 861.11 0.1600 109 41.37 2.1806 701.80 0.1600 C 110 41.55 2.1716 859.93 0.1600 111 41.73 2.1626 837.28 0.1600 112 41.89 2.1547 903.74 0.1600 C 113 42.09 2.1449 946.26 0.1600 114 42.26 2.1369 907.18 0.1600 115 42.44 2.1280 934.39 0.1600 116 42.71 2.1153 910.15 0.1600 A,C 117 43.02 2.1009 868.86 0.1600 A 118 43.20 2.0926 929.16 0.1600 C 119 43.41 2.0827 894.66 0.1600 120 43.59 2.0747 765.93 0.1600 B 121 43.81 2.0646 881.56 0.1600 C 122 43.99 2.0567 798.11 0.1600 A,C 123 44.20 2.0473 897.03 0.1600 124 44.41 2.0384 960.69 0.1600 125 44.60 2.0300 910.45 0.1600 126 44.79 2.0220 840.00 0.1600 127 44.98 2.0137 891.96 0.1600 A 128 45.12 2.0080 818.68 0.1600 129 45.28 2.0010 711.85 0.1600 C 130 45.44 1.9946 880.41 0.1600 131 45.72 1.9828 770.71 0.1600 132 45.91 1.9752 719.40 0.1600 133 46.19 1.9639 806.46 0.1600 134 46.42 1.9547 860.90 0.1600 C 135 46.62 1.9466 740.57 0.1600 136 46.83 1.9384 876.71 0.1600 A,C 137 47.03 1.9307 833.30 0.1600 C 138 47.24 1.9226 921.19 0.1600 A 139 47.51 1.9124 801.13 0.1600 A 140 47.78 1.9021 749.95 0.1600 A 141 47.98 1.8945 944.56 0.1600 A 142 48.22 1.8856 875.39 0.1600
173 54.67 1.6776 500.69 0.1600 A
174 54.79 1.6741 604.11 0.1600 A
175 54.98 1.6687 596.15 0.1600
176 55.36 1.6583 622.81 0.1600 A,C
177 55.60 1.6516 534.52 0.1600 A 178 55.72 1.6483 527.61 0.1600 A 179 55.91 1.6433 489.54 0.1600 C 180 56.01 1.6405 609.25 0.1600 181 56.29 1.6330 519.69 0.1600 B 182 56.40 1.6302 565.90 0.1600 183 56.61 1.6244 511.15 0.1600 A 184 56.77 1.6204 532.15 0.1600 185 56.89 1.6173 500.71 0.1600 A 186 57.05 1.6131 550.50 0.1600 187 57.34 1.6056 528.97 0.1600 A,C 188 57.46 1.6025 437.38 0.1600 C 189 57.67 1.5972 591.13 0.1600 A,B 190 57.94 1.5903 540.43 0.1600 191 58.22 1.5833 574.77 0.1600 192 58.51 1.5762 511.70 0.1600 C 193 58.77 1.5699 493.26 0.1600 A,C 194 59.12 1.5614 459.81 0.1600 C 195 59.64 1.5490 633.92 0.1600 A,C 196 59.84 1.5444 462.85 0.1600 C 197 60.06 1.5392 530.84 0.1600 A,C 198 60.32 1.5333 533.80 0.1600 A 199 60.83 1.5215 450.39 0.1600 C 200 61.09 1.5158 556.34 0.1600 201 61.36 1.5096 681.02 0.1600 A,C 202 61.82 1.4994 575.34 0.1600 203 62.33 1.4886 650.52 0.1600 C 204 62.69 1.4808 585.33 0.1600 B 205 62.97 1.4748 642.36 0.1600 A,C 206 63.31 1.4678 573.83 0.1600 A,C 207 66.27 1.4092 476.53 0.1600 A,B 208 67.16 1.3927 441.11 0.1600 A,C 209 67.60 1.3847 464.96 0.1600 A,C 210 68.63 1.3665 486.39 0.1600 A,C 211 69.00 1.3600 548.34 0.1600 A,C 212 73.65 1.2852 447.58 0.1600 213 77.20 1.2346 481.51 0.1600 A
Rietveld Refinement using FullProf Calculation was not run or did not converge. Integrated Profile Areas Based on calculated profile Profile area Counts Amount
Overall diffraction profile 871373 100.00% Background radiation 665715 76.40% Diffraction peaks 205659 23.60% Peak area belonging to selected phases -28275 -3.25% Unidentified peak area 179924 20.65%
Peak Residuals Peak data Counts Amount Match! Copyright © 2003-2014 CRYSTAL IMPACT, Bonn, Germany
Match! Phase Analysis Report
Sample: BaFe12O19 KOMERSIL (PELET)
Sample Data
File name BaFe12O19 KOMERSIL (PELET).ras File path G:/tesis/PENGUJIAN DAN KARAKTERISASI/DATA XRD DELOVITA/delovita Data collected Jun 16, 2014 09:10:01 Data range 10.064º - 80.034º Number of points 3501 Step size 0.020 Rietveld refinement converged No Alpha2 subtracted Yes Background subtr. No Data smoothed Yes 2theta correction 0.07º Specimen displacement correction T = 0.00005 Radiation X-rays Wavelength 1.540598 Å
Matched Phases
Index Amount (%) Name Formula sumA 100.0 Barium dodecairon(III) oxide Ba Fe12 O19
16.3 Unidentified peak area
Formula sum Ba Fe12 O19 Entry number 96-100-8329 Figure-of-Merit (FoM) 0.781238 Total number of peaks 186 Peaks in range 101 Peaks matched
75 Intensity scale factor
0.97 Space group P 63/m m c Crystal system hexagonal Unit cell a= 5.8650 Å c= 23.0990 Å I/Icor
A: Barium dodecairon(III) oxide (100.0 %)
W", Journal of Magnetism and Magnetic Materials 62, 57-67 (1986)
Search-Match Settings
Reference database used COD-Inorg REV107951 2014.03.25 Automatic zeropoint adaptation Yes Minimum figure-of-merit (FoM)
0.60 Parameter/influence 2theta
0.50 Parameter/influence intensities
0.50 Parameter multiple/single phase(s) 0.50
Selection Criteria Elements: Elements that must be present:
O, Fe, Ba
2.88 Calc. density 5.363 g/cm³ Reference Collomb A, Wolfers P, Obradors X, "Neutron diffraction studies of some hexagonal ferrites: BaFe~12~O~19~, BaMg~2~-W and BaCo~2~-
25 48.86 1.8626 497.23 0.1600 A
70 61.68 1.5025 575.99 0.1600 A
58 57.88 1.5919 559.67 0.1600
59 57.99 1.5891 498.64 0.1600
60 58.41 1.5786 464.59 0.1600
61 58.75 1.5704 778.57 0.1600 A
62 59.05 1.5630 525.65 0.1600
63 59.37 1.5554 556.37 0.1600
64 59.55 1.5511 572.55 0.1600 A
65 59.87 1.5436 608.91 0.1600
66 60.16 1.5370 597.64 0.1600 A
67 60.42 1.5310 513.97 0.1600
68 60.72 1.5241 624.11 0.1600
69 61.30 1.5110 616.27 0.1600
71 61.95 1.4968 484.00 0.1600
56 57.20 1.6091 996.73 0.1600 A
72 62.22 1.4908 473.13 0.1600
73 62.34 1.4884 455.89 0.1600
74 62.62 1.4824 659.64 0.1600
75 62.88 1.4768 597.08 0.1600 A
76 63.17 1.4708 710.16 0.1600 A
77 63.60 1.4617 801.50 0.1600 A
78 63.91 1.4555 453.18 0.1600 A
79 64.11 1.4515 465.21 0.1600
80 64.36 1.4463 679.25 0.1600
81 64.56 1.4423 565.29 0.1600 A
82 64.79 1.4379 517.31 0.1600 A
83 65.09 1.4318 555.06 0.1600
84 65.48 1.4242 534.17 0.1600
57 57.55 1.6002 563.81 0.1600 A
55 56.97 1.6150 1000.00 0.1600
26 49.45 1.8415 441.12 0.1600
39 53.41 1.7142 691.82 0.1600
27 49.94 1.8248 836.35 0.1600 A
28 50.19 1.8161 450.34 0.1600 A
29 50.50 1.8059 593.97 0.1600 A
30 50.74 1.7978 619.30 0.1600 A
31 51.06 1.7873 630.73 0.1600
32 51.37 1.7772 455.91 0.1600
33 51.63 1.7688 447.12 0.1600 A
34 51.83 1.7626 524.51 0.1600
35 52.23 1.7500 756.99 0.1600
36 52.51 1.7412 476.84 0.1600
37 52.96 1.7275 600.36 0.1600
38 53.20 1.7203 476.05 0.1600 A
40 53.63 1.7075 731.12 0.1600 A
54 56.81 1.6194 831.16 0.1600 A
41 53.91 1.6993 471.28 0.1600
42 54.28 1.6886 631.54 0.1600 A
43 54.59 1.6796 676.91 0.1600 A
44 54.87 1.6720 918.92 0.1600 A
45 55.13 1.6646 585.22 0.1600
46 55.45 1.6558 777.05 0.1600 A
47 55.72 1.6483 812.18 0.1600 A
48 56.01 1.6405 820.39 0.1600
49 56.19 1.6357 568.15 0.1600
50 56.30 1.6328 572.65 0.1600
51 56.40 1.6302 565.88 0.1600
52 56.53 1.6266 548.89 0.1600
53 56.67 1.6231 693.25 0.1600 A
85 65.72 1.4197 552.67 0.1600 A
116 75.09 1.2641 850.27 0.1600 A
117 75.28 1.2613 563.26 0.1600 A
118 75.41 1.2594 617.84 0.1600
119 75.52 1.2579 624.51 0.1600
120 75.71 1.2552 611.93 0.1600 A 121 75.84 1.2534 502.98 0.1600 A 122 76.01 1.2510 613.32 0.1600 A 123 76.21 1.2483 449.00 0.1600
Rietveld Refinement using FullProf Calculation was not run or did not converge. Integrated Profile Areas Based on calculated profile Profile area Counts Amount
Overall diffraction profile 445822 100.00% Background radiation 368911 82.75% Diffraction peaks 76910 17.25% Peak area belonging to selected phases 4136 0.93% Unidentified peak area 72774 16.32%
Peak Residuals Peak data Counts Amount
Overall peak intensity 1070 100.00% Peak intensity belonging to selected phases 63 5.93% Unidentified peak intensity 1007 94.07%
Diffraction Pattern Graphics