Poorly Soluble Drugs and Protein

\
-

Proceeding
Thelohternadonal

I

T

on Pharmaceutics & Pharmaceutical Sciences

Drug Delivery Systems:
From Drug-Discovery, Pre-formulation, Formulation and
Poorly Soluble Drugs and Protein

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:

--.-


Proceeding
*

fl re I lnternational Gorfercme
on Pharmaceutics & Pharmaceutical Sciences
Published and Organized by
Faculty of Pharmacy
Universitas Airlangga

Surabayalndonesla

2014

h-a

The l"t I nternationa I Conference on Pharmaceutics
& Pharmaceutical Sciences Proceedings
ISBN : 97&602-72333-G.o
(Lefter of Natlonal ISBN Agency No. 4127E.8/p/03.2015 Date 18 March 2015)


lst edltion Proceedlng
Publlshed by:
Faculty of Pharmacy UniveBitas Airlangga
Surabaya, lndonesia
Addr€ss:
Kampus B rl. Dharmawangsa Dalam
Surabaya 60286
Phone +52 31 5033710
Fax +62 31 5020514
Website: www.icpps2ol4.com or www.ff.
Email: [email protected]

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PREFACE

From Chairman

It is our

pleasure to present you the proceedings of The 1st lntemational Conference on
Pharmaceutics and Pharmaceutical Sciences (ICPPS) oBanized by The Faculty of Pharmacy
Universitas Airlangga Surabaya lndonesia.
The proceeding was produced based on papers and posters presented at The 1st lntemational
Confurence on Pharmaceutics and Pharmaceutical Sciences (ICPPS), held in Sunbaya, lndonesia, 1415 November2014.

The proceeding clearly reflects broad interest, from the participants thatcoming fmm allaround the
world.
The papers presented were pharmaceutics and biopharmaceutics; requirements on how to e\raluate

molecules in discovery and their appropriateness for selection as potential candidate; their
development in context of challenges and benefits, together with associated time and cost
implications and also requirements to progressthrough pre{linieland clinical.
ln this an opportunity, I would like to express my appreciation to the editorialteam ofthe proceeding
who hrve been workin8 hard to review manuscripts, and makingthe first edition ofthis proceedin8
be possible.

I would like also to thanks to all invited speakers and presenters who participated in The lst
lnternational Conference on Pharmaceutics and Pharmaceutical Sciences (ICPPS) and your
mntribution to this proceeding.
Finally,

I hope this proceeding will give contribution to the Pharmaceutics and Pharmaceutical

Sciences research.


Chairman,

Dra. Esti Hendradi, MSl,, Ph.D., Apt

COMMITTEE

Advisor
Chairman

: Dean of Faculty of Pharmary Universitas Airlangga
: Dra. Esti Hendradi, M.Si., Ph.D, Apt.

Editor

: Dr.

Wouter U. Hinrichs (Netherlands)

Prof. Kozo Takayama (Japan)


Mutalik (lndia)
Dr. Nuttakorn Baisaeng (Thailand)
Prof. Dr. Widji Soeratri, DEA (lndonesia)
Dr. Srinivas

Committee

Prof. Dr. Widji Soeratri, DEA, Apt.
Prof. Dr. Siswandono, MS., Apt.
Prof .Dr. Tutuk Budiati, MS., Apt.
Prof. Dr. rer.nat. Muhammad Yuwono, MS., Apt,
Drs. Hadi Poerwonq MSc.,Ph.D, Apt.
Drs. Marcellino Rudyanto, MSi., Ph.D, Apt.
Drs. Bambang Widjaja, M.Si, Apt.
Drs. Sugiyartonq MS, Apt.
Dra.Tutiek Purwanti, MSi, Apt.
Dra.Tristiana Erawati, MSi, Apt.
Dra.Retno Sari, MSc, Apt.
Dra.Dewi lsadiartuti, MSi, Apt.
Dra.Noorma Rosita, MSi, Apt.

Dr. Dwi Setyawan, SSi, MSi., Apt.
Dr. Riesta Primaharinastiti, SSi, MSi, Apt.

Dewi Melani Hariyadi, SSi, M.Phil., Ph.D, Apt.
Helmy Yusuf, SSi, MSc., Ph.D, Apt.
Dr. rer. nat. Maria Lucia Ardhani Dwi Lestari, SSi,MPharmSci., Apt.

Melanny lka Sulistyowati, SFarm, M.Sc, Apt.
Febri Annuryanti, SFarm,M.Sc, Apt.
M. Faris Adrianto, MFarm, Apt.
Dini Retnowati, SFarm,Apt.
Abhimata B SFarm, Apt.

of CONTENT

TABI,T

Preface from Chairman

Committee


tl

Table of Contents

iii

Author lndex

iii

AUTHOR INDEX
COMPARISON OF SODIUM STARCH GLYCOLATE AND CROSSCARMELTOSE SOOIUM AS
SUPERDISINTEGRANT IN MEFENAMIC ACID FAST DISINTEGRATING TABI.ET
Adeltrudls Adelsa D, Oktavia Eka Pusplta, Amalla Ayuningtyas, Marulita lsadora

1

STUDY EXPRESSION OF HUMAN ERYTHROPOIETIN EXPRESSSION IN MAMMAUAN CELL
Adl samoso, Popl Hadiwisnuwardhani, Yana Rublana, Yulalka Romadhani, Endah Puji

Septisetyanl, Dyanin$yas D,P, Putri

4

ANTIOXIDANT STABILITY ASSAY OF ATPHA TOCOPHERYI- ACETATE IN SOLID LIPID NANOPARTICLE
SYSTEM

AnSEie

(t,PlD eqSE BEESWAX AND MONOSTEABIC 6LISEBYL 50:50)

wldhi, Noorma Rosita, lMdii Soe6tri

..............,.....

A BIOACTIVE SOYINE HYDROXYAPATITrcETATIN

..,............,...,.,... 8

IMPLANT FOR IN VITRO GENTAMICIN RELEASE

13

Anlek s€dya Budiatn, M. zainuddin, Junaidi Xhotib, Diah Himawati

EFFECT OF COMPARISON SURFA TA T AND @SURFA TANT IN WATER/OII, MICROEMUTSION IN
REEASE OF OVALBUMIN Microemulsion Water/Oil with Surfactant (Span SGTween E0) :

t'"

,'t,

.nO
Cosu rfactant (Ethanol) =S'1
Anisa Rizki Amalla, Riesta Primahadnasbti, Esti Hendradi
ANALYSIS OF

MYcotlc

ACIDS CTEAVAGE PRODUCT OF


18

MycoDocterium tuberculosis BY GAS

CHROMATOGRAPHY-FIAME IONIZATION DETECTOR

Asrl Darmawati, Deby Kusumaningrum, lsnaeni, Muhamad Zainuddin

2l

PERIPI"ASMIC EXPRESSION OF GENE ENCODING ANT!EGFRvlll SINGLE-CHAIN VARIABLE FRAGMENT

ANTIBODY USING PelB TEADER SEQUENCETN ES6HER|CHIA cOLl

Kartika Sari Dewl, Debble Sofie Retnoringrum, Catur Riani, Asrul Muhamad Fuad

24

IN VIVO ANTIMALARIAL ACTIVIry OF ETHANOL EXTRACT AND ETHYT ACETATE FRACTION OF

Aledryon serrotus LEAVES ON Prasmodrum berghei INFECTED MICE
AW Widyawaruyand, Uswatun Khasanah, Lldya Tumewu, Hilkatul llmi, Achmad Fuad Haffd,
...........'.............. :lO
lndah 5 Tantular ...
PROFILE OF COMMUNITY PHARMACISTS KNOWLEDGE IN PATIENT ASSESSMENT WITH INFIUENZA

SYMPTOMS AND ITS PRODUCTS
Azza Faturrohmah, Atle Sullstyetlni, Ana Yuda

33

soLUBtLtTy AND DTSSOLUTTON SrUDY OF KETOPROFEN
lNcLUslON COMPLEX (Prepared by Kneading Method)

Bambant Wdrala, Achmad RadJaram, Arafah Zulhana

-

HIDROXYPROPYL-p-CYCLODETTRIN

,,.....

,..........'.......... 37

FORMUTATION AND STABILITY TESTING OF MELOXICAM SOLID DISPERSION GEL

Budlpntlwl Wlsudyantnlsih, lnka Dewl Nur Angraraini, Fersiya Wardani
EFFECT OF MENTHOL AS PENEIRATION ENHANCER TO DICLOFENAC

40

SODIUM MEMBRANE-ryPED

TRANSDERMAT PATCH CHARACIERIZANON

Destrla lndah Sarl, Esd Hendradl, Junaldl Khodb

43

PHYSICAL CHARACTERISTICS AND RELEASE STUDY OF OVATBUMIN FROM ALGINATE MICROSPHERES
PREPARED BY DIFFERENT CONCENTRATION OF ALGINAIT AND 8aCI, USING AEROSOLIZATION

TECHNIQUE

Dewl Melanl liarlyadl, Trlsdana

El"yrti, sisilia Ermavahyuningtyas

45

MUCOADHESIVE TABLET OF ETHANOLIC EXTRACT OF SAMBILoTo (Andrographis paniculata)
AS ANTIDIABETIC USING CHITOSAN

Dhadhang wahyu Xumlawan, Henlng Pratiwi, and Uryga lkaditya

50

PHYSICAT INTERACTION STUDY OF IBUPROFEN.STEARIC ACID BINARY MIXTURE

Olalent Putrl Paramlta, Dwl Setyauran, Dewi lsadiartuti

....

.,.,..............,.... 59

MoLEcUtAR MoDELING AND SYNTHESIS oF 1-(3,+Dichlorobenzoyl)-1,3-dimethylurea
DIan Agun8 Pangarlbowo, Slswandono, BambangTri Purwanto

63

EXPRESSION OF RECOMBINANT HUMAN GRANULOCYTE{OLONY STIMUTATING FACTOR WITHIN
PERIPLASMIC COMPARTMENT OF Esc,}ench,o

coli USING PeIB LEADER PEPTIDE

Dlrn Fitrh Atxr3tvantl, Aerul Muhamad Fuad ,--**----.-

..,,.,,..,...,..,,....*

EVALUATION OF ANTIHYPERURICEMIC ACTIVITY FROM BULBS OF BAWANG TIWAI lEleutherine
BY lN VITRO ANO lN VIVO STUDIES

polmifolld (Ll Merr.,

Dlan Radh laksmltawaq Rlnlnta Firdaus, \tulinda, Mediana Asdka

72

lFrogorio x ononosso Duch.) AND SfARFRUff {Averrhod carombolo L.} USING ABTS
SCAVENGING METHOD

Dhna Sedahwaty, lndira Natalia

Timang

FREE

RADICAI

..,.....,...,...,.,.. 76

ENHANCEMENT OF SOLUBILrIY AND DISSOLUTION ATORVASTATIN BY MICROCRYSTATLIZATION
METHOO

Dollh Gorall, Yoga Windu wa.dhana, Ronny Tandela

79

lrv yrIRO ANTIMAIARIAL ACrIVITY OF DICHLOROMETHANE SUB-FRACTION OF Eucalyptus globulus
L, Stem AGAINST P,osmodium folcipdrum
Ells Suwarnl, Achmad Fuad Hafid, Aty WidyawarutBnti
86
Arcongelisid llavo INCREASES RATS' LEUKOCYTES BUT HAS BIPHASIC EFFECT ON RATS' LYMPHOCYTE
Endah Puspitasari, Evi Umayah Ulfa, Vlta Arlatl, Mohammad SuhhonHabibi
E9

IN V]TRO ANTIMAIARIAL ACTIVITY OF CHLOROFORM SUBFRACTION OF sALAM BADAK LEAVES
lAcme na ocu m i noti ssi mol

Erna Caf,vanlwslh,
CHARACTERIZATION

A&Drd Fud Htfd, Aly l,yidyawaruyanf ....,.,........................................92
OF DOSAGE FORM AND PENETRATION DICLOFENAC SODIUM WITH

MICROEMULSION SYSTEM lN HPMC 4000 GEL BASE (Micmemulsion
Span 80 - Tween 80 : Cosurfactan Ethanol 96% = 5:1)

WO with rasio

use of surfactant

Estl Hendndl, Tudek Purwar*i, lGrina Wahyu lrawad

95

CONSTRUCTION AND VALIDATION OF THE STRUCTURE.BASED VIRTUAL SCREENING PROTOCOts
WITH PDB CODE OF 3LN1 TO DISCOVER CYCLOOXYGENASE.2 INHIBITORS

Mumpunl

E,

Nurrcchmad A, Pranowo HD, renie UA lstyastono EP

99

VALIDATED UV SPECTROPHOTOMETRIC METHOD FOR THE DETERMINATION OF ASPIRIN IN RABBIT
PIAsMA : APLICATION TO BIOAVAILABIIITY STUDY OF ASPIRIN MICROCAPSULE lN RASSIT

toz

Falzatun, Novl yantih, Teguh lman Saputra

EFFECT OF COMPARISON OF SURFACTANT AND COSURFACTANT WO MICROEMULSION OVALBUMIN
WITH SOYBEAN OILTO PHYSICOCHEMICAL CHARACfERIZATION (w/o Microemulsion with Surfactant
Span 8G Tween 80 : Cosurfactant Ethanol96% = 5:1; 6:1 and 7:1)
Farlda Mutlara Sarl, Rlesta Prlmaharlnasttd, Esd Hendradi
105

pH INFLUENCE IN DESATTING PROCESS OF CRUDE PERTUSSIS TOXIN (PT) AND FILAMENTOUS
HEMAGGLUTININ (FHA) PURIFICATION FROM Bordetello pertussis BY SEPHADEX G-25 COLUMN
CHROMATOGRAPHY
Faris Adrlanto, Esd Hendradl,

tlenl ,{uElny, lsnaeni

108

SEPARATION OF COSMETIC PRESERVATIVES USING SILICA-BASED MONOLITHIC COTUMN

Febri Annuryanti, Riesta Primaharinastiti, Moch. \tuwono

111

PREPARATION AND CHARACTERIZATION OF TELMISARTAN.CITRIC ACID CO.CRYSTAL

Fikri Alatas, Hesdary Ratih,

Sundani umno So€wandhie

114

PATIENTS' AND CAREGIVERS' LIQUID MEDICATION ADMINISTRATION ERRORS

Gusti Noorrizka vemnika Achma4 Gesnita Nugrahenl

.,.,

,...,.......,......,.... 117

THE POTENCY OF CANARIUM OIL (Conarium indicuml AS A MATERIAL FOR STRUCTURED LIPID
PRODUCTION

Hamidah Rahman, Johnner

P

Sitompul, lfusnandar Angtadiredja, Tutus Gusdlnar .,........,.,.. 121

EFFECT OF TREHALOSE ON THERMAL PROPERTIES OF PHOSPHOTIPID-DDA AND TPGS MIXTURES

Helmy Yusuf

.......,.

,.,...,..,.....,..,,.,,, 124

PEEPABATION AND CHABACTEB'ZATION OF FLUKONAZOLE.9.CYCLODEXTRIN INCLUSION COMPLEXES

Hestiary Ratlh, Flkrl Alatas, Erin xarlina

L27

ISOLATION AND IDENTIFICATION OF ANIIOXIDAI{T COMPOUND BY BIOPRODUCTION OF
ENDOPHYTIC FUNGI OF TURMERIC (Curcuma longo L.l ISOLATE CL.SMl.RF11

Hindra Rahmawati, Bustanussalam, Partomuan Simaniuntak

130

MODIFICATION PROCESS OF NATURAT CASSAVA STARCH : THE STUDY OF CHARACTERISTICS AND
PHYSICAT PROPERTIES

Prasetia, Jemmy A, C,l.S, Arlsanti, I{.P.P,A. Dewl,

6-A.i. Astutf, l{,W,il Yulianiqsih, I M.A.G.

Wirasuta

133

ORUG USE PROFILE OF DIABETIC PATIENTS IN EAST SURABAYA PRIMARY HEALTH CARE
I ilyoman

wijata, A:ra Fatunohmah, Ana Yuda, Mufartlha,

Hlkmah Prasasti

t'1,

Tesa Geoyanl santoso, Dlna xartlka,

Whanni Wido Agustin

136

GLYCINE MAX DETAM II VARIEry AS PREVET{TIVE AND CURATIVE ORGAN DAMAGE DUE TO
EXPOSURE TO ,LEAD (Pb)
Rlka Yulla, Sylvan Septian R6sandy, Gusd AW Putu Puspikaryani, I Putu Atus Yulyastr"wan, D€wa

lq2

AW Kusuma Dewi

AN ACTIVITY TEST OF MATOA LEAVES EXTRACT AS HEART RATE FREQUENCY REDUCTION WITH
ADRENATINE INDUCTION

lk

t4

Purwldy.nlntrum, Elln Yulinah Sukandar, lda Fidrianny

EFFORT TO REDUCE COMPRESSIBITITY OF RAMIPRILTHROUGH CRYSTAT ENGINEERING

lnd6, Smdanl

N

So€sendhi

..-.,,.,...*..*

1|7

IN VITRO ALPHA-GLUCOSIDASE INHIBITORY ACNVIY OF ETHANOLIC LEAF EXTRACT AND FRACNONS

Rouvofio seryenliino (1.) Benth. ex Kurz
Julle Anne D. Bolaftos, lvan L Lawag
OF

.,

.........,............ 15o

PERIPTAsMIC EXPRESSIOI{ OF GENE ENCODING AI{TFEGFRVIII SIN6I.E{HAIN VARIABI.E FRAGMENT

ANTIEO0Y USING PelB LEADER SEQUENCEIN Escherichio coli
(artika Sari Oewi, Debbie Sofie Retnoningrum,catur Riani, Asrul Muhamad Fuad ...,.,,....,. 153
CHARACTERIZATION

AND LD- VALUE DETERMINATION OF

1,s-bis(3'-ethoxy{'-hydroxyphenyl}-1,4-pentadiene.3-one
testarl Rahayu, Septian, Esti

(EHP)

Mumpuni,

,..,..,.,.,........ 159

DEVELOPMENT OF MELOXICAM TRANSDERMAT MATRIX TYPE PATCH USING
POLWINYTPYRROI-IDONE, HYOROXYPROPYL METHYTCELTULOSE, AND ETHYI- CELI.ULOSE

COMBINATION

t62

tldya Am.llana, Monica lwud, Selly Rlo
ANTIHEPATITIS C VIRUS ACTIVITY SCREENIN6 ON

Harpul,io orboreo EXTRACTS AND ISOLATED

COMPOUND
Lldya Tumewu, Evhy Apryani, Mei Ria Sant, Tutik Srl Wahyuni, Adita Ayu Permanasa4

Myma Adlantl, Chle Aoki, Aty Widyawarufanti, Adrmad Fuad Hafd, Maria lnge Lusida,
......,.....,....... 165
Hotta

Soetjipto, Hak

HPLc METHoD PRECISION TO ASSAY OF A-MANGOSTIN lN Mangosteen (6orc,nia mongostano L.l
FRUIT RIND EXTRACT FORMULATED IN ORAL SOLUTION

Liliek Nurhidafat, Siti Sofiah, Ros Sumarny, Xevin

Caesar.

....,......,,....... 168

;qiPARATION AND CHARACTERIZATION OF NARINGENIN.LOADED CHITOSAN NANOPARTICLES FOR
OiEMOPREVENTION
Lira lMnarti, Lusla Oktora Ruma Kumala Sari
t70
IE'.ATIONSHIP OF KNOWLEDGE AND PATIENT BEHAVIOR ON SELF MEDICATION PIROXICAM

i Sludies of Pharmacy in Sukun District, Malang City)
Ljza Pristianty, Reshtia Erlana Putd, Hldayah Rachmawatl

t7t

iFFECT OF CHRONIC USE OF ENEBGY DBI'IX ON XIDNEY

tlahardlan Rahmadi, Zamtotul lzzah, Mareta Rindant A, Aniek Setya
SCREENING OF SURFACE MODIFIERS TO PRODUCE

GUIDANCE

Mada Lucia Ardhani

B,

Suhadono ........... 176

SIABE NANOSUSPENSION : A GENERAI

llxi l€stari ..,......

............,......... 179

,EVETOPMENT OF SIMPLE POLYPHENOL SENSOR BASED ON SODIUM META PERIODATE AND 3.
METHYT-2.BENZOTHIAZOLINONE HYDRAZONE FOR COFFEE SAMPLES

t

och. Amrun

Hidayat

indya Pusp'rtaningtyas, Agus Abdul Ganl, Bambant Kuswandi ...,.. 181

VALIDATION OF AN HPLC ANALYTICAL METHOD FOR DETERMINATION OF LEVOFLOXACIN IN
OPHTHALM IC PREPARATIONS

Mochamad Yuwono, Riesla Primaharlnastiti, Ateng Teguh Wbrdoyo
VAUDATION OF SPECTROPHOTOMETRIC
IN TABLET DOSAGE FORM

Nia Xrlsfnlntrum, Diah Yuli ParyEsti

184

M€THOD FOR ESTIMATION OF EPERISONE HYDROCHLORIDE

...

..,...,.......,..... 187

ANNOSTEOPOROTIC ACNV|TY OF 96% ETHANOUC EXTRACTS OF ABELMOSCHUS MANIHOT LMEDIK
LEAVES AND EXERCISE ON INCREASING BONE DENSITY OF FEMALE MICES FEMORALTRABECULAR

190

Niliestria Ayu Faramitha Sholikhah

EFFECT OF {YCTODETTRIN ON sPF VALUE AND INHIBITION OF KO.,IC ACIDSTYROSINASE ACTIVTTY
IN VANIsHING CREAM BASE FORMUTATION (ON SUNSCREEN PRODUCT CONTAINED OXYBENZONE)

Noorma Rosita, Diana, Diana winarlta, Tristiana Erawati, Wldji sroeratrl

193

ANTIMICROBIAL ACTIVITY OF LACTOBACILLI PROBIOTIC MILK AND GUAVA I FAF ETHANOLIC EXTRACT
(Psidium guajava) COMBINATION AGAINST BACTERIAI CAUSE OF DIARRHEA

197

ur Putri Ranti,lsnaeni, Juniar Moechtar, Febri Annunranti
THE INTTUENCES OF PARTICTE SIZE AND SHAPE ON ZEIA POTENTIAL OF COENZYME Q1O

NANOSUSPENSION

Nuttakom

Baisaeng

.......'.'.'....'... 200

SYNTHESIS, MOIECUTAR DOCKING, AND ANTITUMOS ACTIVITY OF

Dimethylurea AGAINST HUMAN BREAST CANCER CELL LINE (MCF-7)'\I,NLDibENZOYI-N,NL
..".'......'........ 203
Nuzul walryuning Diyah

.........,..,....,....

EXPRESSION OF ANII-EGFRVIII SINGLE CHAIN FRAGMENT ANTIBODY (SCFV)ON THE SURFACE OF

PICHIA PASTORIS

hlka vio&rfi,

Asrut Muh.m.d Fuad,

tuftarsono

.'...'..'.'.---.'.

z)5

SUBCLONING OF csf3syn (COLONY SnMULATING FACTOR-3) GENE INTO pGAPZ? AND
TRANSFORMATION OF RECOMBINANT VECTOR INTO PICHIA PASTORIS

Prety lhda Arfia, Asrul Muhamad

Fuad

,...............,...212

THE USE OF PERICARP MANGOSTEEN (Garcifiia mangostana
CREAM-TYPE O

L) EXIRACr lN

FORMUTATION OF

/W

Rahmah Elfiyanl, ilaniek setladi Radjab, Mla Sadta soffan ,.,.,.....,.,...,,.........,...,...,,..,...,... 218
CHITOSAN BASED PARTICULATE CARRIER OF DITIRPENE LACTON OF SAMBILOTO PREPARED BY IONIC
GELATION-SPRAY DRYING :EFFECT oF STIRRING RATE AND NOZI..E DIAMETER

Retno Sad l-run Suhartanti, Ihxt Setyawan, Esd Hendrrdl, WUI Soeratrt.-.--

*--.*---.....2X2

GAS CHROMATOGRAPHY-MASS SPECTROMETRY METHOD VALIDATION FOR PESTIODES RESIDUES
ANALYSIS IN FOOD USING QUEChERS KIT

22s

Rlesta Prlmaharinastid, Setyo Prlhatinlngty'.s, Mochammad Yuwono

CHARACIERIZATION OF PARACETAMOL ORAUY DISINTEGRATING TABLET USING GEI.ATIN 1% ANO 2%
AS BINDER AND POLYPTASDONE XL-1O 10% AS DISINIEGRANT (Prepared by Freeze Drying Method)

Roisah Nawadla, D{ri Setyawan. Bambant wldjaja

230

ANTIox|DANT STUDY oF COSOTVENT SOLUTION OF MANGOSrEEN (Garcinia manBostana L) RIND
EXTRACT IN RATS BY USING MDA PARAMETER
Ros Sumamy, Liliek ,{urhldafad, Yat Sumlyati, Fransiska Dlana Sanii...........,......,.,...,.,.,.,. 233
SCREENING OF SELECTED PHILIPPINE ROOT CROPS FOR ?-Glucosidase INHIBITION

SaEh Jane

S.

Almazora, lrran L Lawat

...

............,...... 236

NIOSOME EMULGEL FORMUTATION AND STABLITY TEST OF CINNAMON (Gnnamomum burmanii
Nees & Th. Nees) Eark ETHANOIIC EXfRACf AS ANTIoXIDANT
Sasand Dariianto, Fldrhni |rda, Widhita

Pff

239

THEOPHYLTINE RELEASE FROM SUSTAINED RELEASE TABLET USING LACTOSA AND PVP K3O A5 A
CHANETIING AGENT
Sugiyartono, Retno sari, Agus Syamsur Rlral, TriMuhanl, Atustin Maharani
242
EFFORTS TO PRODUCE 1-(EENZOYLOXY)UREA

AS ANTICANCER DRUG CANDIDATE

suko Hardjono

245

DEVELOPMENT OF PEGYIAtEd RAPAMYCIN LITHOCHOTIC ACID MICELLE FOR CANCER THERAPY

Ann Tapsirl, Kanokwan Jaiprasert, Rungtip Nooma, Awadseda Sukgas€m, Supang Xhondee

2Q
FEASIBILITY OF ORAL IMMUNIZATION AGAINST JAPANESE ENCEPHALITIS VIRUS USING CHITOSAN
PARTICLES

Supavadee Boontha, Worawan Boonyo, Hans E. Juntinger, Tasana Pitaksuteepong,
Neti Waranuch, Assadant Polnok, Narong Nitatpattana, Sutee Yokan

251

AT ORTHO ( o ) AND PARA ( p ) POSITIONS
MET1LBENZOAT AGAINST SYNTHESIS OF HIDROKSIBENZOHIDRAZIDA DERIVATIVES

THE INFLUENCE OF HYDROXY GROUP

&.Eana, Adita

& Melanny lla

.S.

oN

Junl Etowati, Marcellino Rudyanto, Hadl Po€rwono,

Tutuk Budiati

254

ANTIOXIDANT ACTIVITY TEST OF BEE PROPOLIS EXTRACT (Apis mellitura L.) USING DPPH (1,1diphenyl-2-picrilhidrazyl) FREE RADICALS SCAVENGING ACnVIW

fitiek Martati, Shahyawidya
CAPSULE FORMUTATION

and

258
EVALUATION COMBINATION OF AQUEOUS EXTRACT OF Phaleria's

(Phaleria macrocarpa (scheff Boero) FRUITS and LEAVES as ANTIHIPERTENSIVE AGENT

IlTlSli:T-Y:Y-::::11:]:1::**:::::::::Y:::::::::l;
MANUfACTURE AND CHARACTERIZATIOI{ OF SOTIO OISPERSION GLIKTAZI} PVP K9O
,......,.,......,.. 264
H Sutama, Fikri Alatas, Clcih Aw ,{lngslh

...................

T.ita

ANTI]NFIAMMATORY ACTIVITY OF PARA METHOXY CINNAMIC AOO (PMCA) IN NANOEMUTSION
USING SOYBEAN OIL
Tristiana Erawati M, Annele lndraswarl P, anda Ghemasih .c, t{oorma Roslta, suwaldl
M

26

artodihardio, Widii Soerattl

PHYSICAT CHARACTERISNCS AND PENETRATION OF DICLOFENAC SODIUM NIOSOMAT SYSTEM
USING SPAN 20 AND SPAN 60
Tutiek Pururand, Esti Hendndl, Noverlka A. Putrl, ,{urtya r,

Dfli ......,.......,...,......,......,..,... 271

FORMULATION AND CHARACTER,SZATION OF JUICE OF LIME GEL USING CMC.NA BASE

275

Uswatun Chasanah, Estl Hendradl, lnayah
HEPATOPROTECTIVE ACTIVITY OF Bidens pilosa L. lN CARBON TETRACHLORIDE INDUCED
H

EPATOTOXICITY IN RATS

274

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CYTOTOXIC ACTIVITY ASSAY AGAINTS HEIA CELL LINES oF NoVEt ANTICANCER DRUG i N(PHENYLCARBAMOYT)ISOEUTIRAM IDE

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297

OF ATTAPULGITE

303

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@wffio*

Proceeding
Itelohrtenradonal

Gonfiercnce

on Pharma€euti€s & Pharmaceutical Sciences

IN VITRO ANTIMATARIAT ACTIVIW OF CHTOROFORM SUBFRACTION
OF SALAM BADAK TEAVES (Acmena acuminatissima)
Erna Cahvaninrsih. Akademi Farmasi Saraswati, Denpasat Eali; A(bn3C-flltC-lhfd. Depanment of Pharmacognosy and Phytochemistry Faculty of Pharmary, Univecitas Airlangga, Surabaya 60826, lnstitute of Tropical
Disease, Universitas Airlaogga, Surabaya 60115; AElflidaBllyeli., Department of Pharmacognosy and Phytochemistry Faculty of Pharmacy, Universttas Airlangga, Surabaya 50826, lnstitute of Tropical Disease, Universitas
Airlangga, Surabaya 50115, [email protected]

INTRODUCTION
Malaria is still an endemic disease in more than

Fractionatlon

90 countries, mainly in developing countries

the fractionation

(Sanchez et a1.,2004). Patients infected with
malaria have doubled in the last two decades.

A.acuminatissima leaves was separated by
vacum liquid chromatography (VLC) using
heune, chloroform, and ethanol at gradient
condition. This separation was produced six
subfractions, then evaporated using a vacum
evaporator and dried. These six subfractions
was then analyzed by TLC and tested for anti-

This occurred mainly due to the emergence
of resistant strains of Plasmodium falciparum
malaria to the chloroquine and its derivatives
(Trape et al.,2OO2l. Perez et al. (1997) stated

that the global spread of malaria parasites
that are resistant to current antimalarial drug
is a major health problem. Therefore, it is need
to find new antimalarial substances to replace
current drugs that are not sensitive anymore.
One attempt to discover new antimalarial substances is through active exploration of the
natural sources,
It is known that some species of the family
Myrtaceae has an antimalarial activity. Previ-

ous $udies shown that ethanol extract and

chloroform fraction

of A. acuminatissima

leaves (Myrtaceael were exhibited antimalarial activity with lC50 value of 0.040 gglml and
0.005 pg/ml, respectively. Therefore, the separation ofthe chloroform fraction was done to
determine the antimalarial activity substances

of A.acuminatissima.
MATERIALS AND METHODS

Plant materials
A.acuminatissia leaves was obtained from
Purwodadi Botanical Garden on December
2012. Sample was authenticated by the authority of Purwodadi Botanical Garden, Pasuruan, East Java.

92

Chloroform fractions which obtained from

of

ethanol extract of

malarial activity.
ln vitro antimalarial activity test
Antimalarial in vitro test was performed based
on Budimulya et al. (1997). Sample prepared
in serial dilution at concentration of 0.01; 0.1;
1; 10 and 10O Eglml in microwells. Each microwell was added with 50O El parasite culture
(1% parasitemia, 5% haematocrit) and incubated for 48 hours in 37oC. After incubation,
thin blood smears were made and stained
using 20% giemsa dye. Percentage of parasitemia was determined by countinB infected
erythrocytes per L000 total eMhrocytes under microscope.
RESULTS

AND DISCUSSION

The separation results of A.acuminatissima
leaves chloroform fraction was produced
six subfractions (A-F). Each subfraction was
tested for in vitro antimalarial activity against
P falciparum (3D7). According to Rasoanaivo
et al. (2004), an extract is very active if lC50 <
5 E/mL, active 5 prglmL < lC50 < 50 gglml,
weakly active 50 Uglml < lC50 < 100 Uglml
and inactive lC50 > 100 Ug/mL. The test re-

koceeding
ft clo hteration* Gonfrrcr

@wffio*

on Pharmaceutirs & Pharmaceutical Sciences

sults showed that all chloroform subfractions
classified as very active and subfraction E was
the most active with lC50 value of 0.007 pgl
mL. The result of antimalarial activity test of
chloroform subfractions (A-F) can be seen in
Table 1.

Figure 1. TLC chromatogram of chloroform
subfraction using silica gel F254 as stationary phase and chloroform-methanol (98;2) as
mobile phase, viewed under UV light : (a) 254
nm; (b) 366 nm; (c) after sprayed with 10%
H2SO4 and heated at 1o5oc for 5 minutes. (d)

ldentification of chloroform subfraction was
performed by TLC method using silica gel
GF254 as stationary phase and chloroform:
methanol (98:2) as a mobile phase. Then observed under UV light in wavelength of 254
nm, 366 nm and sprayed with H25O4 10%. TLC

366 nm after sprayed with 10% H2SO4 and
heated at 105oC for 5 minutes; K = chloroform
fraction, A-F = subfraction.

chromatogram profile showed that allsubfractions contain purple spot (Fig.1). According to
sharifa et al. 120!21, terpenoid compounds
will form a pink to purple or violet after being
sprayed with lV/o HZSO4.lt can be considered
that all subfractions were containing terpe-

Subfraction A-F were exhibited antimalarial
activity (1c50 value of 0.007-1.469 Bglml) and
containing terpenoids substances. Based on
that result, it is possible to conclude that antimalarial activity of subfractions was derived
from terpenoids substances.

i---1

= considered to contain terpenoids.

noids.

coNctustoN

lc,

Sub

ogr1

(rahl)
lm

l0

I

r)

0l

0.01

100

100

15.32

6J,III

56.19

0.0t2

B

1fi,

81.39

63.95

47 69

24.32

0.158

C

86.41

83 94

41.38

l5.l?

20.40

I -469

D

9690

92.48

64.81

15.5

26.40

o.t7z

E

loo

E5

?0

''t0.42

69_E4

56.75

0.m1

F

97.19

er.1r 68rr

59 8t

54.61

0.0t4

I

Table 1. lC50 values of Chloroform subfractions against P falciparum 307

Iti
i\\ltcl)|l
c

h

Subfraction E of A.acuminatissima Ieaves was
the most activ€ as antimalarialwith lC50value
of 0.007 uglml. The antimalarial activity was
possible derived from terpenoids substances.
Further study needed to isolate and identify
the active compounds from A.acuminatissima
ACKNOWLEDGEMENT
The authors acknowledge Satreps Lab-Natural

Product Medicine Research Development Division, lnstitute of Tropical Dlseases Universitas Airlangga for suporting this research.
RIFERENCES

1.

2.

l:-------.--t --'---

K-\
I

BCD

d'

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Perez, H., Diaz, F., Medina, jD.,
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net-nen*oatGorirrgp
on Pharmaceutics & Pharmaceutical Sciences
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