CHAPTER 1: INTRODUCTION CHAPTER 2: LITERATURE REVIEW CHAPTER 3: METHODOLOGY CHAPTER 4: RESULTS AND DISCUSSION CHAPTER 5: CONCLUSION AND RECOMMENDATION

v TABLE OF CONTENT Abstrak i Abstract ii Dedication iii Acknowledgement iv Table of Content v List of Tables x List of Figures xi List of Abbreviations, Symbols and Nomenclatures xiii

1. CHAPTER 1: INTRODUCTION

1

1.1 Background of study

1 1.2 Problem statement 2

1.3 Objectives

3 1.4 Scope of study 3

2. CHAPTER 2: LITERATURE REVIEW

4

2.1 Glass waste

4 2.1.1 Definition of glass 4 2.1.2 Definition of glass waste 5 vi 2.1.3 Type of glass 5 2.1.4 Soda lime glass 6 a Chemical composition 7 b Characteristics 8 c Application 8 2.2 Natural waste 8 2.2.1 Definition of natural waste 8 2.2.2 Spent Bleach Earth SBE 9 2.2.3 Studies on SBE 9 2.3 Composite 10 2.3.1 Definition of composite 10 2.3.2 Type of composite 10 2.3.3 Ceramic matrix composite 11 2.3.4 Studies on glass waste composite 12 2.4 Sintering 12 2.5 Properties characterization 13 2.5.1 Definition of properties characterization 13 2.5.2 X-ray Diffraction XRD 14 a Working principle 15 2.5.3 Scanning Electron Microscopy SEM 15 a Working principle 16 2.5.4 Vickers Microhardness Testing 17 vii a Working principle 17 2.5.5 Flexural testing 18 a Working principle 18 2.5.6 Density, Water absorption, and Porosity 19 2.6 Conclusion 20

3. CHAPTER 3: METHODOLOGY

21 3.1 Scope of work 21 3.2 Powder preparation 23 3.2.1 Glass waste powder 23 3.2.2 Spent bleach earth powder 23 3.3 Sample preparation 24 3.3.1 Batching 24 3.3.2 Mixing 24 3.3.3 Forming 25 3.3.4 Sintering 25 3.3.4.1 Sintering profile 26 3.4 Properties characterization 28 3.4.1 Bulk density, porosity, and water absorption 28 3.4.2 Hardness test 30 3.4.3 Flexural test 30 3.4.4 X-ray diffraction XRD 32 viii 3.4.5 Scanning electron microscopy SEM 32 3.5 Conclusion 33

4. CHAPTER 4: RESULTS AND DISCUSSION

34 4.1 Physical properties analysis 35 4.1.1 Physical observation 35 4.1.2 Porosity, water absorption, and bulk density 36 4.2 Mechanical properties analysis 38 4.2.1 Microhardness testing 38 4.2.2 Flexural testing 39 4.3 Material characterization 41 4.3.1 X-ray diffraction XRD 41 4.3.2 Scanning electron microscope SEM 42 4.4 Conclusion 44

5. CHAPTER 5: CONCLUSION AND RECOMMENDATION

45 5.1 Conclusion 45 5.2 Recommendation 46

6. REFERENCES