Mixing Section Propane to Acrylic Acid design plant proses

23 Table 1.3: Reactor Stream Summary. This table provides temperature, pressure, vapor fraction, and component flow rates for all streams in the reactor section of the process flowsheet. Stream S ‐114 PURGE S‐106 S‐109 S‐110 S‐111 S‐112 S‐116 S‐107 S ‐108 Temperature °F 85 85 228 280 85 82 85 85 740 780 Pressure psia 25 25 54 40 35 30 25 25 49 45 Vapor Fraction 1 1 1 1 0.92 0.92 1 1 1 Total Flow lbhr 55449 1714 9 62023 62023 62023 62023 57163 4859 6 62023 62023 Component Flows Propane 15382 4757 18025 16223 16223 16223 15857 3651 18025 16223 Oxygen 2427 75 2921 2 2505 2505 2505 2502 3 2921 2 2505 Propylene 1914 6 592 1945 1 2011 9 2011 9 2011 9 1973 9 380 1945 1 2011 9 Acrylic Acid 1791 55 1901 2854 8 2854 8 2854 8 1846 2670 2 1901 2854 8 Water 5713 177 7547 2230 9 2230 9 2230 9 5890 1641 9 7547 2230 9 Nitrogen 31341 9693 32324 32324 32324 32324 32311 130 32324 32324 Acetic Acid 379 12 537 1393 1393 1393 390 1003 537 1393 Carbon Dioxide 5779 8 1788 5809 4 5989 4 5989 4 5989 4 5958 5 308 5809 4 5989 4 Dowtherm Stream DOWTHERM ‐1 DOWTHERM ‐6 DOWTHERM ‐2 DOWTHERM ‐3 Temperature °F 198 198 738 458 Pressure psia 40 15 35 30 Vapor Fraction Total Flow lbhr 385000 385000 385000 385000 Component Flows lbhr Dowtherm 385000 385000 385000 385000 24

4.4 Separation Section

Figure 4.4: Separation Process Diagram. This shows the flowsheet of the separation section of the process, which includes the four distillation towers and the Dowtherm heating loop. 25 Table 4.4: Separation Process Stream Summary. This table provides temperature, pressure, vapor fraction, and component flow rates for all streams in the separation section of the process flowsheet. Stream S ‐116 S ‐117 S ‐118 S ‐119 S ‐120 S ‐121 S ‐122 S ‐123 S ‐124 Temperature °F 85 86 86 400 418 318 317 295 307 Pressure psia 25 150 130 125 98 95 90 70 73 Vapor Fraction 1 1 1 1 Total Flow lbhr 48596 48596 48596 48596 23846 24750 24750 19472 5278 Component Flows lbhr Propane 3651 3651 3651 3651 3651 3651 3651 Oxygen 3 3 3 3 3 3 3 Propylene 380 380 380 380 380 380 380 Acrylic Acid 26702 26702 26702 26702 23844 2858 2858 1024 1834 Water 16419 16419 16419 16419 16419 16419 13036 3383 Nitrogen 130 130 130 130 130 130 130 Acetic Acid 1003 1003 1003 1003 1 1001 1001 941 60 Carbon Dioxide 308 308 308 308 308 308 308 Dowtherm Stream S ‐125 S ‐126 S ‐127 S ‐128 S ‐129 S ‐130 S ‐131 S ‐132 WASTE Temperature °F 374 371 415 100 298 287 265 264. 236 Pressure psia 68 68 68 63 65 67 65 60 25 Vapor Fraction 1 1 1 1 1 0.3 Total Flow lbhr 5278. 1469 25314 25314 3809 13819. 5653 5653. 17628 Component Flows lbhr Propane 834. 2817. 2817. 834 Oxygen 3 3 Propylene 75 305 305. 75 Acrylic Acid 1834 1443 25286 25286 392 913. 110. 110. 1305 Water 3383. 25 25 25 3358 11202. 1834. 1834. 14560 Nitrogen 130. 130. Acetic Acid 60 1 3 3 59 783 158. 158. 842 Carbon Dioxide 12 296. 296. 12 Dowtherm Stream DOWTHERM ‐3 DOWTHERM‐4 DOWTHERM‐5 DOWTHERM‐6 Temperature °F 458 299 203 198 Pressure psia 30 25 20 15 Vapor Fraction Total Flow lbhr 385000 385000 385000 385000 Component Flows lbhr Dowtherm 385000 385000 385000 385000