Pembuatan dan Karakterisasi Semi-Hard Magnetic Fe2O3 Berbasis Mill Scale Limbah Industri Baja dengan Penambahan FeMo
21
22
Thermolyne Furnice High Temperature
Planetary Ball Mill
23
Magnetic field Press
25
24
Aquades
Peralatan Archimedes
Universitas Sumatera Utara
Universitas Sumatera Utara
LAMPIRAN 2
DATA PENGUKURAN TRUE DENSITY
1. Pengukuran True Density mill scale
No
m1 (g)
m2 (g)
m3 (g) m4 (g)
ρ Toluen
True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,06
23,18
0,86
5.561
2
14,09
22,36
15,07
23,19
0,86
5.619
3
14,09
22,36
15,09
23,21
0,86
5.733
Rata-rata
5.638
2. Pengukuran True Density FeMo
m3 (g) m4 (g)
ρ Toluen
True Density
(g/cm3)
(g/cm3)
No
m1 (g)
m2 (g)
1
14,09
22,36
15
23,19
0,86
9.783
2
14,09
22,36
15
23,19
0,86
9.783
Rata-rata
9.783
3. Pengukuran True Density campuran mill scale + FeMo (99:1)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,06
23,18
0,86
5.561
2
14,09
22,36
15,08
23,20
0,86
5.676
3
14,09
22,36
15,08
23,20
0,86
5.676
Rata-rata
14,09
22,36
15,08.
23,193
0,86
5.638
Universitas Sumatera Utara
4. Pengukuran True Density campuran mill scale + FeMo (97:3)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09 22,36 15,08
23,2
0,86
5.676
2
14,09 22,36 15,08
23,2
0,86
5.676
3
14,09 22,36 15,09 23,21
0,86
5.733
Rata-rata
5.695
5. Pengukuran True Density campuran mill scale + FeMo (95:5)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36 15,09 23,21
0,86
5.733
2
14,09
22,36 15,08
23,2
0,86
5.676
3
14,09
22,36 15,09 23,21
0,86
5.733
14,09
22,36 15,087 23,207
0,86
5.714
Ratarata
6. Pengukuran True Density campuran mill scale + FeMo (93:7)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,1
23,22
0,86
5.791
2
14,09
22,36 15,09
23,22
0,86
6.143
3
14,09
22,36 15,08
23,2
0,86
5.676
Rata-rata
5.870
Universitas Sumatera Utara
7. Pengukuran True Density campuran mill scale + FeMo (91:9)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,1
23,23
0,86
6.204
2
14,09
22,36
15,1
23,22
0,86
5.791
3
14,09
22,36
15,1
23,22
0,86
5.791
Rata-rata
5.929
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
LAMPIRAN 4
HASIL ANALISIS XRD
Match! Phase Analysis Report
Sample: mill scale
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
sampel.rd
d:\xrd\mill scale\mill scale (milling)\
10/08/2015 16:00:38
10.000° to 79.980°
3500
0.020
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
186
Name
(Wustite)
and 186 others...
Formula
Fe0.925 O
Entry No.
96-900-9772
Peak List
No.
1
2
3
4
5
6
7
8
9
2theta [°]
30.10
35.52
36.27
42.18
43.11
54.19
56.99
61.06
73.18
d [Å]
2.9693
2.5273
2.4771
2.1427
2.0985
1.6925
1.6159
1.5176
1.2934
I/I0
63.80
190.36
479.67
715.89
88.16
62.51
84.15
229.67
84.96
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
Universitas Sumatera Utara
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-8637
Phase classification
Name
Mineral Name Wustite
Formula
FeO
I/Ic
6.03
Sample Name 9008636
Quality
C (calculated)
References
Publication
Bibliography
Origin of data
Source of
entry
Link to orig.
entry
Wyckoff R. W. G., "Second edition. Interscience Publishers, New York, New York
rocksalt structure", Crystal Structures 1, 85-237 (1963)
COD (Crystallography Open Database)
9008636
Crystal structure
Crystallographic data
Space group F m -3 m (225)
Crystal
cubic
system
Cell
a=4.3108 Å
parameters
Universitas Sumatera Utara
Atom
coordinates
Element Oxid. x
Fe
O
y
z
Bi
Focc
0.000 0.000 0.000 1.000000 1.000000
0.500 0.500 0.500 1.000000 1.000000
Diffraction data
Diffraction lines
d [Å]
Int. h k l Mult.
2.4888
2.1554
1.5241
1.2998
1.2444
1.0777
684.5
1000.0
515.5
208.6
140.7
59.0
1
2
2
3
2
4
1
0
0
1
2
0
1
0
2
1
2
0
8
6
12
24
8
6
Experimental
Physical Properties
Calc. density 5.95600 g/cm³
Remarks
Remarks
Comments
- Diffraction pattern calculated by Match!.
- I/Icor calculated by Match!.
Universitas Sumatera Utara
Match! Phase Analysis Report
Sample: mill scale
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
sampel.rd
d:\xrd\mill scale\mill scale (milling)\
10/08/2015 16:00:38
10.000° to 79.980°
3500
0.020
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
186
Name
(Wustite)
and 186 others...
Formula
Fe0.925 O
Entry No.
96-900-9772
Peak List
No.
1
2
3
4
5
6
7
8
9
2theta [°]
30.10
35.52
36.27
42.18
43.11
54.19
56.99
61.06
73.18
d [Å]
2.9693
2.5273
2.4771
2.1427
2.0985
1.6925
1.6159
1.5176
1.2934
I/I0
63.80
190.36
479.67
715.89
88.16
62.51
84.15
229.67
84.96
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
Universitas Sumatera Utara
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-101-1085
Phase classification
Name
Iron diiron(III) oxide
Mineral
Magnetite
Name
Formula
Fe3O4
I/Ic
6.06
Sample
1011084
Name
Quality
C (calculated)
References
Publication
Bibliography
Origin of data
Source of
entry
Link to orig.
entry
, "The scattering power of oxygen and iron for X-Rays", Proceedings of the
Physical Society, London 38, 482-487 (1926)
COD (Crystallography Open Database)
1011084
Crystal structure
Crystallographic data
Space group
F d -3 m (227)
Crystal
cubic
system
Cell
a=8.4000 Å
parameters
Z
8
Atom
Element Oxid.
coordinates
Fe
2.0
Fe
3.0
O
-2.0
x
0.000
0.625
0.379
y
0.000
0.625
0.379
z
0.000
0.625
0.379
Bi
1.000000
1.000000
1.000000
Focc
1.000000
1.000000
1.000000
Universitas Sumatera Utara
Diffraction data
Diffraction lines
d [Å]
4.8497
2.9698
2.5327
2.4249
2.1000
1.9271
1.7146
1.6166
1.4849
1.4199
1.4000
1.3282
1.2810
1.2663
1.2124
1.1762
1.1225
1.0936
1.0500
1.0262
1.0186
Int.
78.3
282.1
1000.0
80.6
201.2
7.3
90.0
291.1
388.7
8.9
0.0
31.0
77.4
33.2
24.2
4.2
31.7
119.2
44.9
0.3
0.0
h
1
2
1
2
0
3
2
1
4
5
4
6
3
2
4
1
6
5
0
3
4
k
1
0
3
2
4
1
4
5
0
1
2
0
5
6
4
7
2
3
8
7
6
l
1
2
1
2
0
3
2
1
4
3
4
2
3
2
4
1
4
5
0
3
4
Mult.
8
12
24
8
6
24
24
24
12
48
24
24
24
24
8
24
48
24
6
24
24
Experimental
Physical Properties
Meas.
5.17900 g/cm³
density
Calc. density
5.18900 g/cm³
Remarks
Remarks
Comments
-
Diffraction pattern calculated by Match!.
I/Icor calculated by Match!.
Space group has been derived from given symmetry operations.
Ambiguous space group information in source file.
Universitas Sumatera Utara
Entry # 96-231-0324
Phase classification
Name
Fe Mo
Formula
FeMo
I/Ic
3.910000
Sample
2310323
Name
Quality
C (calculated)
References
Publication
Bibliography
Origin of data
Source of
entry
Link to orig.
entry
Wilson C.G., Spooner F.J., "Ordering of atoms in the sigma phase of Fe Mo",
Acta Crystallographica (1,1948-23,1967)16, 230-230 (1963)
COD (Crystallography Open Database)
2310323
Crystal structure
Crystallographic data
Space group
P 42/m n m (136)
Crystal
tetragonal
system
Cell
a= 9.1280 Å c= 4.8130 Å
parameters
Z
15
Element Oxid.
x
Atom
coordinates
Fe
0.182
Fe
0.738
Fe
0.000
Mo
0.398
Mo
0.182
Fe
0.398
Fe
0.463
Mo
0.463
y
0.182
0.065
0.000
0.398
0.182
0.398
0.132
0.132
z
0.252
0.000
0.000
0.000
0.252
0.000
0.000
0.000
Bi
1.000000
1.000000
1.000000
1.000000
1.000000
1.000000
1.000000
1.000000
Focc
0.250000
1.000000
1.000000
0.750000
0.750000
0.250000
0.250000
0.750000
Diffraction data
Diffraction lines
d [Å]
6.4545
4.5640
4.2574
4.0822
3.8584
3.2272
3.1132
2.8865
2.6804
2.5718
2.5317
2.4755
2.4065
2.2820
2.2549
2.2406
2.2139
2.1515
2.1287
2.0731
Int.
5.7
2.4
21.0
27.3
6.8
6.5
10.7
22.3
3.9
28.0
19.0
147.1
183.8
13.5
50.4
19.4
967.6
464.5
448.7
783.2
h
1
2
1
1
1
2
2
1
2
3
2
3
0
4
1
3
1
3
2
2
k
1
0
0
2
1
2
1
3
2
0
3
1
0
0
1
2
4
3
0
1
l
0
0
1
0
1
0
1
0
1
1
0
1
2
0
2
1
0
0
2
2
Mult.
4
4
8
8
8
4
16
8
8
8
8
16
2
4
8
16
8
4
8
16
Universitas Sumatera Utara
2.0411
2.0113
1.9642
1.9292
1.8791
1.8484
1.8256
1.7901
1.7442
1.7069
1.6950
1.6778
1.6559
1.6293
1.6136
1.6039
1.5988
1.5801
1.5654
1.5570
1.5566
1.5299
1.5213
1.5006
1.4932
1.4887
1.4544
1.4433
1.4366
1.4363
1.4326
1.4256
1.4191
1.4023
1.3858
1.3824
1.3669
1.3607
1.3551
1.3402
1.3122
1.3094
1.2991
1.2909
1.2861
1.2859
1.2733
1.2658
1.2613
1.2586
1.2538
1.2468
1.2377
1.2265
1.2242
1.2133
1.2051
1.2033
1.1986
1.1947
1.1845
1.1829
1.1687
1.1652
1.1635
2.1
1000.0
438.4
111.1
4.4
126.0
0.3
3.0
14.9
18.5
1.2
7.9
0.1
0.8
0.6
0.1
4.6
0.8
3.2
1.4
13.5
0.4
3.3
0.5
0.7
0.1
53.3
7.8
0.8
41.0
3.3
10.8
5.9
18.7
90.7
22.9
13.4
1.0
2.0
1.0
188.5
7.0
185.5
64.9
84.9
79.1
69.8
0.8
1.9
13.8
156.1
61.9
40.7
27.3
10.1
65.9
4.3
87.8
0.0
2.3
1.9
0.1
4.7
0.7
0.1
2
4
3
2
4
3
3
1
3
4
2
5
4
4
4
3
5
0
3
1
4
4
6
1
2
5
4
2
2
5
6
4
3
3
5
6
5
3
3
4
5
6
4
1
3
6
6
4
4
7
2
5
6
5
6
7
4
0
3
5
6
1
5
5
0
4
1
3
2
2
1
4
5
2
3
5
1
0
1
4
3
2
1
5
1
2
4
0
6
1
3
3
6
2
1
1
5
0
1
2
2
4
6
2
4
3
3
1
7
3
0
1
6
2
0
7
5
2
4
4
2
3
0
7
1
3
1
6
2
2
0
1
1
2
1
2
0
0
2
1
0
1
2
2
0
2
1
3
0
3
2
1
0
0
3
1
2
0
3
2
1
0
3
3
2
1
1
0
3
2
2
1
3
0
3
2
2
0
3
1
0
1
2
2
1
1
3
4
0
3
2
4
0
3
4
8
16
8
8
16
16
8
8
16
16
8
16
8
16
4
8
16
8
8
8
16
8
4
8
16
16
16
8
8
16
16
8
8
16
16
16
16
8
16
8
16
16
16
8
8
8
16
8
16
8
8
8
16
16
16
16
16
2
8
16
16
8
8
16
8
Universitas Sumatera Utara
1.1630
1.1542
1.1410
1.1377
1.1376
1.1357
1.1322
1.1274
1.1204
1.1203
1.1120
1.1106
1.1069
1.1021
1.0959
1.0867
1.0788
1.0757
1.0730
1.0729
1.0684
1.0656
1.0644
1.0611
1.0572
1.0513
1.0502
1.0498
1.0430
1.0377
1.0365
1.0362
1.0310
1.0245
1.0205
1.0119
1.0080
1.0057
1.0056
0.1
1.1
1.5
0.5
2.5
0.7
4.2
0.5
0.0
6.5
14.1
1.9
74.9
4.4
1.6
2.3
57.7
28.8
8.3
5.0
0.0
5.7
2.2
0.0
125.6
1.5
66.1
36.8
0.1
4.3
0.7
8.0
50.9
102.5
1.0
6.6
0.0
29.6
8.2
7
2
8
4
5
6
1
2
5
6
7
3
2
7
6
3
8
6
6
7
3
5
4
5
4
6
3
6
8
6
4
7
8
7
4
7
1
5
8
3
1
0
4
5
5
8
2
3
4
2
1
8
4
1
2
2
6
2
3
8
4
0
7
1
5
3
6
3
3
2
5
0
4
8
0
9
5
2
1
4
0
3
2
1
0
4
3
2
2
4
0
1
3
4
1
0
3
2
0
3
4
0
4
2
4
1
1
3
4
1
2
2
0
3
0
3
2
16
16
4
8
8
16
8
8
16
16
16
16
8
16
16
16
16
4
16
16
8
16
8
8
16
16
8
8
16
16
16
16
8
16
8
8
8
8
16
Experimental
Physical Properties
Calc. density
9.42600 g/cm³
Remarks
Remarks
Comments
- Diffraction pattern calculated by Match!.
- I/Ic calculated by Match!.
Universitas Sumatera Utara
Match! Phase Analysis Report
Sample: 93%millscale+7%femo tk 900
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
93%millscale+7%femo tk 900.ras
d:\xrd\93%millscale+7%femo-tk 900\
12/05/2016 10:14:04
20.000° to 90.000°
7000
0.010
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
186
Name
Formula
Fe2 O3
and 186 others...
Entry No.
96-210-1169
Peak List
No.
1
2
3
4
5
6
7
8
9
10
2theta [°]
24.20
33.20
35.69
40.93
49.55
54.15
57.69
62.51
64.08
72.04
d [Å]
3.6782
2.6985
2.5156
2.2051
1.8397
1.6938
1.5980
1.4858
1.4532
1.3110
I/I0
334.44
867.94
506.49
189.29
478.13
405.10
127.81
193.52
183.99
107.86
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
Universitas Sumatera Utara
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-0140
Phase classification
Name
Miner
Hematite
al
Name
Form
Fe2O3
ula
I/Ic
3.83
Samp
9000139
le
Name
Quali
C (calculated)
ty
References
Publication
Biblio
Blake R. L., Hessevick R. E., Zoltai T., Finger L. W., "Refinement of the hematite
graph
structure", American Mineralogist 51, 123-129 (1966)
y
Origin of data
Sourc
COD (Crystallography Open Database)
e of
entry
Link
9000139
to
orig.
entry
Crystal structure
Crystallographic data
Space
R -3 c (167)
group
Cryst
trigonal (hexagonal axes)
al
syste
Universitas Sumatera Utara
m
Cell
para
meter
s
Atom
coord
inate
s
a=5.0380 Å c=13.7720 Å
Ele
me
nt
Fe
O
xi
d.
O
x
y
z
Bi
Foc
c
U11
U22
U33
U12
U13
U23
0.
00
0
0.
30
6
0.
00
0
0.
00
0
0.
35
5
0.
25
0
1.0
000
00
1.0
000
00
1.0
000
00
1.0
000
00
0.0
077
00
0.0
065
00
0.0
077
00
0.0
080
00
0.0
027
00
0.0
044
00
0.0
037
00
0.0
040
00
0.0
000
00
0.0
017
00
0.0
000
00
0.0
036
00
Diffraction data
Diffraction lines
d [Å]
3.6855
2.7028
2.5190
2.2953
2.2084
2.0797
1.8428
1.6966
1.6374
1.6037
1.6014
1.4873
1.4543
1.4149
1.3514
1.3133
1.3078
1.2638
1.2595
1.2285
1.2146
1.2054
1.1918
1.1909
1.1646
1.1477
1.1416
1.1079
1.1042
1.0773
1.0571
1.0444
1.0398
1.0307
Int.
292.1
1000.0
732.7
20.2
176.8
19.0
359.4
427.4
4.6
21.9
79.8
282.4
270.2
2.2
27.3
96.8
15.4
1.3
61.2
22.0
8.7
0.5
13.6
36.5
48.2
1.0
73.4
0.3
66.4
6.7
72.4
4.5
22.4
0.2
h
0
1
1
0
1
2
0
1
2
1
0
2
3
1
2
1
1
2
2
0
2
1
3
1
0
0
1
3
2
0
2
1
4
1
k
1
0
1
0
1
0
2
1
1
2
1
1
0
2
0
0
1
1
2
3
2
3
1
2
2
0
3
1
2
4
1
1
0
3
l
2
4
0
6
3
2
4
6
1
2
8
4
0
5
8
10
9
7
0
6
3
1
2
8
10
12
4
5
6
2
10
12
4
7
Mult.
6
6
6
2
12
6
6
12
12
12
6
12
6
12
6
6
12
12
6
6
12
12
12
12
6
2
12
12
12
6
12
12
6
12
Experimental
Physical Properties
Calc.
5.25600 g/cm³
densi
ty
Universitas Sumatera Utara
Match! Phase Analysis Report
Sample: 93%millscale+7%femo ts 1250
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
93%millscale+7%femo ts 1250.ras
d:\xrd\93%millscale+7%femo-ts 1250\
12/05/2016 10:34:52
20.000° to 90.000°
7000
0.010
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
21
Name
Formula
Fe2 O3
and 21 others...
Entry No.
96-210-1169
Peak List
No.
1
2
3
4
5
6
7
8
9
10
11
2theta [°]
24.16
33.20
35.68
40.90
49.52
54.14
57.62
62.49
64.08
72.05
76.09
d [Å]
3.6843
2.6986
2.5163
2.2067
1.8406
1.6942
1.5999
1.4863
1.4532
1.3108
1.2510
I/I0
187.75
793.49
476.08
239.81
408.65
458.43
166.16
267.05
247.18
137.62
55.73
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
A
A
A
A
A
A
A
A
A
A
Diffraction Pattern Graphics
Universitas Sumatera Utara
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-0140
Phase classification
Name
Miner
Hematite
al
Name
Form
Fe2O3
ula
I/Ic
3.83
Samp
9000139
le
Name
Quali
C (calculated)
ty
References
Publication
Biblio
Blake R. L., Hessevick R. E., Zoltai T., Finger L. W., "Refinement of the hematite
graph
structure", American Mineralogist 51, 123-129 (1966)
y
Origin of data
Sourc
COD (Crystallography Open Database)
e of
entry
Link
9000139
to
orig.
entry
Crystal structure
Crystallographic data
Space
R -3 c (167)
group
Cryst
trigonal (hexagonal axes)
al
syste
m
Cell
a=5.0380 Å c=13.7720 Å
para
meter
s
Atom
Ele
O
x
y
z
Bi
Foc
U11
U22
U33
U12
U13
U23
Universitas Sumatera Utara
coord
inate
s
me
nt
xi
d.
Fe
O
c
0.
00
0
0.
30
6
0.
00
0
0.
00
0
0.
35
5
0.
25
0
1.0
000
00
1.0
000
00
1.0
000
00
1.0
000
00
0.0
077
00
0.0
065
00
0.0
077
00
0.0
080
00
0.0
027
00
0.0
044
00
0.0
037
00
0.0
040
00
0.0
000
00
0.0
017
00
0.0
000
00
0.0
036
00
Diffraction data
Diffraction lines
d [Å]
3.6855
2.7028
2.5190
2.2953
2.2084
2.0797
1.8428
1.6966
1.6374
1.6037
1.6014
1.4873
1.4543
1.4149
1.3514
1.3133
1.3078
1.2638
1.2595
1.2285
1.2146
1.2054
1.1918
1.1909
1.1646
1.1477
1.1416
1.1079
1.1042
1.0773
1.0571
1.0444
1.0398
1.0307
Int.
292.1
1000.0
732.7
20.2
176.8
19.0
359.4
427.4
4.6
21.9
79.8
282.4
270.2
2.2
27.3
96.8
15.4
1.3
61.2
22.0
8.7
0.5
13.6
36.5
48.2
1.0
73.4
0.3
66.4
6.7
72.4
4.5
22.4
0.2
h
0
1
1
0
1
2
0
1
2
1
0
2
3
1
2
1
1
2
2
0
2
1
3
1
0
0
1
3
2
0
2
1
4
1
k
1
0
1
0
1
0
2
1
1
2
1
1
0
2
0
0
1
1
2
3
2
3
1
2
2
0
3
1
2
4
1
1
0
3
l
2
4
0
6
3
2
4
6
1
2
8
4
0
5
8
10
9
7
0
6
3
1
2
8
10
12
4
5
6
2
10
12
4
7
Mult.
6
6
6
2
12
6
6
12
12
12
6
12
6
12
6
6
12
12
6
6
12
12
12
12
6
2
12
12
12
6
12
12
6
12
Experimental
Physical Properties
Calc.
5.25600 g/cm³
densi
ty
Universitas Sumatera Utara
22
Thermolyne Furnice High Temperature
Planetary Ball Mill
23
Magnetic field Press
25
24
Aquades
Peralatan Archimedes
Universitas Sumatera Utara
Universitas Sumatera Utara
LAMPIRAN 2
DATA PENGUKURAN TRUE DENSITY
1. Pengukuran True Density mill scale
No
m1 (g)
m2 (g)
m3 (g) m4 (g)
ρ Toluen
True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,06
23,18
0,86
5.561
2
14,09
22,36
15,07
23,19
0,86
5.619
3
14,09
22,36
15,09
23,21
0,86
5.733
Rata-rata
5.638
2. Pengukuran True Density FeMo
m3 (g) m4 (g)
ρ Toluen
True Density
(g/cm3)
(g/cm3)
No
m1 (g)
m2 (g)
1
14,09
22,36
15
23,19
0,86
9.783
2
14,09
22,36
15
23,19
0,86
9.783
Rata-rata
9.783
3. Pengukuran True Density campuran mill scale + FeMo (99:1)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,06
23,18
0,86
5.561
2
14,09
22,36
15,08
23,20
0,86
5.676
3
14,09
22,36
15,08
23,20
0,86
5.676
Rata-rata
14,09
22,36
15,08.
23,193
0,86
5.638
Universitas Sumatera Utara
4. Pengukuran True Density campuran mill scale + FeMo (97:3)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09 22,36 15,08
23,2
0,86
5.676
2
14,09 22,36 15,08
23,2
0,86
5.676
3
14,09 22,36 15,09 23,21
0,86
5.733
Rata-rata
5.695
5. Pengukuran True Density campuran mill scale + FeMo (95:5)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36 15,09 23,21
0,86
5.733
2
14,09
22,36 15,08
23,2
0,86
5.676
3
14,09
22,36 15,09 23,21
0,86
5.733
14,09
22,36 15,087 23,207
0,86
5.714
Ratarata
6. Pengukuran True Density campuran mill scale + FeMo (93:7)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,1
23,22
0,86
5.791
2
14,09
22,36 15,09
23,22
0,86
6.143
3
14,09
22,36 15,08
23,2
0,86
5.676
Rata-rata
5.870
Universitas Sumatera Utara
7. Pengukuran True Density campuran mill scale + FeMo (91:9)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ Toluen True Density
(g/cm3)
(g/cm3)
1
14,09
22,36
15,1
23,23
0,86
6.204
2
14,09
22,36
15,1
23,22
0,86
5.791
3
14,09
22,36
15,1
23,22
0,86
5.791
Rata-rata
5.929
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
LAMPIRAN 4
HASIL ANALISIS XRD
Match! Phase Analysis Report
Sample: mill scale
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
sampel.rd
d:\xrd\mill scale\mill scale (milling)\
10/08/2015 16:00:38
10.000° to 79.980°
3500
0.020
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
186
Name
(Wustite)
and 186 others...
Formula
Fe0.925 O
Entry No.
96-900-9772
Peak List
No.
1
2
3
4
5
6
7
8
9
2theta [°]
30.10
35.52
36.27
42.18
43.11
54.19
56.99
61.06
73.18
d [Å]
2.9693
2.5273
2.4771
2.1427
2.0985
1.6925
1.6159
1.5176
1.2934
I/I0
63.80
190.36
479.67
715.89
88.16
62.51
84.15
229.67
84.96
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
Universitas Sumatera Utara
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-8637
Phase classification
Name
Mineral Name Wustite
Formula
FeO
I/Ic
6.03
Sample Name 9008636
Quality
C (calculated)
References
Publication
Bibliography
Origin of data
Source of
entry
Link to orig.
entry
Wyckoff R. W. G., "Second edition. Interscience Publishers, New York, New York
rocksalt structure", Crystal Structures 1, 85-237 (1963)
COD (Crystallography Open Database)
9008636
Crystal structure
Crystallographic data
Space group F m -3 m (225)
Crystal
cubic
system
Cell
a=4.3108 Å
parameters
Universitas Sumatera Utara
Atom
coordinates
Element Oxid. x
Fe
O
y
z
Bi
Focc
0.000 0.000 0.000 1.000000 1.000000
0.500 0.500 0.500 1.000000 1.000000
Diffraction data
Diffraction lines
d [Å]
Int. h k l Mult.
2.4888
2.1554
1.5241
1.2998
1.2444
1.0777
684.5
1000.0
515.5
208.6
140.7
59.0
1
2
2
3
2
4
1
0
0
1
2
0
1
0
2
1
2
0
8
6
12
24
8
6
Experimental
Physical Properties
Calc. density 5.95600 g/cm³
Remarks
Remarks
Comments
- Diffraction pattern calculated by Match!.
- I/Icor calculated by Match!.
Universitas Sumatera Utara
Match! Phase Analysis Report
Sample: mill scale
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
sampel.rd
d:\xrd\mill scale\mill scale (milling)\
10/08/2015 16:00:38
10.000° to 79.980°
3500
0.020
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
186
Name
(Wustite)
and 186 others...
Formula
Fe0.925 O
Entry No.
96-900-9772
Peak List
No.
1
2
3
4
5
6
7
8
9
2theta [°]
30.10
35.52
36.27
42.18
43.11
54.19
56.99
61.06
73.18
d [Å]
2.9693
2.5273
2.4771
2.1427
2.0985
1.6925
1.6159
1.5176
1.2934
I/I0
63.80
190.36
479.67
715.89
88.16
62.51
84.15
229.67
84.96
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
Universitas Sumatera Utara
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-101-1085
Phase classification
Name
Iron diiron(III) oxide
Mineral
Magnetite
Name
Formula
Fe3O4
I/Ic
6.06
Sample
1011084
Name
Quality
C (calculated)
References
Publication
Bibliography
Origin of data
Source of
entry
Link to orig.
entry
, "The scattering power of oxygen and iron for X-Rays", Proceedings of the
Physical Society, London 38, 482-487 (1926)
COD (Crystallography Open Database)
1011084
Crystal structure
Crystallographic data
Space group
F d -3 m (227)
Crystal
cubic
system
Cell
a=8.4000 Å
parameters
Z
8
Atom
Element Oxid.
coordinates
Fe
2.0
Fe
3.0
O
-2.0
x
0.000
0.625
0.379
y
0.000
0.625
0.379
z
0.000
0.625
0.379
Bi
1.000000
1.000000
1.000000
Focc
1.000000
1.000000
1.000000
Universitas Sumatera Utara
Diffraction data
Diffraction lines
d [Å]
4.8497
2.9698
2.5327
2.4249
2.1000
1.9271
1.7146
1.6166
1.4849
1.4199
1.4000
1.3282
1.2810
1.2663
1.2124
1.1762
1.1225
1.0936
1.0500
1.0262
1.0186
Int.
78.3
282.1
1000.0
80.6
201.2
7.3
90.0
291.1
388.7
8.9
0.0
31.0
77.4
33.2
24.2
4.2
31.7
119.2
44.9
0.3
0.0
h
1
2
1
2
0
3
2
1
4
5
4
6
3
2
4
1
6
5
0
3
4
k
1
0
3
2
4
1
4
5
0
1
2
0
5
6
4
7
2
3
8
7
6
l
1
2
1
2
0
3
2
1
4
3
4
2
3
2
4
1
4
5
0
3
4
Mult.
8
12
24
8
6
24
24
24
12
48
24
24
24
24
8
24
48
24
6
24
24
Experimental
Physical Properties
Meas.
5.17900 g/cm³
density
Calc. density
5.18900 g/cm³
Remarks
Remarks
Comments
-
Diffraction pattern calculated by Match!.
I/Icor calculated by Match!.
Space group has been derived from given symmetry operations.
Ambiguous space group information in source file.
Universitas Sumatera Utara
Entry # 96-231-0324
Phase classification
Name
Fe Mo
Formula
FeMo
I/Ic
3.910000
Sample
2310323
Name
Quality
C (calculated)
References
Publication
Bibliography
Origin of data
Source of
entry
Link to orig.
entry
Wilson C.G., Spooner F.J., "Ordering of atoms in the sigma phase of Fe Mo",
Acta Crystallographica (1,1948-23,1967)16, 230-230 (1963)
COD (Crystallography Open Database)
2310323
Crystal structure
Crystallographic data
Space group
P 42/m n m (136)
Crystal
tetragonal
system
Cell
a= 9.1280 Å c= 4.8130 Å
parameters
Z
15
Element Oxid.
x
Atom
coordinates
Fe
0.182
Fe
0.738
Fe
0.000
Mo
0.398
Mo
0.182
Fe
0.398
Fe
0.463
Mo
0.463
y
0.182
0.065
0.000
0.398
0.182
0.398
0.132
0.132
z
0.252
0.000
0.000
0.000
0.252
0.000
0.000
0.000
Bi
1.000000
1.000000
1.000000
1.000000
1.000000
1.000000
1.000000
1.000000
Focc
0.250000
1.000000
1.000000
0.750000
0.750000
0.250000
0.250000
0.750000
Diffraction data
Diffraction lines
d [Å]
6.4545
4.5640
4.2574
4.0822
3.8584
3.2272
3.1132
2.8865
2.6804
2.5718
2.5317
2.4755
2.4065
2.2820
2.2549
2.2406
2.2139
2.1515
2.1287
2.0731
Int.
5.7
2.4
21.0
27.3
6.8
6.5
10.7
22.3
3.9
28.0
19.0
147.1
183.8
13.5
50.4
19.4
967.6
464.5
448.7
783.2
h
1
2
1
1
1
2
2
1
2
3
2
3
0
4
1
3
1
3
2
2
k
1
0
0
2
1
2
1
3
2
0
3
1
0
0
1
2
4
3
0
1
l
0
0
1
0
1
0
1
0
1
1
0
1
2
0
2
1
0
0
2
2
Mult.
4
4
8
8
8
4
16
8
8
8
8
16
2
4
8
16
8
4
8
16
Universitas Sumatera Utara
2.0411
2.0113
1.9642
1.9292
1.8791
1.8484
1.8256
1.7901
1.7442
1.7069
1.6950
1.6778
1.6559
1.6293
1.6136
1.6039
1.5988
1.5801
1.5654
1.5570
1.5566
1.5299
1.5213
1.5006
1.4932
1.4887
1.4544
1.4433
1.4366
1.4363
1.4326
1.4256
1.4191
1.4023
1.3858
1.3824
1.3669
1.3607
1.3551
1.3402
1.3122
1.3094
1.2991
1.2909
1.2861
1.2859
1.2733
1.2658
1.2613
1.2586
1.2538
1.2468
1.2377
1.2265
1.2242
1.2133
1.2051
1.2033
1.1986
1.1947
1.1845
1.1829
1.1687
1.1652
1.1635
2.1
1000.0
438.4
111.1
4.4
126.0
0.3
3.0
14.9
18.5
1.2
7.9
0.1
0.8
0.6
0.1
4.6
0.8
3.2
1.4
13.5
0.4
3.3
0.5
0.7
0.1
53.3
7.8
0.8
41.0
3.3
10.8
5.9
18.7
90.7
22.9
13.4
1.0
2.0
1.0
188.5
7.0
185.5
64.9
84.9
79.1
69.8
0.8
1.9
13.8
156.1
61.9
40.7
27.3
10.1
65.9
4.3
87.8
0.0
2.3
1.9
0.1
4.7
0.7
0.1
2
4
3
2
4
3
3
1
3
4
2
5
4
4
4
3
5
0
3
1
4
4
6
1
2
5
4
2
2
5
6
4
3
3
5
6
5
3
3
4
5
6
4
1
3
6
6
4
4
7
2
5
6
5
6
7
4
0
3
5
6
1
5
5
0
4
1
3
2
2
1
4
5
2
3
5
1
0
1
4
3
2
1
5
1
2
4
0
6
1
3
3
6
2
1
1
5
0
1
2
2
4
6
2
4
3
3
1
7
3
0
1
6
2
0
7
5
2
4
4
2
3
0
7
1
3
1
6
2
2
0
1
1
2
1
2
0
0
2
1
0
1
2
2
0
2
1
3
0
3
2
1
0
0
3
1
2
0
3
2
1
0
3
3
2
1
1
0
3
2
2
1
3
0
3
2
2
0
3
1
0
1
2
2
1
1
3
4
0
3
2
4
0
3
4
8
16
8
8
16
16
8
8
16
16
8
16
8
16
4
8
16
8
8
8
16
8
4
8
16
16
16
8
8
16
16
8
8
16
16
16
16
8
16
8
16
16
16
8
8
8
16
8
16
8
8
8
16
16
16
16
16
2
8
16
16
8
8
16
8
Universitas Sumatera Utara
1.1630
1.1542
1.1410
1.1377
1.1376
1.1357
1.1322
1.1274
1.1204
1.1203
1.1120
1.1106
1.1069
1.1021
1.0959
1.0867
1.0788
1.0757
1.0730
1.0729
1.0684
1.0656
1.0644
1.0611
1.0572
1.0513
1.0502
1.0498
1.0430
1.0377
1.0365
1.0362
1.0310
1.0245
1.0205
1.0119
1.0080
1.0057
1.0056
0.1
1.1
1.5
0.5
2.5
0.7
4.2
0.5
0.0
6.5
14.1
1.9
74.9
4.4
1.6
2.3
57.7
28.8
8.3
5.0
0.0
5.7
2.2
0.0
125.6
1.5
66.1
36.8
0.1
4.3
0.7
8.0
50.9
102.5
1.0
6.6
0.0
29.6
8.2
7
2
8
4
5
6
1
2
5
6
7
3
2
7
6
3
8
6
6
7
3
5
4
5
4
6
3
6
8
6
4
7
8
7
4
7
1
5
8
3
1
0
4
5
5
8
2
3
4
2
1
8
4
1
2
2
6
2
3
8
4
0
7
1
5
3
6
3
3
2
5
0
4
8
0
9
5
2
1
4
0
3
2
1
0
4
3
2
2
4
0
1
3
4
1
0
3
2
0
3
4
0
4
2
4
1
1
3
4
1
2
2
0
3
0
3
2
16
16
4
8
8
16
8
8
16
16
16
16
8
16
16
16
16
4
16
16
8
16
8
8
16
16
8
8
16
16
16
16
8
16
8
8
8
8
16
Experimental
Physical Properties
Calc. density
9.42600 g/cm³
Remarks
Remarks
Comments
- Diffraction pattern calculated by Match!.
- I/Ic calculated by Match!.
Universitas Sumatera Utara
Match! Phase Analysis Report
Sample: 93%millscale+7%femo tk 900
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
93%millscale+7%femo tk 900.ras
d:\xrd\93%millscale+7%femo-tk 900\
12/05/2016 10:14:04
20.000° to 90.000°
7000
0.010
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
186
Name
Formula
Fe2 O3
and 186 others...
Entry No.
96-210-1169
Peak List
No.
1
2
3
4
5
6
7
8
9
10
2theta [°]
24.20
33.20
35.69
40.93
49.55
54.15
57.69
62.51
64.08
72.04
d [Å]
3.6782
2.6985
2.5156
2.2051
1.8397
1.6938
1.5980
1.4858
1.4532
1.3110
I/I0
334.44
867.94
506.49
189.29
478.13
405.10
127.81
193.52
183.99
107.86
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
Universitas Sumatera Utara
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-0140
Phase classification
Name
Miner
Hematite
al
Name
Form
Fe2O3
ula
I/Ic
3.83
Samp
9000139
le
Name
Quali
C (calculated)
ty
References
Publication
Biblio
Blake R. L., Hessevick R. E., Zoltai T., Finger L. W., "Refinement of the hematite
graph
structure", American Mineralogist 51, 123-129 (1966)
y
Origin of data
Sourc
COD (Crystallography Open Database)
e of
entry
Link
9000139
to
orig.
entry
Crystal structure
Crystallographic data
Space
R -3 c (167)
group
Cryst
trigonal (hexagonal axes)
al
syste
Universitas Sumatera Utara
m
Cell
para
meter
s
Atom
coord
inate
s
a=5.0380 Å c=13.7720 Å
Ele
me
nt
Fe
O
xi
d.
O
x
y
z
Bi
Foc
c
U11
U22
U33
U12
U13
U23
0.
00
0
0.
30
6
0.
00
0
0.
00
0
0.
35
5
0.
25
0
1.0
000
00
1.0
000
00
1.0
000
00
1.0
000
00
0.0
077
00
0.0
065
00
0.0
077
00
0.0
080
00
0.0
027
00
0.0
044
00
0.0
037
00
0.0
040
00
0.0
000
00
0.0
017
00
0.0
000
00
0.0
036
00
Diffraction data
Diffraction lines
d [Å]
3.6855
2.7028
2.5190
2.2953
2.2084
2.0797
1.8428
1.6966
1.6374
1.6037
1.6014
1.4873
1.4543
1.4149
1.3514
1.3133
1.3078
1.2638
1.2595
1.2285
1.2146
1.2054
1.1918
1.1909
1.1646
1.1477
1.1416
1.1079
1.1042
1.0773
1.0571
1.0444
1.0398
1.0307
Int.
292.1
1000.0
732.7
20.2
176.8
19.0
359.4
427.4
4.6
21.9
79.8
282.4
270.2
2.2
27.3
96.8
15.4
1.3
61.2
22.0
8.7
0.5
13.6
36.5
48.2
1.0
73.4
0.3
66.4
6.7
72.4
4.5
22.4
0.2
h
0
1
1
0
1
2
0
1
2
1
0
2
3
1
2
1
1
2
2
0
2
1
3
1
0
0
1
3
2
0
2
1
4
1
k
1
0
1
0
1
0
2
1
1
2
1
1
0
2
0
0
1
1
2
3
2
3
1
2
2
0
3
1
2
4
1
1
0
3
l
2
4
0
6
3
2
4
6
1
2
8
4
0
5
8
10
9
7
0
6
3
1
2
8
10
12
4
5
6
2
10
12
4
7
Mult.
6
6
6
2
12
6
6
12
12
12
6
12
6
12
6
6
12
12
6
6
12
12
12
12
6
2
12
12
12
6
12
12
6
12
Experimental
Physical Properties
Calc.
5.25600 g/cm³
densi
ty
Universitas Sumatera Utara
Match! Phase Analysis Report
Sample: 93%millscale+7%femo ts 1250
Sample Data
Filename
File path
Data collected
Data range
Number of points
Step size
Alpha2 subtracted
Background subtr.
Data smoothed
Radiation
Wavelength
93%millscale+7%femo ts 1250.ras
d:\xrd\93%millscale+7%femo-ts 1250\
12/05/2016 10:34:52
20.000° to 90.000°
7000
0.010
No
No
Yes
Cu-Ka
1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne
OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR
Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y
OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe
OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho
OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl
OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR
Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries
21
Name
Formula
Fe2 O3
and 21 others...
Entry No.
96-210-1169
Peak List
No.
1
2
3
4
5
6
7
8
9
10
11
2theta [°]
24.16
33.20
35.68
40.90
49.52
54.14
57.62
62.49
64.08
72.05
76.09
d [Å]
3.6843
2.6986
2.5163
2.2067
1.8406
1.6942
1.5999
1.4863
1.4532
1.3108
1.2510
I/I0
187.75
793.49
476.08
239.81
408.65
458.43
166.16
267.05
247.18
137.62
55.73
FWHM
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
0.1000
Matched
A
A
A
A
A
A
A
A
A
A
Diffraction Pattern Graphics
Universitas Sumatera Utara
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-0140
Phase classification
Name
Miner
Hematite
al
Name
Form
Fe2O3
ula
I/Ic
3.83
Samp
9000139
le
Name
Quali
C (calculated)
ty
References
Publication
Biblio
Blake R. L., Hessevick R. E., Zoltai T., Finger L. W., "Refinement of the hematite
graph
structure", American Mineralogist 51, 123-129 (1966)
y
Origin of data
Sourc
COD (Crystallography Open Database)
e of
entry
Link
9000139
to
orig.
entry
Crystal structure
Crystallographic data
Space
R -3 c (167)
group
Cryst
trigonal (hexagonal axes)
al
syste
m
Cell
a=5.0380 Å c=13.7720 Å
para
meter
s
Atom
Ele
O
x
y
z
Bi
Foc
U11
U22
U33
U12
U13
U23
Universitas Sumatera Utara
coord
inate
s
me
nt
xi
d.
Fe
O
c
0.
00
0
0.
30
6
0.
00
0
0.
00
0
0.
35
5
0.
25
0
1.0
000
00
1.0
000
00
1.0
000
00
1.0
000
00
0.0
077
00
0.0
065
00
0.0
077
00
0.0
080
00
0.0
027
00
0.0
044
00
0.0
037
00
0.0
040
00
0.0
000
00
0.0
017
00
0.0
000
00
0.0
036
00
Diffraction data
Diffraction lines
d [Å]
3.6855
2.7028
2.5190
2.2953
2.2084
2.0797
1.8428
1.6966
1.6374
1.6037
1.6014
1.4873
1.4543
1.4149
1.3514
1.3133
1.3078
1.2638
1.2595
1.2285
1.2146
1.2054
1.1918
1.1909
1.1646
1.1477
1.1416
1.1079
1.1042
1.0773
1.0571
1.0444
1.0398
1.0307
Int.
292.1
1000.0
732.7
20.2
176.8
19.0
359.4
427.4
4.6
21.9
79.8
282.4
270.2
2.2
27.3
96.8
15.4
1.3
61.2
22.0
8.7
0.5
13.6
36.5
48.2
1.0
73.4
0.3
66.4
6.7
72.4
4.5
22.4
0.2
h
0
1
1
0
1
2
0
1
2
1
0
2
3
1
2
1
1
2
2
0
2
1
3
1
0
0
1
3
2
0
2
1
4
1
k
1
0
1
0
1
0
2
1
1
2
1
1
0
2
0
0
1
1
2
3
2
3
1
2
2
0
3
1
2
4
1
1
0
3
l
2
4
0
6
3
2
4
6
1
2
8
4
0
5
8
10
9
7
0
6
3
1
2
8
10
12
4
5
6
2
10
12
4
7
Mult.
6
6
6
2
12
6
6
12
12
12
6
12
6
12
6
6
12
12
6
6
12
12
12
12
6
2
12
12
12
6
12
12
6
12
Experimental
Physical Properties
Calc.
5.25600 g/cm³
densi
ty
Universitas Sumatera Utara