0,09 Logam berat ≤ 0,0003 < 0,0003 Lead ≤ 2 ppm < 2 ppm Kemurnian larutan Lolos Warna larutan

Lampiran 1. Spesifikasi Vitamin C Parameter Standar Analisa Hasil

  Karakteristik Kristal putih Lolos

Identifikasi Reaksi positif Lolos

Titik leleh 191-192 o

  C 191,0 o

  C Rotasi spesifik + 20,5 o

  o

  o pH 2,1 – 2,6 2,4 Abu sulfat

• 21,5
• 21,1

  ≤ 0,1% 0,03% Assay 99,5-100% 99,7% Kehilangan selama pengeringan ≤ 0,15%

  0,09% Logam berat ≤ 0,0003% &lt; 0,0003%

  Lead ≤ 2 ppm &lt; 2 ppm Kemurnian larutan Lolos Lolos

  Warna larutan ≤ BY 7 &lt; BY

  7 Oksalat ≤ 0,2% &lt; 0,2%

  Garam tembaga ≤ 0,0005% &lt; 0,0005% Ferrite

  ≤ 0,0002% &lt; 0,0002% Arsenik ≤ 0,0003%

  &lt; 0,0003% Kotoran organik Lolos Lolos

Lampiran 2. Perhitungan Asam Askorbat

  1. Pembuatan kurva standar Konsentrasi vitamin C standar Absorbansi (y) 0,25 0.6547 0,5 0.6453

  1 0.6193 2 0.6117 2,5 0.5012 vit C standar y = -0.0341x + 0.7086

  2 R = 0.7679

  0.8 si

  0.6 abs an

  0.4 rb

  Linear (abs) so

  0.2 b a

  0.25

  0.5

  1

  2

  2.5 konst konsentrasi Dari kurva didapatkan persamaan, y = -0,0341x + 0.7086.

  2. Pengukuran sampel Jumlah vitamin c Absorbansi (y) Konsentrasi asam mg asam askorbat (mg/ml) askorbat (x) 0,1 0,0269 19,9912 79,9648

  0,5 0,0042 20,6569 82,6276 1 0,0176 20,2639 81,0557 Kandungan vitamin C dihitung menggunakan rumus : konsentrasi asam askorbat x volume x 100

  (dari kurva standar) ekstrak total Mg asam askorbat =

per 100 g/ml sampel ml ekstrak sampel x 100 x berat/ volume sampel

yang dianalisa yang dianalisa

  Dimana: Volume ekstrak total = 25 ml

  Lampiran 3. SNI Minuman Sari Buah

  Lampiran 4. SNI Cara Uji Cemaran Mikroba

Lampiran 5. Hasil Analisa SPSS Tests of Normality

  .222 48 .000 .834 48 .000 .418 48 .000 .633 48 .000 .442 48 .000 .638 48 .000 .342 48 .000 .751 48 .000 .249 48 .000 .832 48 .000 .312 48 .000 .775 48 .000 .240 48 .000 .825 48 .000 .240 48 .000 .835 48 .000 .223 48 .000 .852 48 .000 .209 48 .000 .890 48 .000 .171 48 .001 .897 48 .000 .161 48 .003 .918 48 .003 .208 48 .000 .894 48 .000 .151 48 .008 .940 48 .016 .125 48 .059 .943 48 .021 .108 48 .200* .959 48 .089 .199 48 .000 .896 48 .000 .127 48 .049 .960 48 .104 .271 48 .000 .766 48 .000 .230 48 .000 .813 48 .000 .207 48 .000 .865 48 .000 .177 48 .001 .887 48 .000 .168 48 .002 .869 48 .000 .194 48 .000 .858 48 .000 .327 48 .000 .676 48 .000 .322 48 .000 .689 48 .000 .323 48 .000 .693 48 .000 .314 48 .000 .678 48 .000 .324 48 .000 .673 48 .000 .321 48 .000 .674 48 .000 hari hari ke 1 hari ke 3 hari ke 7 hari ke 14 hari ke 21 hari ke 28 hari ke 1 hari ke 3 hari ke 7 hari ke 14 hari ke 21 hari ke 28 hari ke 1 hari ke 3 hari ke 7 hari ke 14 hari ke 21 hari ke 28 hari ke 1 hari ke 3 hari ke 7 hari ke 14 hari ke 21 hari ke 28 hari ke 1 hari ke 3 hari ke 7 hari ke 14 hari ke 21 hari ke 28

  TSS warna pH antioksidan vitaminC Statistic df Sig. Statistic df Sig.

  Kolmogorov-Smirnov

  

a

  Shapiro-Wilk This is a lower bound of the true significance.

• .

  Lilliefors Significance Correction a.

  Tests of Normality .162 36 .018 .892 36 .002 .450

  36 .000 .624 36 .000 .310 36 .000 .818 36 .000 .401 36 .000 .723 36 .000 .239 36 .000 .868 36 .001 .220 36 .000 .890 36 .002 .289 36 .000 .848 36 .000 .378 36 .000 .773 36 .000 .140 36 .073 .888 36 .002 .136 36 .089 .887 36 .002 .156 36 .027 .901 36 .004 .143 36 .060 .898 36 .003 .155 36 .029 .887 36 .002 .231 36 .000 .786 36 .000 .138 36 .081 .909 36 .006 .216 36 .000 .822 36 .000 .088 36 .200* .980 36 .734 .082 36 .200* .961 36 .237 .084 36 .200* .974 36 .541 .090 36 .200* .975 36 .564 .155 36 .028 .934 36 .034 .121 36 .200* .944 36 .069 .125 36 .172 .934 36 .034 .134 36 .099 .931 36 .028 .138 36 .079 .923 36 .015 .187 36 .003 .918 36 .011 .137 36 .084 .893 36 .002 .199 36 .001 .919 36 .012 .109 36 .200* .930 36 .025 .151 36 .036 .937 36 .041 .145 36 .053 .935 36 .036 .130 36 .127 .923 36 .015 .153 36 .032 .907 36 .005 .109 36 .200* .930 36 .025 .121 36 .200* .923 36 .015 .143 36 .059 .933 36 .031 .119 36 .200* .934 36 .034 .102 36 .200* .943 36 .062 .109 36 .200* .951 36 .112 .097 36 .200* .945 36 .075 perlakuan non fortifikasi-b. gelap-ruang non fortifikasi-b.gelap-refri non fortifikasi-b. bening-ruang non fortifikasi-b. bening-refri fortifikasi-b.gelap-ruang fortfikasi-b.gelap-refri fortifikasi-b.bening-ruang fortifikasi-b.bening-refri non fortifikasi-b. gelap-ruang non fortifikasi-b.gelap-refri non fortifikasi-b. bening-ruang non fortifikasi-b. bening-refri fortifikasi-b.gelap-ruang fortfikasi-b.gelap-refri fortifikasi-b.bening-ruang fortifikasi-b.bening-refri non fortifikasi-b. gelap-ruang non fortifikasi-b.gelap-refri non fortifikasi-b. bening-ruang non fortifikasi-b. bening-refri fortifikasi-b.gelap-ruang fortfikasi-b.gelap-refri fortifikasi-b.bening-ruang fortifikasi-b.bening-refri non fortifikasi-b. gelap-ruang non fortifikasi-b.gelap-refri non fortifikasi-b. bening-ruang non fortifikasi-b. bening-refri fortifikasi-b.gelap-ruang fortfikasi-b.gelap-refri fortifikasi-b.bening-ruang fortifikasi-b.bening-refri non fortifikasi-b. gelap-ruang non fortifikasi-b.gelap-refri non fortifikasi-b. bening-ruang non fortifikasi-b. bening-refri fortifikasi-b.gelap-ruang fortfikasi-b.gelap-refri fortifikasi-b.bening-ruang fortifikasi-b.bening-refri TSS warna pH antioksidan vitaminC

  Statistic df Sig. Statistic df Sig.

  Kolmogorov-Smirnov ^a Shapiro-Wilk

  

Sari buah tanpa fortifikasi kemasan botol gelap penyimpanan suhu ruang (25-30

o

C) Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 3

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z -2.887 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 7

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U .000 Wilcoxon W 21.000 Z -2.887 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 14

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.887 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z -2.887 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U .000 Wilcoxon W 21.000 Z -2.892 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 7

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 14

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z -2.887 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 7

  6

  9.50

  57.00 hari ke 14

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U .000 Wilcoxon W 21.000 Z -2.882 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 7

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 7

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.887 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 14

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 14

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z -2.887 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks NF_BG_RG hari ke 21

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  NF_BG_RG Mann-Whitney U .000 Wilcoxon W 21.000 Z -2.887 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  o Sari buah fortifikasi kemasan botol gelap penyimpanan suhu ruang (25-30

C) Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 1

  6

  9.33

  56.00 hari ke 3

  6

  3.67

  22.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  1.000 Wilcoxon W

  22.000 Z -2.722 Asymp. Sig. (2-tailed) .006

  a

  Exact Sig. [2*(1-tailed .004

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 7

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U .000 Wilcoxon W

  21.000 Z

• 2.887 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 14

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 1

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 7

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U .000 Wilcoxon W

  21.000 Z

• 2.887 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 14

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U .000 Wilcoxon W 21.000 Z

• 2.882 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 3

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 7

  6

  9.50

  57.00 hari ke 14

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.887 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 7

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U .000 Wilcoxon W

  21.000 Z

• 2.887 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 7

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U .000 Wilcoxon W 21.000 Z

• 2.887 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 14

  6

  9.50

  57.00 hari ke 21

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 14

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed) .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.

  Grouping Variable: hari_ke

  Ranks

  hari_ke N Mean Rank Sum of Ranks F_BG_RG hari ke 21

  6

  9.50

  57.00 hari ke 28

  6

  3.50

  21.00 Total

  12

  b Test Statistics

  F_BG_RG Mann-Whitney U

  .000 Wilcoxon W

  21.000 Z

• 2.882 Asymp. Sig. (2-tailed)

  .004

  a

  Exact Sig. [2*(1-tailed .002

  Sig.)] a.

  Not corrected for ties.

  b.