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Pedoman Rietica Lanjutan 2fasa

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  • | Phase: 1 |
  • PHASE SCALE FACTOR = 0.236462E-03-.515320E-070.991738E-05 OVERALL TEMP. FACTOR = 0.000000 0.000000 0.000000 CELL PARAMETERS = 4.762982 0.000000 0.000564 4.762983 0.000000 0.000564 13.005280 0.000010 0.002151

  90.000008 0.000000 0.000000 90.000008 0.000000 0.000000 120.000015 0.000000 0.000001 RECIPROCAL CELL = 0.242 0.242 0.077 90.000 90.000 60.000 CELL VOLUME = 255.510223 0.060120 SCALE * VOLUME = 0.060419 0.002534 MOLECULAR WEIGHT = 611.757 DENSITY = 3.974 ABSOLUTE PHASE VALUES:

  INC = NEUTRONS ON SAMPLE/CM^2 ( in cm^-2) MASS = MASS OF PHASE IN BEAM (in g) ls/R = RATIO OF DETECTOR HEIGHT TO SAMPLE-DETECTOR Then:

  INC*MASS*ls/R = 10542.7

  | Histogram: 1 |

  • SCALE FACTOR = 1.0000 0.00000 0.00000 ZEROPOINT = -0.02600 0.00000 0.00000 SAMPLE DISPLACEMENT = -0.10988 -0.00002 0.01096 BACKGROUND PARAMETER B 0 = -0.532927E-01 0.101903E-03 1.85364 BACKGROUND PARAMETER B 1 = 0.221694 -0.896348E-04 0.140911

  BACKGROUND PARAMETER B 2 = -0.127168E-02 0.393399E-05 0.248544E-02 PREFERRED ORIENTATION = 0.92730 0.00006 0.00963 ABSORPTION R = 0.00000 0.00000 0.00000 ASYMMETRY PARAMETERS = 0.08005 -0.00001 0.00351 0.00000 0.00000 0.00000 HALFWIDTH PARAMETERS U = 0.040932 0.000007 0.005510 V = -0.005000 0.000000 0.000000 W = 0.004000 0.000000 0.000000 ANISOTROPIC GAUSSIAN BROADENING = 0.000000 0.000000 0.000000 LORENZTIAN COMPONENTS = 0.024269 0.000008 0.002259 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 EQUIVALENT TO A PARTICLE SIZE OF 3637.0( 338.5) ANGSTROMS EXTINCTION PARAMETER = 0.000000 0.000000 0.000000 PHASE 2: Aluminium Titanate

  • | Phase: 2 |
  • PHASE SCALE FACTOR = 0.323519E-040.106304E-070.225919E-05 OVERALL TEMP. FACTOR = 0.000000 0.000000 0.000000 CELL PARAMETERS = 3.588099 0.000015 0.001225 9.460348 0.000003 0.002631 9.685102 0.000045 0.002160

  90.000008 0.000000 0.000000 90.000008 0.000000 0.000000 90.000008 0.000000 0.000000 RECIPROCAL CELL = 0.279 0.106 0.103 90.000 90.000 90.000 CELL VOLUME = 328.757507 0.162252 SCALE * VOLUME = 0.010636 0.000743 MOLECULAR WEIGHT = 727.440 DENSITY = 3.673 ABSOLUTE PHASE VALUES:

  INC = NEUTRONS ON SAMPLE/CM^2 ( in cm^-2) MASS = MASS OF PHASE IN BEAM (in g) ls/R = RATIO OF DETECTOR HEIGHT TO SAMPLE-DETECTOR Then:

  INC*MASS*ls/R = 2206.85

  • | Histogram: 1 |
  • SCALE FACTOR = 1.0000 0.00000 0.00000 ZEROPOINT = -0.02600 0.00000 0.00000 SAMPLE DISPLACEMENT = -0.10988 -0.00002 0.01096 BACKGROUND PARAMETER B 0 = -0.532927E-01 0.101903E-03 1.85364 BACKGROUND PARAMETER B 1 = 0.221694 -0.896348E-04 0.140911

  BACKGROUND PARAMETER B 2 = -0.127168E-02 0.393399E-05 0.248544E-02 PREFERRED ORIENTATION = 0.91098 0.00007 0.02098 ABSORPTION R = 0.00000 0.00000 0.00000

  0.00000 0.00000 0.00000 HALFWIDTH PARAMETERS U = 0.279297 0.000149 0.046754 V = -0.005000 0.000000 0.000000 W = 0.004000 0.000000 0.000000 ANISOTROPIC GAUSSIAN BROADENING = 0.000000 0.000000 0.000000 LORENZTIAN COMPONENTS = 0.025478 -0.000017 0.007953 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 EQUIVALENT TO A PARTICLE SIZE OF 3464.5( 1081.4) ANGSTROMS EXTINCTION PARAMETER = 0.000000 0.000000 0.000000 PHASE 3: Rutile

  • | Phase: 3 |
  • PHASE SCALE FACTOR = 0.311855E-030.180519E-050.549470E-04 OVERALL TEMP. FACTOR = 0.000000 0.000000 0.000000 CELL PARAMETERS = 4.596533 0.000010 0.001133 4.596533 0.000010 0.001133 2.964037 0.000011 0.000690

  90.000008 0.000000 0.000000 90.000008 0.000000 0.000000 90.000008 0.000000 0.000000 RECIPROCAL CELL = 0.218 0.218 0.337 90.000 90.000 90.000 CELL VOLUME = 62.624535 0.026243 SCALE * VOLUME = 0.019530 0.003441 MOLECULAR WEIGHT = 159.800 DENSITY = 4.235 ABSOLUTE PHASE VALUES:

  INC = NEUTRONS ON SAMPLE/CM^2 ( in cm^-2) MASS = MASS OF PHASE IN BEAM (in g) ls/R = RATIO OF DETECTOR HEIGHT TO SAMPLE-DETECTOR Then:

  INC*MASS*ls/R = 890.175

  • | Histogram: 1 |
  • SCALE FACTOR = 1.0000 0.00000 0.00000 ZEROPOINT = -0.02600 0.00000 0.00000 SAMPLE DISPLACEMENT = -0.10988 -0.00002 0.01096 BACKGROUND PARAMETER B 0 = -0.532927E-01 0.101903E-03 1.85364 BACKGROUND PARAMETER B 1 = 0.221694 -0.896348E-04 0.140911

  BACKGROUND PARAMETER B 2 = -0.127168E-02 0.393399E-05 0.248544E-02 PREFERRED ORIENTATION = 0.91510 0.00069 0.02558 ABSORPTION R = 0.00000 0.00000 0.00000 ASYMMETRY PARAMETERS = 0.07911 0.00001 0.00863 0.00000 0.00000 0.00000 HALFWIDTH PARAMETERS U = 0.084596 -0.000052 0.026272 V = -0.005000 0.000000 0.000000 W = 0.002000 0.000000 0.000000 ANISOTROPIC GAUSSIAN BROADENING = 0.000000 0.000000 0.000000 LORENZTIAN COMPONENTS = 0.027202 -0.000023 0.007265 0.000000 0.000000 0.000000 0.000000 0.000000 0.000000 EQUIVALENT TO A PARTICLE SIZE OF 3244.9( 866.6) ANGSTROMS EXTINCTION PARAMETER = 0.000000 0.000000 0.000000

  PHASE 1: 81.63 4.63 77.29 4.28 PHASE 2: 9.58 0.76 16.18 1.27 PHASE 3: 8.79 1.59 6.53 1.17

  • | Hist | Rp | Rwp | Rexp |Durbin Unwght| Durbin Wght | N-P |
  • | 1 | 17.09 | 23.23 | 14.15 | 1.066 | 1.119 | 710 |
  • | SUMYDIF | SUMYOBS | SUMYCALC | SUMWYOBSSQ | GOF | CONDITION |
  • | 0.6058E+04| 0.3545E+05| 0.3355E+05| 0.3545E+05| 0.2694E+01| 0.2237E+14 |
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