Report of Analysis SUCOFINDO
Perpustakaan Unika
LAMPIRAN 1. Kriteria kitosan yang dibeli dari PT BIOTECH SURINDO dan
Report of Analysis SUCOFINDOPerpustakaan Unika LAMPIRAN 2. Kuisioner Survei Tingkat Konsumsi Kerang Survei ini dilakukan untuk mengetahui tingkat konsumsi kerang masyarakat Semarang.
Berikut ini ada beberapa pertanyaan yang diperlukan untuk kepentingan di atas. Diharapkan Anda dapat menjawab pertanyaan ini dengan baik.
Nama : Jenis Kelamin : L / P Usia : Berat Badan : Dalam 1 minggu, Anda mengkonsumsi masakan kerang berapa kali?
1x 2x 3x > 3x
□ □ □ □
Berapa banyak kerang yang Anda konsumsi dalam sekali makan? 10 butir 20 butir 30 butir 40 butir > 40 butir
□ □ □ □ □
Terima kasih
Perpustakaan Unika LAMPIRAN 3. Rata-rata Berat Kerang Darah
Berat kerang (gr) 7.414 7.741 6.456 6.885 6.597 4.715 5.158 4.950 5.170 5.041 4.615 4.645 6.184 4.762 4.888 5.714 5.263 6.180 5.909 5.925 6.046 6.185 6.233 5.065 6.293
Total : 144.034 gr Rata-rata : 1.92 gr
Keterangan: masing-masing berat kerang di atas merupakan gabungan dari 3 kerang dalam 1 cawan.
LAMPIRAN 4. Hasil Survei Tingkat Konsumsi Kerang No. Nama Jenis Kelamin Usia Berat Badan (kg) Konsumsi Kerang (per minggu) Banyak Konsumsi (ekor)
21
51
1
20
27 Yunita P
22
40
1
20
28 Theresia P
52
26 Donna P
1
20
29 Marlinda P
22
54
1
20
30 Ina P
21
56
25
20
20
28
60
1
20
22 Kuntum R. P
29
59
1
20
23 Felisia P
45
1
1
20
24 Santi P
24
57
1
20
25 Dewi P
28
60
1
31 Linda P
21 Marta R. P
52
1
40
37 Sarita P
21
48
1
40
38 Lani P
28
2
24
30
39 Iin P
31
50
3
20
40 Keshia P
30
67
4
45
36 Rida L. D. P
27
52
55
1
20
32 Stephanie P
31
75
1
20
33 Agustina P
24
1
30
20
34 Rina P
20
53
1
20
35 Monica S. P
21
40
1
23
20
1 Maria A. C. P
8 Kartika P
21
60
1
10
7 Metta P
23
48
1
10
21
10
50
1
10
9 Ayu P
35
72
1
10
10 Dian P
22
6 Ina P
1
1
3 Yuli P
26
52
1
10
2 Nike L P
24
55
1
10
22
50
48
1
10
4 Natalia P
21
44
1
10
5 Lala P
25
51
10
1
34
43
1
10
17 Imaniar A P
21
55
1
10
18 Novita P
60
16 Triana K. D P
1
10
19 Trifosa K. P
22
44
1
20
20 Melani P. P
22
68
20
10
11 Hany P
33
25
58
1
10
12 Sylvia P
26
51
1
10
13 Sri Erawati P
60
1
1
10
14 Dina P
24
50
1
10
15 Chusnul R. D P
24
55
30 Rata-rata 53,625 1,15 17,25 Perpustakaan Unika
LAMPIRAN 5. Penyeragaman Kerang Darah Uji Pendahuluan
Berat (gr) Berat (gr) Berat (gr) 4,64 4,74 4,39 4,25 4,23 4,46 4,74 4,24 4,79 4,65 4,84 4,52 4,30 4,24 4,80
4,84 4,66 4,29 4,60 4,41 4,59 4,68 4,74 4,67 4,66 4,65 4,69 4,65 4,68 4,74
4,68 4,70
4,10 4,83 4,04 4,86 4,32 4,11 4,07 4,95 4,60 4,11 4,28 4,92 5,01
Rata-rata : 4,55 SD : 0,26 CV : 6%
Perpustakaan Unika
LAMPIRAN 6. Penyeragaman Kerang Darah Uji Utama
Berat (gr) Berat (gr) Berat (gr) 8,24 8,43 8,77 8,78 8,78 8,68 8,03 8,14 8,22 8,49 8,15 8,22 8,83 8,17 8,16 8,11 8,13 8,14 8,01
8,5 8,51 8,55 8,72 8,49 8,89
8,8 8,41 8,78 8,23 8,92 8,97 8,23 8,36 8,42 8,86 8,38
8,2 8,55 8,27 8,64 8,41 8,33 8,94 8,88 8,12 7,93 7,44 7,81 7,69 7,95
7,42 7,62 7,57 7,63 7,52 7,68 7,64 7,87 7,42 7,45 7,59 7,73 7,79 7,56 7,64 7,89 7,49 7,61 7,35 8,53 8,63 8,85 8,89 8,72 7,82
Rata-rata : 8,21 SD : 0,47 CV : 6%
Perpustakaan Unika
Perpustakaan Unika LAMPIRAN 7. Kandungan Logam Cd Uji Pendahuluan
Berat Berat Kadar Konversi Kadar
Sampel Ulangan basah kering Abs Cd Cd KA (mg/kg Air
(gr) (gr) (mg/kg) berat basah) asam 0.084 kontrol 1 3.64 0.75 79.40% 0.219 2.70 0.5562
2
3.68 0.65 82.34% 0.229 2.90 0.5121
3
3.60 0.62 82.78% 0.210 2.52 0.4339 Rata-rata
2.71 0.5008 SD 0.19 0.0619
1 3.19 0.67 79.00% 0.242 3.16 0.6636 0,5% 2 3.15 0.69 78.10% 0.231 2.94 0.6439 3 3.15
0.67 78.73% 0.181 1.94 0.4126 Rata-rata
2.68 0.5734 SD 0.65 0.1395
1 2.80 0.58 79.29% 0.209 2.50 0.5178 1% 2 3.18 0.59 81.45% 0.207 2.46 0.4563 3 3.14
0.56 82.17% 0.199 2.30 0.4101 Rata-rata
2.42 2.4614 SD 0.11 0.0540
1 2.70 0.64 76.30% 0.213 2.58 0.6115 3% 2 3.19 0.74 76.80% 0.177 1.86 0.4315 3 3.11
0.69 77.81% 0.164 1.60 0.3550 Rata-rata
2.01 0.4660 SD 0.51 0.1316
1 3.31 0.72 78.25% 0.184 2.00 0.4350 5% 2 3.95 0.72 81.77% 0.174 1.80 0.3281 3 3.20
0.68 78.75% 0.165 1.62 0.3443 Rata-rata
1.81 0.3691 SD 0.19 0.0576
Perpustakaan Unika LAMPIRAN 8. Kandungan Logam Cu Uji Pendahuluan
Berat Berat Kadar Konversi Kadar
Sampel Ulangan basah kering Abs Cu Cu KA (mg/kg Air
(gr) (gr) (mg/kg) berat basah) asam 0.097 kontrol 1 3.64 0.75 79.40% 0.121 0.48 0.0989
2
3.68 0.65 82.34% 0.119 0.44 0.0777
3
3.60 0.62 82.78% 0.123 0.52 0.0895 Rata-rata
0.48 0.0887 SD 0.04 0.0106
1 3.19 0.67 79.00% 0.169 1.44 0.3024 0,5% 2 3.15 0.69 78.10% 0.163 1.32 0.2891 3 3.15
0.67 78.73% 0.143 0.92 0.1957 Rata-rata
1.23 0.2624 SD 0.27 0.0582
1 2.80 0.58 79.29% 0.155 1.16 0.2402 1% 2 3.18 0.59 81.45% 0.146 0.98 0.1818 3 3.14
0.56 82.17% 0.145 0.96 0.1712 Rata-rata
1.03 0.1977 SD 0.11 0.0372
1 2.70 0.64 76.30% 0.156 1.18 0.2797 3% 2 3.19 0.74 76.80% 0.098 0.02 0.0046 3 3.11
0.69 77.81% 0.090 -0.14 -0.0311 Rata-rata
0.35 0.0844 SD 0.72 0.1700
1 3.31 0.72 78.25% 0.113 0.32 0.0696 5% 2 3.95 0.72 81.77% 0.148 1.02 0.1859 3 3.20
0.68 78.75% 0.136 0.78 0.1658 Rata-rata
0.70 0.1404 SD 0.35 0.0622
LAMPIRAN 9. Kandungan Logam Cd Uji Utama
1.4791 SD 0.2997
0.6760
1.7052 SD
5% 1 6.05 1.36 77.49% 0.478 7.64 1.7198 2 6.19 1.48 76.01% 0.329 4.66 1.1179 3 6.23 1.38 77.86% 0.311 4.30 0.9520 4 5.07 1.22 75.97% 0.561 9.30 2.2348 5 6.29 1.43 77.34% 0.648 11.04 2.5017 rata-rata
1.3288 SD 0.3621
3% 1 5.71 1.16 79.72% 0.402 6.12 1.2411 2 5.26 1.19 77.31% 0.418 6.44 1.4612 3 6.18 1.24 79.89% 0.554 9.16 1.8421 4 5.91 1.44 75.72% 0.271 3.50 0.8498 5 5.93 1.33 77.60% 0.375 5.58 1.2499 rata-rata
1.5783 SD 0.5209
1% 1 4.62 1.14 75.41% 0.443 6.94 1.7065 2 4.65 1.07 77.03% 0.435 6.78 1.5574 3 6.18 1.42 76.97% 0.396 6.00 1.3818 4 4.76 1.05 77.89% 0.625 10.58 2.3392 5 4.89 1.15 76.51% 0.289 3.86 0.9067 rata-rata
0,5% 1 4.72 1.24 73.70% 0.473 7.54 1.9830 2 5.16 1.26 75.49% 0.350 5.08 1.2451 3 4.95 1.07 78.30% 0.393 5.94 1.2890 4 5.17 1.18 77.20% 0.428 6.64 1.5139 5 5.04 1.13 77.56% 0.400 6.08 1.3644 rata-rata
Sampel Ulangan Berat basah (gr)
2.2428 SD 0.4936
1 7.41 1.62 78.20% 0.759 13.26 2.8907 2 7.74 1.89 75.64% 0.564 9.36 2.2801 3 6.46 1.41 78.24% 0.673 11.54 2.5111 4 6.89 1.63 76.37% 0.445 6.98 1.6494 5 6.60 1.55 76.58% 0.498 8.04 1.8830 rata-rata
KA (mg/kg berat basah) kontrol
(mg/kg) Konversi
Abs Cd Kadar Cd
Kadar Air
Berat kering (gr)
Perpustakaan Unika
LAMPIRAN 10. Kandungan Cu Uji Utama
0.1956 1% 1 4.62
0.2360 Asam 0,090
0.8188 SD
1.36 77.49% 0.240 3.00 0.6753 2 6.19 1.48 76.01% 0.190 2.00 0.4798 3 6.23 1.38 77.86% 0.300 4.20 0.9299 4 5.07 1.22 75.97% 0.310 4.40 1.0573 5 6.29 1.43 77.34% 0.300 4.20 0.9517 rata-rata
0.1078 5% 1 6.05
0.7059 SD
1.16 79.72% 0.300 4.20 0.8518 2 5.26 1.19 77.31% 0.220 2.60 0.5899 3 6.18 1.24 79.89% 0.260 3.40 0.6837 4 5.91 1.44 75.72% 0.250 3.20 0.7770 5 5.93 1.33 77.60% 0.230 2.80 0.6272 rata-rata
0.2012 3% 1 5.71
0.8691 SD
1.14 75.41% 0.250 3.20 0.7869 2 4.65 1.07 77.03% 0.320 4.60 1.0566 3 6.18 1.42 76.97% 0.230 2.80 0.6448 4 4.76 1.05 77.89% 0.340 5.00 1.1055 5 4.89 1.15 76.51% 0.250 3.20 0.7517 rata-rata
0.9401 SD
Sampel Ulangan Berat basah
1.24 73.70% 0.310 4.40 1.1572 2 5.16 1.26 75.49% 0.230 2.80 0.6863 3 4.95 1.07 78.30% 0.310 4.40 0.9548 4 5.17 1.18 77.20% 0.330 4.80 1.0944 5 5.04 1.13 77.56% 0.270 3.60 0.8078 rata-rata
0.0892 0,5% 1 4.72
1.0797 SD
1.62 78.20% 0.360 5.40 1.1772 2 7.74 1.89 75.64% 0.300 4.20 1.0231 3 6.46 1.41 78.24% 0.360 5.40 1.1750 4 6.89 1.63 76.37% 0.300 4.20 0.9925 5 6.60 1.55 76.58% 0.310 4.40 1.0305 rata-rata
Konversi KA (mg/kg berat basah) kontrol 1 7.41
Cu (mg/kg)
Cu Kadar
Air Abs
(gr) Kadar
(gr) Berat kering
Perpustakaan Unika
Perpustakaan Unika LAMPIRAN 11. Hasil Analisa Anova Satu Arah untuk Logam Cd Tests of Normality a
Kolmogorov-Smirnov Shapiro-Wilk perlakuan Statistic df Sig. Statistic df Sig. cd kontrol .167
5 .200* .979 5 .926 0.5% .254 5 .200* .826 5 .130 1% .203 5 .200* .978 5 .925 3% .204 5 .200* .969 5 .866 5% .208 5 .200* .924 5 .558 *.
This is a lower bound of the true significance.
a.
Lilliefors Significance Correction
Descriptives
cd95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum kontrol
5 2.242860 .4936421 .2207635 1.629922 2.855798 1.6494 2.8907 0.5% 5 1.479080 .2996566 .1340105 1.107007 1.851153 1.2451 1.9830 1% 5 1.578320 .5209366 .2329699 .931492 2.225148 .9067 2.3392 3% 5 1.328820 .3620650 .1619204 .879257 1.778383 .8498 1.8421 5% 5 1.705240 .6758944 .3022692 .866006 2.544474 .9520 2.5017 Total
25 1.666864 .5486425 .1097285 1.440395 1.893333 .8498 2.8907
Perpustakaan Unika Test of Homogeneity of Variances cd Levene
Statistic df1 df2 Sig.
1.104
4 20 .382 ANOVA cd Sum of
Squares df Mean Square F Sig. Between Groups 2.453
4 .613 2.571 .069 Within Groups 4.771 20 .239 Total 7.224
24 cd a
Duncan Subset for alpha = .05 perlakuan N
1
2 3% 5 1.328820 0.5% 5 1.479080 1% 5 1.578320 1.578320 5% 5 1.705240 1.705240 kontrol 5 2.242860 Sig.
.277 .054 Means for groups in homogeneous subsets are displayed.
a.
Uses Harmonic Mean Sample Size = 5.000.
Perpustakaan Unika LAMPIRAN 12. Hasil Analisa Anova Satu Arah untuk Logam Cu Tests of Normality a
Kolmogorov-Smirnov Shapiro-Wilk perlakuan Statistic df Sig. Statistic df Sig. cu kontrol .309
5 .133 .799 5 .079 0.5% .185 5 .200* .954 5 .766 1% .259
5 .200* .891 5 .362 3% .182 5 .200* .951 5 .742 5% .281 5 .200* .913 5 .484 *. This is a lower bound of the true significance.
a.
Lilliefors Significance Correction
Descriptives
cu95% Confidence Interval for Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum kontrol
5 1.079660 .0891857 .0398851 .968921 1.190399 .9925 1.1772 0.5% 5 .940100 .1956238 .0874856 .697201 1.182999 .6863 1.1572 1% 5 .869100 .2011786 .0899698 .619304 1.118896 .6448 1.1055 3% 5 .705920 .1078014 .0482102 .572067 .839773 .5899 .8518 5% 5 .818800 .2357971 .1054517 .526019 1.111581 .4798 1.0573 Total
25 .882716 .2045019 .0409004 .798302 .967130 .4798 1.1772
Perpustakaan Unika Test of Homogeneity of Variances cu Levene
Statistic df1 df2 Sig.
2.677
4 20 .062 ANOVA cu Sum of
Squares df Mean Square F Sig. Between Groups .388 4 .097 3.151 .037 Within Groups
.616 20 .031 Total 1.004
24 cu a
Duncan Subset for alpha = .05 perlakuan N
1
2 3% 5 .705920 5% 5 .818800 1% 5 .869100 .869100 0.5% 5 .940100 .940100 kontrol 5 1.079660 Sig.
.065 .086 Means for groups in homogeneous subsets are displayed.
a.
Uses Harmonic Mean Sample Size = 5.000.
Perpustakaan Unika
LAMPIRAN 13. Perhitungan Hazard Quotients (HQ) dan Jumlah Maksimal
Konsumsi (JMK) pada Kerang Darah yang Masih Mengandung Logam CdPercentil Perlakuan C Ke- WC WI HQ JMK
Kontrol 2.2428 10 19.0000 42.6140 0.1 171.6570 50 38.0000 85.2281 0.2 171.6570 90 76.0000 170.4562 0.4 171.6570
K0.5% 1.4791 10 19.0000 28.1024 0.1 260.2976 50 38.0000 56.2049 0.1 260.2976 90 76.0000 112.4098 0.3 260.2976
K1% 1.5783 10 19.0000 29.9883 0.1 243.9283 50 38.0000 59.9766 0.2 243.9283 90 76.0000 119.9533 0.3 243.9283
K3% 1.3288 10 19.0000 25.2478 0.1 289.7278 50 38.0000 50.4957 0.1 289.7278 90 76.0000 100.9914 0.3 289.7278
K5% 1.7052 10 19.0000 32.3995 0.1 225.7754 50 38.0000 64.7989 0.2 225.7754 90 76.0000 129.5978 0.3 225.7754
Menurut perhitungan dengan MS Excel : Contoh perhitungan perlakuan Kontrol percentil ke-10: WI = C x WC = 2,2428 (µg/g) x 19 (g/minggu) = 42,6140 µg/minggu HQ = WI / PTWI = 42,6140 µg / (7 (µg/kg) x 55kg) = 0,11 JMK = (1/HQ) x WC = (1/0,11) x 19 = 171,6570 (menurut perhitungan dengan MS Excel)