Process Description Design Simulation of Filing Sequence and Solidification Time for Cast Metal Matrix Composite by Low Pressure Die Casting.

Special Issue on Heat Transfer, February 2011 Manuscript received and revised January 2011, accepted February 2011 Copyright © 2011 Praise Worthy Prize S.r.l. - All rights reserved 257 Simulation of Thermal Transfer Process in Cast Ingots at Electron Beam Melting and Refining Katia Zh. Vutova, Elena G. Koleva, Georgi M. Mladenov Abstract – Computer simulations of the heat transfer processes at electron beam melting and refining is a tool for better understanding and choice of optimal regimes of application of this expensive modern technology. The heat exchange at different interfaces between the casting ingot and both the water-cooled crucible and the pulling mechanism is studied. Radiation and evaporation losses from the top molten surface of drip cast ingots are also evaluated. Regression equations for the heat flows through the concrete boundary surfaces, as well as for the volume of the molten metal pool have been created. They are considered as functions of the coefficients of the heat transfer and the width of the heat contact ring between the top part of the casting ingot and the copper crucible. The response surface plots are obtained to visualize these dependences. They can be used for choosing proper process conditions and for the optimization of the heat flows according to the process requirements. Copyright © 2011 Praise Worthy Prize S.r.l. - All rights reserved. Keywords: Electron Beam, Heat Transfer, Crucible, Molten Pool, Cast Ingot

I. Introduction

The electron beam melting and refining EBMR is a widely used method of the special electric-metallurgy, due to the vacuum environment, the use of water-cooled crucibles and the possibility to elevate the metal temperature to high values 30–50 higher, than the melting temperature of the metal T m . The energy of the heating source in this method can be controlled independently from the melted material properties, from the cross-section of the re-melted material, from the volume of the melted metal pool and from the design peculiarities of the crucible used. This extends the ability to control the speed of melting or the speed of crystallization of the casting ingot and in this way the quality of the manufactured metal. In comparison with other metallurgic methods the EBMR provides a better refining of the casting metal from solvable gases and non-metal inclusions, as well as from easily evaporated metal components. The blocks produced by EBMR have more isotropic mechanical properties and the density of the produced metal is comparable with the densities of deformed metals. Metals such as W, Ta, Ti, Nb, Mo, Zr, Hf, V, Pt, Cu, alloys, steels and precision alloys based on Fe, Ni, Co and Cu are produced by this flexible technology. The up to date EBMR plants manufacture samples ranging from small quantities such as pure metal tablets of a few grams to large scale ingots weighting up to 5 000–25 000 kg. At the same time, the composition control and the inclusion cleanliness of the metal alloys remain a delicate problem not completely solved. The optimization of the process and equipment designs is hard task due to unknown process parameters that are difficult to be directly measured. Computer simulation can give a better understanding of the coupled mechanisms heat and mass transfer involved in the melting operation. Previous numerical study of heat flows during EBMR was made in [1] – [8]. The calculations reveal the importance of the some process characteristics that values are not exactly known. A need for more clear understanding of the EBMR process details was indicated. In this paper results based on our heat transfer computer tool [1]– [3] and regression analysis [9]-[11] of the obtained, by numerical experiments, data are given. The aim is to clarify the influence of the heat exchange at different interfaces between the casting ingot and both the water-cooled crucible and the pulling mechanism as well as to get some data for evaporation and irradiation losses from the top surface of the melting pool at electron beam drip melting and refining because in the case of use of hearth the main transfer processes are similar.

II. Process Description

Two kinds of electron beam melting and refining EBMR could be distinguished: i drip EBMR and ii hearth EBMR. The drip melting is the classical method for processing of refractory metals. Raw material in form of bars is fed horizontally or vertically in vacuum Copyright © 2011 Praise Worthy Prize S.r.l. - All rights reserved International Review of Mechanical Engineering, Vol. 5, N. 2 Special Issue on Heat Transfer 258 environment and is drip-melted directly into the withdrawal bottom of a copper water-cooled crucible Fig. 1. The refined metal is extremely pure, due to lack of contact with a ceramic pot surface, typical for conventional metallurgical re-melting technologies. During the EBMR droplets, created on the front surface of the feeding rod, fall on the surface of the molten pool, situated on the upper part of the cast ingot. At the same time the electron beams heat this surface, keeping it molten. The liquid pool surface is maintained on a constant level, suitable to be viewed by the operator and to adequate withdrawal continuously or by small steps of the bottom of the growing cast ingot. Refining is based on degassing and selective evaporation of metallic and non-metallic constituents with vapor pressures higher than the base material. Hard inclusions that can exist there could floats or being solute in the molten metal. Mostly repeated re-melting of the first-melt-ingots is applied to achieve the required final quality of the performed metal. Often, for repeated re-melting vertical feeding is applied due to more uniform irradiation of the molten pool surface. Fig. 1. Drip melting A principle scheme of electron beam drip-melting- furnace is shown in Fig. 1. The process is held in a vacuum chamber, one or several electron-optical systems 2 are mounted, and in which intense electron beams 3 are generated and directed to interaction zones on the re- melting bar and on the molten pool on the top surface of the cast ingot. The electrons that fall on the refining metal 4, heat it and the molten metal in the form of drops fall in a copper crucible 5 with water cooling 6 and cast ingot 7, solidified on a moving down bottom. The surface of the molten metal in the crucible is also heated by the electrons. The electron beam and the high vacuum provide degassing and high level of refining, as well as homogeneity of the chemical composition and optimal structure of the cast ingots. The method provides independent control of the melting speed and the crystallization speed; the power distribution and overheating of the molten material can be optimal, there are no impurities from the crucible and there is possibility to realize electro-dynamic movement of the molten metal in the crucible. Second important scheme of EBMR is shown in Fig. 2. An intermediate water cooled copper pot, termed hearth, is used to reach higher refining level due to the higher ratio between the surface area and molten metal depth there and due to the additional possibility to stop transportation of refractory nonmetallic inclusions that form slag on the top of the molten pool in the hearth by a cooled surface barrier on its surface or heavier metallic inclusions such as tungsten carbide chips from machining instruments in titanium. After refining in the intermediate cold hearth the molten metal goes to the water cooled crucible, as it was in the drip melting. This technology method is applied in the case of performing extremely pure metals at higher energy consumption. Fig. 2. Electron beam melting and refining with a hearth: 1-electron guns, 2- electron beams, 3-feeding mechanism for scrap or compacted fed ingot, 4- hearth, filled with molten metal, 5- crucible, 6- water cooling, 7- cast ingot pulled down Often the raw material is fed into the melting space after compacting by cold pressing without oil or after casting and welding of tablets as compact ingots 4 in Fig. 1 or 3 in Fig. 2. Another important possibility is when the re-melted scrap or raw material for example sponge is fed as small particles utilizing a vibrating or screw-like feeding mechanism. The main characteristics of the melting process which the operator can control are: beam power and beam current, because usually the accelerated voltage is constant during the melting; beam focusing current that defines the average power density in the beam spot on the molten material; melting rate andor casting velocity, or speed of feeding and pulling mechanisms together with the cross section and densities of the transported metal that define the residual times of molten metal in the hearth and in the molten pool. Using a deflection control unit the operator moves the beams on the molten surface. The frequency and the trajectory of the beam deflection, together with the beam energy values and chosen energy densities as well as the material thermo- physical parameters and the dimensions of hearth and crucible determine the heating flows, mass transport in the molten pool and evaporation rates. Copyright © 2011 Praise Worthy Prize S.r.l. - All rights reserved International Review of Mechanical Engineering, Vol. 5, N. 2 Special Issue on Heat Transfer 259

III. Heat Model for Solidification of