Specimen’s Microstructure Study

52 without calcium carbonate fillers. As for the tensile stress improvement due to addition of calcium carbonate fillers, there is bonding happens between the epoxy composite. The bond’s strength is good, hence causing higher energy to break the bond. This is resulting higher tensile stress needed. 53 SAMPLE wt of CaCO 3 MAGNIFICATION 21 X 500 X 1.00 K X 2 Figure 4.11 : Scanning Electron Micrograph of tensile Fractured Surface of 0 and 2 weight of nano-CaCO 3 54 SAMPLE wt of CaCO 3 MAGNIFICATION 21 X 500 X 1.00 K X 4 6 Figure 4.12 : Scanning Electron Micrograph of tensile Fractured Surface of 4 and 6 weight of nano-CaCO 3 55 SAMPLE wt of CaCO3 MAGNIFICATION 21 X 500 X

1.00 K X

8 Figure 4.13 : Scanning Electron Micrograph of tensile Fractured Surface of 8 weight of nano-CaCO 3 56 56 CHAPTER 5 CONCLUSIONS AND RECOMMENDATIONS

5.0 CONCLUSIONS

After all the testing and result analysis, it can be concluded that the objective to determine the effect of nano-CaCO 3 to mechanical properties of e p o x y c o m p o s i t e r e i n f o r c e d recycle rubber has been achieved. All the mechanical properties of these specimens were determine by conducting the tensile test, impact test, Scanning Electron Microscope SEM and microhardness test. The effects of nano-CaCO 3 towards mechanical properties of epoxy composite can be explained by the analysis of the microstructure. The whole experiment and the study effect of nano- CaCO 3 towards mechanical properties can be summarized as below: 1. The tensile stress of polymer matrix composite are been affected by the nano CaCo 3 . Higher nano CaCo 3 produced higher tensile stress and tensile strain. The maximum stress obtained at higher nano CaCo 3 is 22.64 Mpa 2. The tensile strain increase as the nano-CaCo 3 is increase. Material behaves more ductile as the nano-CaCo 3 is increase. 3. The tensile strain is decrease as nano CaCo 3 increase. This means the brittle increase as nano CaCo 3 is lower.