5000 rpm selama 30 menit Fraksi tidak terlarut Fraksi terlarut Pengujian kandungan logam kadmium dan tembaga (AAS) Destruksi logam 1 gram ekstrak pektin dari masing-masing daun bayam 1 ml larutan logam tembaga atau kadmium
Lampiran 1. Diagram Alir Penelitian Pendahuluan 1 gram ekstrak pektin 50 ml larutan 1 ml larutan logam dari masing-masing buffer natrium tembaga atau kadmium bikarbonat daun bayam Dilakukan proses inkubasi pada suhu 37°C pada hotplate dan diaduk dengan stirrer
Inkubasi selama 90 Inkubasi selama 30 Inkubasi selama 60 menit menit menit Dimasukkan ke dalam tabung reaksi Disentrifugasi pada kecepatan
5000 rpm selama 30 menit
Fraksi tidak terlarut Fraksi terlarut Lampiran 2. Diagram Alir Penelitian Utama Dimasukkan ke dalam tabung reaksi
Disentrifugasi pada kecepatan 5000 rpm selama 30 menit Fraksi tidak terlarut Fraksi terlarut Destruksi logam
1 gram ekstrak pektin dari masing-masing daun bayam 1 ml larutan logam tembaga atau kadmium 50 ml larutan buffer natrium bikarbonat Dilakukan proses inkubasi pada suhu 37°C pada hotplate dan diaduk dengan stirrer
Inkubasi selama 60 menit Inkubasi selama 90 menit
Inkubasi selama 120 menit
Lampiran 3. Tabel Uji Normalitas Penyerapan Pektin Daun Bayam Terhadap
Logam Kadmium (Cd) Tests of Normal ity.189 5 .200* .933 5 .615 .253 5 .200* .892 5 .369 .201 5 .200* .942 5 .678 .173 5 .200* .971 5 .882 .204 5 .200* .946 5 .707 .202 5 .200* .924 5 .553 .199 5 .200* .912 5 .481 .222 5 .200* .908 5 .456 .153 5 .200* .988 5 .972 .217 5 .200* .888 5 .348 .209 5 .200* .966 5 .846 .186 5 .200* .930 5 .593 .178 5 .200* .982 5 .946 .262 5 .200* .914 5 .495 .204 5 .200* .943 5 .689 .183 5 .200* .948 5 .724 .243 5 .200* .944 5 .695 .184 5 .200* .950 5 .738 .200 5 .200* .943 5 .685 .136 5 .200* .987 5 .967 .266 5 .200* .889 5 .354 .202 5 .200* .933 5 .615 .180 5 .200* .952 5 .753 .246 5 .200* .924 5 .556 .219 5 .200* .916 5 .501 .198 5 .200* .929 5 .588 .206 5 .200* .886 5 .336 .261 5 .200* .951 5 .741 .293 5 .185 .778 5 .053 .201 5 .200* .978 5 .922 .154 5 .200* .969 5 .870 .270 5 .200* .860 5 .229 .296 5 .175 .737 5 .022 .239 5 .200* .926 5 .567 .202 5 .200* .921 5 .534 .294 5 .183 .920 5 .530
Kombinasi PDBS 60 Menit PDBS 90 Menit PDBS 120 Menit PDBM 60 Menit PDBM 90 Menit PDBM 120 Menit PDBK 60 Menit PDBK 90 Menit PDBK 120 Menit PK 60 Menit PK 90 Menit PK 120 Menit PDBS 60 Menit PDBS 90 Menit PDBS 120 Menit PDBM 60 Menit PDBM 90 Menit PDBM 120 Menit PDBK 60 Menit PDBK 90 Menit PDBK 120 Menit PK 60 Menit PK 90 Menit PK 120 Menit PDBS 60 Menit PDBS 90 Menit PDBS 120 Menit PDBM 60 Menit PDBM 90 Menit PDBM 120 Menit PDBK 60 Menit PDBK 90 Menit PDBK 120 Menit PK 60 Menit PK 90 Menit PK 120 Menit
Cd_Padat Cd_Cair Cd_Total Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnov
a
Shapiro-Wilk This is a lower bound of t he t rue signif icance.
- .
a.
Lampiran 4. Tabel Uji Normalitas Penyerapan Pektin Daun Bayam Terhadap
Logam Tembaga (Cu) Tests of Normal ity.223 5 .200* .957 5 .787 .180 5 .200* .967 5 .859 .157 5 .200* .990 5 .979 .234 5 .200* .883 5 .324 .319 5 .107 .861 5 .233 .248 5 .200* .929 5 .588 .220 5 .200* .869 5 .263 .286 5 .200* .813 5 .103 .212 5 .200* .932 5 .608 .226 5 .200* .946 5 .707 .262 5 .200* .866 5 .250 .330 5 .079 .735 5 .021 .158 5 .200* .981 5 .939 .130 5 .200* .994 5 .992 .200 5 .200* .946 5 .711 .306 5 .143 .757 5 .035 .189 5 .200* .980 5 .935 .292 5 .188 .895 5 .384 .227 5 .200* .960 5 .805 .251 5 .200* .896 5 .391 .178 5 .200* .958 5 .794 .323 5 .095 .896 5 .389 .222 5 .200* .911 5 .471 .211 5 .200* .942 5 .682 .147 5 .200* .987 5 .970 .246 5 .200* .922 5 .543 .281 5 .200* .881 5 .312 .270 5 .200* .879 5 .303 .291 5 .191 .862 5 .236 .270 5 .200* .910 5 .465 .165 5 .200* .966 5 .848 .247 5 .200* .834 5 .149 .207 5 .200* .927 5 .574 .213 5 .200* .919 5 .520 .386 5 .014 .716 5 .014 .361 5 .032 .725 5 .017
Kombinasi PDBS 60 Menit PDBS 90 Menit PDBS 120 Menit PDBM 60 Menit PDBM 90 Menit PDBM 120 Menit PDBK 60 Menit PDBK 90 Menit PDBK 120 Menit PK 60 Menit PK 90 Menit PK 120 Menit PDBS 60 Menit PDBS 90 Menit PDBS 120 Menit PDBM 60 Menit PDBM 90 Menit PDBM 120 Menit PDBK 60 Menit PDBK 90 Menit PDBK 120 Menit PK 60 Menit PK 90 Menit PK 120 Menit PDBS 60 Menit PDBS 90 Menit PDBS 120 Menit PDBM 60 Menit PDBM 90 Menit PDBM 120 Menit PDBK 60 Menit PDBK 90 Menit PDBK 120 Menit PK 60 Menit PK 90 Menit PK 120 Menit
Cu_Padat Cu_Cair Cu_Total Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnov
a
Shapiro-Wilk This is a lower bound of t he t rue signif icance.
- .
a. Lampiran 5. Tabel Uji Beda Pektin Daun Bayam Terhadap Logam Kadmium (Cd) oleh Fraksi Tidak Terlarut Antara Waktu Kontak dan Varietas Lampiran 6. Tabel Uji Beda Pektin Daun Bayam Terhadap Logam Kadmium (Cd) oleh Fraksi Terlarut Antara Waktu Kontak dan Varietas
Cd_Padat Duncan a
7
5 Subset f or alpha = .05
4
3
2
1
Kombinasi PK 60 Menit PDBM 60 Menit PK 90 Menit PK 120 Menit PDBS 60 Menit PDBM 90 Menit PDBS 90 Menit PDBK 60 Menit PDBM 120 Menit PDBK 90 Menit N
5 15. 1554 5 16. 0202 5 16. 7470 5 17. 0826 5 21. 6886 5 22. 5514
5 24. 5918
5 24. 9542
5 25. 4050
5 30. 4260Duncan a
a.
Uses Harmonic Mean Sample Size = 5.000.
8 Subset f or alpha = .05 Means f or groups in homogeneous s ubset s are display ed.
6
5 104.2002 5 106.9020 5 118.9590 5 129.4018 5 129.9740 129.9740 5 133.1170 5 139.2850
5
4
3
2
1
N
Kombinasi PK 120 Menit PDBK 60 Menit PK 90 Menit PK 60 Menit PDBK 90 Menit PDBK 120 Menit PDBM 60 Menit PDBS 60 Menit PDBM 90 Menit PDBS 90 Menit PDBM 120 Menit PDBS 120 Menit Sig.
5 180.1870 .106 1. 000 .729 .061 1. 000 .649 .220 1. 000
5 163.9310
5 161.8936
5 154.1208
5 153.3696
Cd_Cai r
Lampiran 7. Tabel Uji Beda Pektin Daun Bayam Terhadap Logam Tembaga (Cu) oleh Fraksi Tidak Terlarut Antara Waktu Kontak dan Varietas Lampiran 8. Tabel Uji Beda Pektin Daun Bayam Terhadap Logam Tembaga (Cu) oleh Fraksi Terlarut Antara Waktu Kontak dan Varietas
7 Subset f or alpha = .05 Means f or groups in homogeneous s ubset s are display ed.
4
3
2
1
N
Kombinasi PDBM 60 Menit PDBM 120 Menit PDBM 90 Menit PDBS 60 Menit PDBS 90 Menit PDBK 60 Menit PDBS 120 Menit PK 120 Menit PDBK 90 Menit
5 8. 4074 5 10. 0150 10. 0150 5 10. 8950 5 13. 7188 5 14. 0676 5 15. 1834 5 15. 3600 5 17. 1602 5 17. 3710
a
Duncan
Cu_Cai r
a.
Uses Harmonic Mean Sample Size = 5.000.
6
Cu_Padat
5
4
3
2
1
N
1. 000 .288 .081 .154 .446 .075 1. 000 Kombinasi PDBS 60 Menit PDBS 90 Menit PK 120 Menit PK 60 Menit PK 90 Menit PDBK 90 Menit PDBK 60 Menit PDBS 120 Menit PDBM 60 Menit PDBK 120 Menit PDBM 90 Menit PDBM 120 Menit Sig.
5 158.9310
5 143.0412
5 137.7958
5 87. 7130 5 96. 5460 5 98. 8650 5 99. 8388 99. 8388 5 104.9768 104.9768 5 109.2986 5 109.4020 5 127.1262 5 129.3414
a
Duncan
5 Subset f or alpha = .05
Lampiran 9. Tabel Uji ANOVA Penyerapan Pektin Daun Bayam Terhadap
Logam Kadmium (Cd)Lampiran 10. Tabel Uji ANOVA Penyerapan Pektin Daun Bayam Terhadap
Logam Tembaga (Cu)Test of Homogenei ty of Variances
1. 548
Cu_Padat Sum of Squares df Mean Square F Sig.
59 Between Groups Within Groups Tot al
27421.605
26423.205 11 2402.110 115.486 .000 998.400 48 20. 800
ANOVA
Lev ene Stat is tic df 1 df 2 Sig.
11 48 .561 Cu_Padat Cu_Cair
11 48 .146 .885
Sum of Squares df Mean Square F Sig.
1. 388
Cd_Padat Cd_Cair
59 Between Groups Within Groups Tot al Between Groups Within Groups Tot al
96. 834 48 2. 017 2628.043
59 2531.209 11 230.110 114.064 .000
30942.380
30619.541 11 2783.595 413.868 .000 322.839 48 6. 726
ANOVA
Lev ene Stat is tic df 1 df 2 Sig.
11 48 .541 Cd_Padat Cd_Cair
11 48 .210 .907