Pengaruh Temperatur Kalsinasi Pada Ekstraksi Silika Dari Abu Cangkang Kelapa Sawit
LAMPIRAN
Universitas Sumatera Utara
LAMPIRAN ALAT
File: C:\2020\DATA\ECH-300.SMP
Started
:11/09/2015 7:13:08
Completed
:14/09/2015 16:12:11
Report Time
:14/09/2015 7:38:21
Sample Mass
:0.3050 gWarm
Measured
Cold Free Space
:81.9857 cm³
Ambient Temperature :22.00 °CLow Pressure
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.009798
0.029125
0.057176
0.082912
0.099599
0.119381
0.139487
0.159724
0.179931
0.200131
0.244191
0.303063
0.350105
0.399961
0.450287
0.500379
0.55012
0.600017
0.649804
0.699978
0.745752
0.805859
0.826617
0.850981
0.874563
0.897243
0.923802
0.949563
0.973346
0.983102
0.995622
0.996341
71.49968
86.29842
97.4559
104.7595
108.795
113.1938
117.3405
121.3005
125.1794
128.9702
137.1807
148.5905
158.4583
169.9559
182.6863
196.6297
212.2304
230.4077
252.3323
279.1239
308.9076
351.4478
363.9205
375.5537
384.5922
393.4653
405.6988
420.6743
438.5448
447.9589
456.6125
463.9799
Analysis Adsorptive :N2
Analysis Bath Temp. :77.257 K
Thermal Correction :No
Free Space
:25.7288 cm³
Equilibration Interval :10 s
Dose
:None
SIO2 - Desorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.996341
463.9799
0.986397
458.7902
0.977309
453.289
0.968518
449.2385
0.958063
441.5128
0.932852
427.6534
0.904992
415.2422
0.877274
404.1742
0.850288
394.524
0.82551
386.5197
0.800266
379.1814
0.754841
365.4489
0.699447
338.2937
0.655842
296.4074
0.57313
239.1486
0.554505
230.2329
0.498024
206.891
0.454405
189.1147
0.393737
169.5922
0.352448
159.8215
0.305672
149.8134
0.254144
139.633
0.200678
129.5569
0.141334
118.2091
0.078811
104.2582
Universitas Sumatera Utara
File: C:\2020\DATA\ECH-300.SMP
Started
:11/09/2015 7:13:08
Completed
:14/09/2015 16:12:11
Report Time
:14/09/2015 7:38:21
Sample Mass
:0.3050 gWarm
Measured
Cold Free Space
:81.9857 cm³
Ambient Temperature :22.00 °CLow Pressure
BJH Adsorpsi Pore Size Distribution
Average Width
(nm)
136.6822
86.37838
47.3277
30.65912
22.3052
17.81721
14.91053
12.75069
11.23543
9.044592
7.396786
6.275653
5.403861
4.722241
4.171159
3.711787
3.319114
2.979563
2.689533
2.394109
2.145129
2.001254
1.906235
1.811464
1.716411
Incremental
Pore Volume
(cm³/g)
0.014179
0.015774
0.031082
0.026807
0.022482
0.016669
0.017482
0.02352
0.026145
0.093798
0.067346
0.061183
0.050171
0.04123
0.03504
0.030978
0.027911
0.024481
0.019813
0.021119
0.013672
0.005926
0.005911
0.005676
0.005853
Analysis Adsorptive :N2
Analysis Bath Temp. :77.257 K
Thermal Correction :No
Free Space
:25.7288 cm³
Equilibration Interval :10 s
Dose
:None
Cumulative
Pore Volume
(cm³/g)
0.014179
0.029953
0.061035
0.087841
0.110324
0.126992
0.144475
0.167994
0.19414
0.287937
0.355284
0.416467
0.466638
0.507868
0.542908
0.573886
0.601797
0.626278
0.646092
0.66721
0.680882
0.686808
0.692719
0.698395
0.704248
Incremental
Pore Area
(m²/g)
0.414953
0.730451
2.626956
3.497362
4.031726
3.742201
4.689962
7.378272
9.308169
41.48233
36.41926
38.99705
37.13735
34.92448
33.60183
33.38348
33.63626
32.86575
29.46738
35.28417
25.49356
11.84425
12.40429
12.53315
13.64087
Cumulative
Pore Area
(m²/g)
0.414953
1.145404
3.77236
7.269722
11.30145
15.04365
19.73361
27.11188
36.42005
77.90239
114.3216
153.3187
190.456
225.3805
258.9824
292.3658
326.0021
358.8678
388.3352
423.6194
449.113
460.9572
473.3615
485.8946
499.5355
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-500.SMP
Started
:14/09/2015 7:49:03
Completed
:15/09/2015 12:19:52
Report Time
:15/09/2015 7:05:34
Sample Mass
:0.2350 g
Measured
Cold Free Space
:78.1496 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.009688
61.59142
0.03121
77.31448
0.060277
88.42426
0.085027
95.37787
0.099647
98.9834
0.119407
103.4594
0.139392
107.7212
0.159527
111.8166
0.179591
115.7819
0.199908
119.7255
0.244772
128.4186
0.30143
139.8411
0.352563
150.9898
0.401041
162.4774
0.451504
175.2858
0.499529
188.9161
0.54986
205.15
0.599509
223.9598
0.649766
246.7072
0.699617
274.2414
0.749635
307.6294
0.798838
342.9726
0.827138
359.2642
0.851673
369.5842
0.87492
377.3806
0.899269
385.5834
0.923524
395.2019
0.949459
407.7845
0.973596
423.4444
0.982216
430.8404
0.990347
439.6403
0.995144
447.0302
Analysis Adsorptive :N2
Analysis Bath Temp. :77.267 K
Thermal Correction :No
Warm Free Space:24.2568 cm³
Equilibration Interval :10 s
Low Pressure Dose :None
SIO2 - Desorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.995144
0.982884
0.973902
0.954929
0.923809
0.903036
0.876876
0.851088
0.825631
0.80085
0.753437
0.698762
0.648864
0.599359
0.545728
0.493925
0.444302
0.391842
0.35491
0.304031
0.250151
0.202862
0.141296
0.082457
447.0302
441.6817
435.8327
424.7504
410.4255
402.4593
393.4906
385.3702
378.1456
371.8051
359.6826
335.9458
288.2631
249.0841
219.7384
198.1495
176.875
160.671
151.7933
140.5161
129.5115
120.335
108.2113
94.8736
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-500.SMP
Started
:14/09/2015 7:49:03
Completed
:15/09/2015 12:19:52
Report Time
:15/09/2015 7:05:34
Sample Mass
:0.2350 g
Measured
Cold Free Space
:78.1496 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
BJH Adsorpsi Pore Size Distribution
Average Width
Incremental
(nm)
Pore Volume
(cm³/g)
241.5124
0.011962
131.2857
0.014456
86.07397
0.012325
47.19616
0.027084
30.48069
0.022348
22.51849
0.017503
17.88811
0.015253
14.89033
0.014927
12.71739
0.020616
10.92915
0.033965
8.971182
0.076954
7.351761
0.074439
6.19349
0.061841
5.320021
0.050954
4.638948
0.041734
4.086112
0.035402
3.636084
0.029131
3.248448
0.026643
2.912799
0.023441
2.61055
0.021619
2.31399
0.020322
2.066639
0.013877
1.920981
0.005824
1.826106
0.005632
1.731899
0.005578
Analysis Adsorptive :N2
Analysis Bath Temp. :77.267 K
Thermal Correction :No
Warm Free Space:24.2568 cm³
Equilibration Interval :10 s
Low Pressure Dose :None
Cumulative Pore
Volume (cm³/g)
0.011962
0.026418
0.038743
0.065826
0.088175
0.105677
0.12093
0.135856
0.156473
0.190437
0.267391
0.34183
0.40367
0.454625
0.496359
0.531761
0.560891
0.587534
0.610976
0.632595
0.652917
0.666794
0.672619
0.678251
0.683828
Incremental
Pore Area
(m²/g)
0.198112
0.440457
0.572744
2.29542
2.93279
3.109012
3.410657
4.009717
6.484402
12.43087
34.31147
40.50128
39.93912
38.31148
35.98591
34.65559
32.04615
32.80706
32.19082
33.12584
35.12972
26.85922
12.1276
12.33686
12.88226
Cumulative Pore
Area (m²/g)
0.198112
0.638569
1.211312
3.506732
6.439523
9.548535
12.95919
16.96891
23.45331
35.88418
70.19565
110.6969
150.636
188.9475
224.9334
259.589
291.6352
324.4422
356.6331
389.7589
424.8886
451.7478
463.8754
476.2123
489.0946
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-700.SMP
Started
:15/09/2015 7:45:17
Completed
:15/09/2015 7:45:01
Report Time
:15/09/2015 15:59:21
Sample Mass
:0.1900 g
Measured
Cold Free Space
:82.5904 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.01003
0.030701
0.059143
0.077235
0.099746
0.119825
0.139848
0.159961
0.180016
0.200151
0.247716
0.302264
0.35324
0.400277
0.450164
0.500676
0.550436
0.600681
0.650205
0.700004
0.749299
0.799322
0.824218
0.853217
0.878192
0.900638
0.924453
0.950535
0.975529
0.983727
0.995868
0.99711
33.17376
41.29888
47.04626
49.74762
52.61896
54.90581
57.02176
59.00787
60.90864
62.75785
67.02337
71.90316
76.73678
81.61825
87.49305
94.44343
102.8611
113.5164
127.2798
146.1564
172.947
212.4979
235.3901
261.3243
279.8934
293.9669
308.6755
326.2579
346.8893
355.5568
365.0856
377.0766
Analysis Adsorptive :N2
Analysis Bath Temp. :77.246 K
Thermal Correction :No
Warm Free Space:25.9767 cm³
Equilibration Interval:10 s
Low Pressure Dose :None
SIO2 - Desorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.99711
377.0766
0.990749
366.6811
0.974991
359.8925
0.954732
347.1838
0.924648
330.2734
0.903314
319.9489
0.876606
307.7925
0.850644
296.3747
0.826561
284.9547
0.800596
271.555
0.754026
239.8788
0.70588
193.2598
0.645881
147.1869
0.59838
125.7952
0.542133
108.663
0.506361
100.7168
0.454937
90.32428
0.398244
81.33079
0.349897
76.18548
0.303014
71.68985
0.25045
66.91978
0.2004
62.40045
0.140529
56.67238
0.080557
49.75306
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-700.SMP
Started
:15/09/2015 7:45:17
Analysis Adsorptive :N2
Completed
:15/09/2015 7:45:01
Analysis Bath Temp. :77.246 K
Report Time
:15/09/2015 15:59:21
Thermal Correction :No
Sample Mass
:0.1900 g
Warm Free Space:25.9767 cm³
Measured
Cold Free Space
:82.5904 cm³
Equilibration Interval:10 s
Ambient Temperature :22.00 °C
Low Pressure Dose :None
Automatic Degas
:Yes
BJH Adsorpsi Pore Size Distribution
Average Width Incremental Cumulative
Incremental
Cumulative
(nm)
Pore
Pore Volume Pore Area
Pore Area
Volume
(cm³/g)
(m²/g)
(m²/g)
(cm³/g)
141.5333
0.015513
0.015513
0.438413
0.438413
92.98003
0.014412
0.029925
0.620006
1.058419
48.35907
0.035692
0.065617
2.952274
4.010694
30.88384
0.031292
0.096909
4.052921
8.063615
22.79387
0.026922
0.123832
4.724484
12.7881
18.26394
0.026504
0.150335
5.804584
18.59268
15.11038
0.036219
0.186554
9.587778
28.18046
12.61127
0.052369
0.238923
16.61011
44.79057
10.85712
0.047236
0.286159
17.40276
62.19333
8.950387
0.083339
0.369498
37.24499
99.43832
7.335724
0.05581
0.425308
30.43203
129.8703
6.182685
0.038072
0.46338
24.63124
154.5016
5.314385
0.026428
0.489808
19.89184
174.3934
4.62974
0.019116
0.508924
16.51546
190.9089
4.076148
0.013893
0.522817
13.63391
204.5428
3.614106
0.010194
0.533012
11.28286
215.8256
3.222058
0.007631
0.540643
9.473602
225.2993
2.89425
0.005468
0.546111
7.55729
232.8565
2.595811
0.004645
0.550756
7.157657
240.0142
2.306052
0.003955
0.554711
6.860396
246.8746
2.053673
0.003171
0.557882
6.175536
253.0501
1.903453
0.001296
0.559178
2.723497
255.7736
1.808967
0.001331
0.560509
2.943559
258.7172
1.71484
0.001387
0.561896
3.234707
261.9519
Universitas Sumatera Utara
C:\2020\DATA\ECH-900.SMP
Started
:15/09/2015 16:11:00
Completed
:16/09/2015 18:10:54
Report Time
:16/09/2015 7:24:10
Sample Mass
:0.2800 g
Measured
Cold Free Space
:81.7593 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.011152
4.100603
0.032029
5.071684
0.066855
5.87981
0.079617
6.103362
0.099913
6.417791
0.12014
6.698195
0.14016
6.948123
0.159785
7.185942
0.179766
7.411308
0.199764
7.622845
0.249174
8.146273
0.300558
8.657114
0.350732
9.149714
0.399955
9.650325
0.449983
10.16782
0.499896
10.71215
0.549758
11.2977
0.599717
11.96249
0.649733
12.71752
0.699569
13.60701
0.749363
14.71981
0.799028
16.24785
0.8199
17.13452
0.849209
18.81537
0.873644
20.97894
0.89775
24.63322
0.920585
31.57259
0.951204
54.36078
0.966926
76.4219
0.974181
90.53974
0.986767
118.3726
0.992431
129.2093
Analysis Adsorptive :N2
Analysis Bath Temp. :77.240 K
Thermal Correction :No
Warm Free Space:25.7123 cm³
Equilibration Interval :10 s
Low Pressure Dose :None
SIO2 – Desorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.992431
0.97934
0.968998
0.949829
0.924251
0.896586
0.873598
0.851785
0.825828
0.803495
0.75321
0.703263
0.652541
0.600763
0.550276
0.500752
0.450517
0.400596
0.350619
0.300693
0.250717
0.200754
0.121173
0.069055
129.2093
125.7058
120.2861
100.3231
66.78152
45.82331
34.02169
26.41426
21.25293
18.64492
15.51915
13.86915
12.72316
11.83561
11.11288
10.4865
9.880975
9.355215
8.850689
8.3513
7.857176
7.335342
6.405588
5.615526
Universitas Sumatera Utara
:\2020\DATA\ECH-900.SMP
Started
:15/09/2015 16:11:00
Analysis Adsorptive :N2
Completed
:16/09/2015 18:10:54
Analysis Bath Temp. :77.240 K
Report Time
:16/09/2015 7:24:10
Thermal Correction :No
Sample Mass
:0.2800 g
Warm Free Space:25.7123 cm³
Measured
Cold Free Space
:81.7593 cm³
Equilibration Interval :10 s
Ambient Temperature :22.00 °C
Low Pressure Dose :None
Automatic Degas
:Yes
BJH Adsorpsi Pore Size Distribution
Average Width
Incremental
Cumulative
Incremental Cumulative
(nm)
Pore Volume
Pore
Pore Area
Pore Area
(cm³/g)
Volume
(m²/g)
(m²/g)
(cm³/g)
174.7332
0.017745
0.017745
0.406223
0.406223
91.45912
0.046732
0.064477
2.043855
2.450079
66.45846
0.023946
0.088423
1.441247
3.891326
47.1301
0.038092
0.126515
3.232898
7.124223
29.80583
0.040201
0.166716
5.395082
12.51931
22.1008
0.011712
0.178428
2.119677
14.63898
17.73901
0.005699
0.184127
1.285189
15.92417
14.73903
0.00304
0.187168
0.825129
16.7493
12.37407
0.002098
0.189266
0.67832
17.42762
10.81869
0.001001
0.190267
0.370234
17.79785
9.023031
0.001531
0.191798
0.678489
18.47634
7.404204
0.000992
0.19279
0.53604
19.01238
6.248743
0.000751
0.193541
0.480672
19.49306
5.377764
0.000629
0.19417
0.467916
19.96097
4.69523
0.000564
0.194734
0.480729
20.4417
4.143906
0.000479
0.195213
0.461941
20.90364
3.685714
0.000466
0.195679
0.505241
21.40888
3.295303
0.000467
0.196145
0.566521
21.9754
2.959044
0.000498
0.196643
0.673371
22.64878
2.65944
0.000488
0.197132
0.734184
23.38296
2.382578
0.000543
0.197674
0.911445
24.2944
2.130333
0.000632
0.198307
1.186851
25.48125
1.977156
0.000229
0.198536
0.463676
25.94493
1.88316
0.000271
0.198807
0.576608
26.52154
1.790484
0.000314
0.199121
0.700486
27.22202
Universitas Sumatera Utara
Universitas Sumatera Utara
LAMPIRAN ALAT
File: C:\2020\DATA\ECH-300.SMP
Started
:11/09/2015 7:13:08
Completed
:14/09/2015 16:12:11
Report Time
:14/09/2015 7:38:21
Sample Mass
:0.3050 gWarm
Measured
Cold Free Space
:81.9857 cm³
Ambient Temperature :22.00 °CLow Pressure
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.009798
0.029125
0.057176
0.082912
0.099599
0.119381
0.139487
0.159724
0.179931
0.200131
0.244191
0.303063
0.350105
0.399961
0.450287
0.500379
0.55012
0.600017
0.649804
0.699978
0.745752
0.805859
0.826617
0.850981
0.874563
0.897243
0.923802
0.949563
0.973346
0.983102
0.995622
0.996341
71.49968
86.29842
97.4559
104.7595
108.795
113.1938
117.3405
121.3005
125.1794
128.9702
137.1807
148.5905
158.4583
169.9559
182.6863
196.6297
212.2304
230.4077
252.3323
279.1239
308.9076
351.4478
363.9205
375.5537
384.5922
393.4653
405.6988
420.6743
438.5448
447.9589
456.6125
463.9799
Analysis Adsorptive :N2
Analysis Bath Temp. :77.257 K
Thermal Correction :No
Free Space
:25.7288 cm³
Equilibration Interval :10 s
Dose
:None
SIO2 - Desorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.996341
463.9799
0.986397
458.7902
0.977309
453.289
0.968518
449.2385
0.958063
441.5128
0.932852
427.6534
0.904992
415.2422
0.877274
404.1742
0.850288
394.524
0.82551
386.5197
0.800266
379.1814
0.754841
365.4489
0.699447
338.2937
0.655842
296.4074
0.57313
239.1486
0.554505
230.2329
0.498024
206.891
0.454405
189.1147
0.393737
169.5922
0.352448
159.8215
0.305672
149.8134
0.254144
139.633
0.200678
129.5569
0.141334
118.2091
0.078811
104.2582
Universitas Sumatera Utara
File: C:\2020\DATA\ECH-300.SMP
Started
:11/09/2015 7:13:08
Completed
:14/09/2015 16:12:11
Report Time
:14/09/2015 7:38:21
Sample Mass
:0.3050 gWarm
Measured
Cold Free Space
:81.9857 cm³
Ambient Temperature :22.00 °CLow Pressure
BJH Adsorpsi Pore Size Distribution
Average Width
(nm)
136.6822
86.37838
47.3277
30.65912
22.3052
17.81721
14.91053
12.75069
11.23543
9.044592
7.396786
6.275653
5.403861
4.722241
4.171159
3.711787
3.319114
2.979563
2.689533
2.394109
2.145129
2.001254
1.906235
1.811464
1.716411
Incremental
Pore Volume
(cm³/g)
0.014179
0.015774
0.031082
0.026807
0.022482
0.016669
0.017482
0.02352
0.026145
0.093798
0.067346
0.061183
0.050171
0.04123
0.03504
0.030978
0.027911
0.024481
0.019813
0.021119
0.013672
0.005926
0.005911
0.005676
0.005853
Analysis Adsorptive :N2
Analysis Bath Temp. :77.257 K
Thermal Correction :No
Free Space
:25.7288 cm³
Equilibration Interval :10 s
Dose
:None
Cumulative
Pore Volume
(cm³/g)
0.014179
0.029953
0.061035
0.087841
0.110324
0.126992
0.144475
0.167994
0.19414
0.287937
0.355284
0.416467
0.466638
0.507868
0.542908
0.573886
0.601797
0.626278
0.646092
0.66721
0.680882
0.686808
0.692719
0.698395
0.704248
Incremental
Pore Area
(m²/g)
0.414953
0.730451
2.626956
3.497362
4.031726
3.742201
4.689962
7.378272
9.308169
41.48233
36.41926
38.99705
37.13735
34.92448
33.60183
33.38348
33.63626
32.86575
29.46738
35.28417
25.49356
11.84425
12.40429
12.53315
13.64087
Cumulative
Pore Area
(m²/g)
0.414953
1.145404
3.77236
7.269722
11.30145
15.04365
19.73361
27.11188
36.42005
77.90239
114.3216
153.3187
190.456
225.3805
258.9824
292.3658
326.0021
358.8678
388.3352
423.6194
449.113
460.9572
473.3615
485.8946
499.5355
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-500.SMP
Started
:14/09/2015 7:49:03
Completed
:15/09/2015 12:19:52
Report Time
:15/09/2015 7:05:34
Sample Mass
:0.2350 g
Measured
Cold Free Space
:78.1496 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.009688
61.59142
0.03121
77.31448
0.060277
88.42426
0.085027
95.37787
0.099647
98.9834
0.119407
103.4594
0.139392
107.7212
0.159527
111.8166
0.179591
115.7819
0.199908
119.7255
0.244772
128.4186
0.30143
139.8411
0.352563
150.9898
0.401041
162.4774
0.451504
175.2858
0.499529
188.9161
0.54986
205.15
0.599509
223.9598
0.649766
246.7072
0.699617
274.2414
0.749635
307.6294
0.798838
342.9726
0.827138
359.2642
0.851673
369.5842
0.87492
377.3806
0.899269
385.5834
0.923524
395.2019
0.949459
407.7845
0.973596
423.4444
0.982216
430.8404
0.990347
439.6403
0.995144
447.0302
Analysis Adsorptive :N2
Analysis Bath Temp. :77.267 K
Thermal Correction :No
Warm Free Space:24.2568 cm³
Equilibration Interval :10 s
Low Pressure Dose :None
SIO2 - Desorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.995144
0.982884
0.973902
0.954929
0.923809
0.903036
0.876876
0.851088
0.825631
0.80085
0.753437
0.698762
0.648864
0.599359
0.545728
0.493925
0.444302
0.391842
0.35491
0.304031
0.250151
0.202862
0.141296
0.082457
447.0302
441.6817
435.8327
424.7504
410.4255
402.4593
393.4906
385.3702
378.1456
371.8051
359.6826
335.9458
288.2631
249.0841
219.7384
198.1495
176.875
160.671
151.7933
140.5161
129.5115
120.335
108.2113
94.8736
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-500.SMP
Started
:14/09/2015 7:49:03
Completed
:15/09/2015 12:19:52
Report Time
:15/09/2015 7:05:34
Sample Mass
:0.2350 g
Measured
Cold Free Space
:78.1496 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
BJH Adsorpsi Pore Size Distribution
Average Width
Incremental
(nm)
Pore Volume
(cm³/g)
241.5124
0.011962
131.2857
0.014456
86.07397
0.012325
47.19616
0.027084
30.48069
0.022348
22.51849
0.017503
17.88811
0.015253
14.89033
0.014927
12.71739
0.020616
10.92915
0.033965
8.971182
0.076954
7.351761
0.074439
6.19349
0.061841
5.320021
0.050954
4.638948
0.041734
4.086112
0.035402
3.636084
0.029131
3.248448
0.026643
2.912799
0.023441
2.61055
0.021619
2.31399
0.020322
2.066639
0.013877
1.920981
0.005824
1.826106
0.005632
1.731899
0.005578
Analysis Adsorptive :N2
Analysis Bath Temp. :77.267 K
Thermal Correction :No
Warm Free Space:24.2568 cm³
Equilibration Interval :10 s
Low Pressure Dose :None
Cumulative Pore
Volume (cm³/g)
0.011962
0.026418
0.038743
0.065826
0.088175
0.105677
0.12093
0.135856
0.156473
0.190437
0.267391
0.34183
0.40367
0.454625
0.496359
0.531761
0.560891
0.587534
0.610976
0.632595
0.652917
0.666794
0.672619
0.678251
0.683828
Incremental
Pore Area
(m²/g)
0.198112
0.440457
0.572744
2.29542
2.93279
3.109012
3.410657
4.009717
6.484402
12.43087
34.31147
40.50128
39.93912
38.31148
35.98591
34.65559
32.04615
32.80706
32.19082
33.12584
35.12972
26.85922
12.1276
12.33686
12.88226
Cumulative Pore
Area (m²/g)
0.198112
0.638569
1.211312
3.506732
6.439523
9.548535
12.95919
16.96891
23.45331
35.88418
70.19565
110.6969
150.636
188.9475
224.9334
259.589
291.6352
324.4422
356.6331
389.7589
424.8886
451.7478
463.8754
476.2123
489.0946
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-700.SMP
Started
:15/09/2015 7:45:17
Completed
:15/09/2015 7:45:01
Report Time
:15/09/2015 15:59:21
Sample Mass
:0.1900 g
Measured
Cold Free Space
:82.5904 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.01003
0.030701
0.059143
0.077235
0.099746
0.119825
0.139848
0.159961
0.180016
0.200151
0.247716
0.302264
0.35324
0.400277
0.450164
0.500676
0.550436
0.600681
0.650205
0.700004
0.749299
0.799322
0.824218
0.853217
0.878192
0.900638
0.924453
0.950535
0.975529
0.983727
0.995868
0.99711
33.17376
41.29888
47.04626
49.74762
52.61896
54.90581
57.02176
59.00787
60.90864
62.75785
67.02337
71.90316
76.73678
81.61825
87.49305
94.44343
102.8611
113.5164
127.2798
146.1564
172.947
212.4979
235.3901
261.3243
279.8934
293.9669
308.6755
326.2579
346.8893
355.5568
365.0856
377.0766
Analysis Adsorptive :N2
Analysis Bath Temp. :77.246 K
Thermal Correction :No
Warm Free Space:25.9767 cm³
Equilibration Interval:10 s
Low Pressure Dose :None
SIO2 - Desorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.99711
377.0766
0.990749
366.6811
0.974991
359.8925
0.954732
347.1838
0.924648
330.2734
0.903314
319.9489
0.876606
307.7925
0.850644
296.3747
0.826561
284.9547
0.800596
271.555
0.754026
239.8788
0.70588
193.2598
0.645881
147.1869
0.59838
125.7952
0.542133
108.663
0.506361
100.7168
0.454937
90.32428
0.398244
81.33079
0.349897
76.18548
0.303014
71.68985
0.25045
66.91978
0.2004
62.40045
0.140529
56.67238
0.080557
49.75306
Universitas Sumatera Utara
File:C:\2020\DATA\ECH-700.SMP
Started
:15/09/2015 7:45:17
Analysis Adsorptive :N2
Completed
:15/09/2015 7:45:01
Analysis Bath Temp. :77.246 K
Report Time
:15/09/2015 15:59:21
Thermal Correction :No
Sample Mass
:0.1900 g
Warm Free Space:25.9767 cm³
Measured
Cold Free Space
:82.5904 cm³
Equilibration Interval:10 s
Ambient Temperature :22.00 °C
Low Pressure Dose :None
Automatic Degas
:Yes
BJH Adsorpsi Pore Size Distribution
Average Width Incremental Cumulative
Incremental
Cumulative
(nm)
Pore
Pore Volume Pore Area
Pore Area
Volume
(cm³/g)
(m²/g)
(m²/g)
(cm³/g)
141.5333
0.015513
0.015513
0.438413
0.438413
92.98003
0.014412
0.029925
0.620006
1.058419
48.35907
0.035692
0.065617
2.952274
4.010694
30.88384
0.031292
0.096909
4.052921
8.063615
22.79387
0.026922
0.123832
4.724484
12.7881
18.26394
0.026504
0.150335
5.804584
18.59268
15.11038
0.036219
0.186554
9.587778
28.18046
12.61127
0.052369
0.238923
16.61011
44.79057
10.85712
0.047236
0.286159
17.40276
62.19333
8.950387
0.083339
0.369498
37.24499
99.43832
7.335724
0.05581
0.425308
30.43203
129.8703
6.182685
0.038072
0.46338
24.63124
154.5016
5.314385
0.026428
0.489808
19.89184
174.3934
4.62974
0.019116
0.508924
16.51546
190.9089
4.076148
0.013893
0.522817
13.63391
204.5428
3.614106
0.010194
0.533012
11.28286
215.8256
3.222058
0.007631
0.540643
9.473602
225.2993
2.89425
0.005468
0.546111
7.55729
232.8565
2.595811
0.004645
0.550756
7.157657
240.0142
2.306052
0.003955
0.554711
6.860396
246.8746
2.053673
0.003171
0.557882
6.175536
253.0501
1.903453
0.001296
0.559178
2.723497
255.7736
1.808967
0.001331
0.560509
2.943559
258.7172
1.71484
0.001387
0.561896
3.234707
261.9519
Universitas Sumatera Utara
C:\2020\DATA\ECH-900.SMP
Started
:15/09/2015 16:11:00
Completed
:16/09/2015 18:10:54
Report Time
:16/09/2015 7:24:10
Sample Mass
:0.2800 g
Measured
Cold Free Space
:81.7593 cm³
Ambient Temperature :22.00 °C
Automatic Degas
:Yes
Isotherm Linear Plot
SIO2 - Adsorption
Relative Pressure
Quantity
(p/p°)
Adsorbed (cm³/g
STP)
0.011152
4.100603
0.032029
5.071684
0.066855
5.87981
0.079617
6.103362
0.099913
6.417791
0.12014
6.698195
0.14016
6.948123
0.159785
7.185942
0.179766
7.411308
0.199764
7.622845
0.249174
8.146273
0.300558
8.657114
0.350732
9.149714
0.399955
9.650325
0.449983
10.16782
0.499896
10.71215
0.549758
11.2977
0.599717
11.96249
0.649733
12.71752
0.699569
13.60701
0.749363
14.71981
0.799028
16.24785
0.8199
17.13452
0.849209
18.81537
0.873644
20.97894
0.89775
24.63322
0.920585
31.57259
0.951204
54.36078
0.966926
76.4219
0.974181
90.53974
0.986767
118.3726
0.992431
129.2093
Analysis Adsorptive :N2
Analysis Bath Temp. :77.240 K
Thermal Correction :No
Warm Free Space:25.7123 cm³
Equilibration Interval :10 s
Low Pressure Dose :None
SIO2 – Desorption
Relative Pressure
Quantity Adsorbed
(p/p°)
(cm³/g STP)
0.992431
0.97934
0.968998
0.949829
0.924251
0.896586
0.873598
0.851785
0.825828
0.803495
0.75321
0.703263
0.652541
0.600763
0.550276
0.500752
0.450517
0.400596
0.350619
0.300693
0.250717
0.200754
0.121173
0.069055
129.2093
125.7058
120.2861
100.3231
66.78152
45.82331
34.02169
26.41426
21.25293
18.64492
15.51915
13.86915
12.72316
11.83561
11.11288
10.4865
9.880975
9.355215
8.850689
8.3513
7.857176
7.335342
6.405588
5.615526
Universitas Sumatera Utara
:\2020\DATA\ECH-900.SMP
Started
:15/09/2015 16:11:00
Analysis Adsorptive :N2
Completed
:16/09/2015 18:10:54
Analysis Bath Temp. :77.240 K
Report Time
:16/09/2015 7:24:10
Thermal Correction :No
Sample Mass
:0.2800 g
Warm Free Space:25.7123 cm³
Measured
Cold Free Space
:81.7593 cm³
Equilibration Interval :10 s
Ambient Temperature :22.00 °C
Low Pressure Dose :None
Automatic Degas
:Yes
BJH Adsorpsi Pore Size Distribution
Average Width
Incremental
Cumulative
Incremental Cumulative
(nm)
Pore Volume
Pore
Pore Area
Pore Area
(cm³/g)
Volume
(m²/g)
(m²/g)
(cm³/g)
174.7332
0.017745
0.017745
0.406223
0.406223
91.45912
0.046732
0.064477
2.043855
2.450079
66.45846
0.023946
0.088423
1.441247
3.891326
47.1301
0.038092
0.126515
3.232898
7.124223
29.80583
0.040201
0.166716
5.395082
12.51931
22.1008
0.011712
0.178428
2.119677
14.63898
17.73901
0.005699
0.184127
1.285189
15.92417
14.73903
0.00304
0.187168
0.825129
16.7493
12.37407
0.002098
0.189266
0.67832
17.42762
10.81869
0.001001
0.190267
0.370234
17.79785
9.023031
0.001531
0.191798
0.678489
18.47634
7.404204
0.000992
0.19279
0.53604
19.01238
6.248743
0.000751
0.193541
0.480672
19.49306
5.377764
0.000629
0.19417
0.467916
19.96097
4.69523
0.000564
0.194734
0.480729
20.4417
4.143906
0.000479
0.195213
0.461941
20.90364
3.685714
0.000466
0.195679
0.505241
21.40888
3.295303
0.000467
0.196145
0.566521
21.9754
2.959044
0.000498
0.196643
0.673371
22.64878
2.65944
0.000488
0.197132
0.734184
23.38296
2.382578
0.000543
0.197674
0.911445
24.2944
2.130333
0.000632
0.198307
1.186851
25.48125
1.977156
0.000229
0.198536
0.463676
25.94493
1.88316
0.000271
0.198807
0.576608
26.52154
1.790484
0.000314
0.199121
0.700486
27.22202
Universitas Sumatera Utara