Lampiran 4 Analisis pH, kekentalan viskositas kekentalan gel terbaik dan kadar air pH
Ulangan 1 Ulangan 2
Sampel Uji 1 2 1 2
Rata-rata SD AMDK 6.52
6.52 6.51
6.50 6.5125
0.0096 Aquades 6.25
6.24 6.24
6.24 6.2425
0.0050 Gel terbaik
4.68 4.68
4.69 4.68
4.6825 0.005
EDTA 0.028 M 10.99
10.99 11.00
11.00 10.995
0.0058 Gel + EDTA 0.028 M 20
10.25 10.26
10.26 10.26
10.26 0.0058
Nilai viskositas dari gel terbaik Brookfield
Gel terbaik 1 : 15 Sentipoise cP
Rata-rata Ulangan I
70 x 50 71 x 50
70.5 x 50 Ulangan II
73 x 50 72 x50
72.5 x 50
Kadar air gel segar
NO UL
Cawan Cawan + Spl
Berat sampel BERAT
SELISIH KA Kosong g
g B. AWAL
g g
B. AKHIR g
bb U1
1 23.7654 29.6085
5.8431 23.8355 0.0701 98.8002 2
17.6146 22.4246 4.8100 17.6709 0.0563 98.8295
U2 1
19.7665 25.4113 5.6448 19.8441 0.0776 98.6252
2 18.1905 22.1345
3.944 18.2397 0.0492 98.7525
Rata-rata 98.7519
SD 0.0901
Lampiran 5 Kehilangan berat gel selama 5 jam disimpan pada suhu kamar 25
o
C Berat
Awal Berat Akhir
Kehilangan Massa Selama 5 jam penyimpanan
Ulangan g g 1 2 3 4 5
1 11.2843 11.0608
1.9806 2 11.3473
11.1318 1.8991
1 12.0092 11.7805
1.9044 2 10.8247
10.6293 1.8051
Rata-rata 1.8973
sd 0.0622
1 11.6960 10.6911
8.5918 2 11.6610
10.7594 7.7318
1 12.3024 11.3188
7.9952 2 11.4975
10.4762 8.8828
Rata-rata 8.3004
sd 0.5293
1 12.0116 10.3359
13.9507 2 11.8935
10.3934 12.6128
1 11.9363 10.3224
13.5209 2 12.0501
10.4270 13.4696
Rata-rata 13.3885
sd 0.5603
1 12.0110 9.7250
19.0326 2 12.1247
9.9328 18.0780
1 12.1488 9.8323
19.0677 2 11.492
9.3404 18.7226
Rata-rata 18.7252
sd 0.4585
1 11.3266 8.8209
22.1223 2 11.4825
8.7495 23.8014
1 11.6042 8.9674
22.7228 2 11.7475
8.9763 23.5897
Rata-rata 23.0591
sd 0.7796
Lampiran 6 Kehilangan berat gel selama 5 jam disimpan pada suhu rendah8
o
C Berat
Awal Berat Akhir
Kehilangan Massa Selama 5 jam penyimpanan
Ulangan g g 1 2 3 4 5
1 12.2965 10.7715
12.4019 2 11.6996
10.2294 12.5662
1 11.9018 10.3856
12.7392 2 12.7534
11.1257 12.7628
Rata-rata 12.6175
sd 0.1683
1 11.5748
17.2967 16.9592 2
10.9839 16.5194 17.8880
1 11.6578
17.2087 16.8402 2
11.9777 17.5212 17.6144
Rata-rata 17.3254
sd 0.5054
1 11.3978 16.7162
20.5451 2 11.4893
16.5897 20.8533
1 12.3653 17.2345
21.2206 2 12.3961
17.2628 21.0800
Rata-rata 20.9248
sd 0.2948
1 11.9693 15.8154
31.2658 2 11.8407
15.8259 30.2186
1 11.9906 15.9525
30.8183 2 10.8131
15.0249 29.5752
Rata-rata 30.4695
sd 0.7344
1 11.7870 14.0555
44.9121 2 12.2829
14.4259 44.4194
1 12.6921 14.5324
45.3534 2 11.1564
13.6377 45.7979
Rata-rata 45.1207
sd 0.5910
Lampiran 7 Komposisi Kimia Gel Segar
BB AIR
SERAT Mg
Ca KLOROFIL
FENOL KAP. AN
TIOK KH
UL Total
Larut Tidak
Total a
b mMmg
1 98.8003 1.1453
0.7495 0.3958 0.0034 0.0066 0.0015 0.0008
0.0007 0.0324
0.0031
1.1997
2 98.6253 1.1274
0.7321 0.3953 0.0034 0.0068 0.0015 0.0007
0.0007 0.0324
0.0031
1.3747
1 98.8295 1.1151
0.7201 0.3950 0.0037 0.0068 0.0014 0.0009
0.0007 0.0336
0.0032
1.1705
2 98.7525 1.1360
0.7412 0.3948 0.0036 0.0068 0.0014 0.0008
0.0007 0.0336
0.0030
1.2475
RATA-RATA 98.7519 1.1310
0.7357 0.3952
0.0035 0.0068
0.0015 0.0008 0.0007
0.0330
0.0031
1.2481
SD 0.0902 0.0128
0.0126 0.0004
0.0002 0.0001
0.0001 0.0001 0.0000
0.0007
0.0001
0.0902
34.1527 66.4777
14.6669 7.5867
7.0847 32.4440
33.5287 68.2488
14.6484 7.4834
7.1695 32.4440
36.6142 68.1732
14.4641 7.5263
6.9423 33.6595
35.5232 68.1732
14.4752 7.5123
6.9673 33.6595
mgKg mgKg mgKg mgKg
mgKg mg100g
RATA-RATA 34.9547 67.7682 14.5637
7.5272 7.0410
33.0518 SD
1.3849 0.8611
0.1089 0.0435
0.1058 0.7018
BASIS KERING AIR
SERAT Mg
Ca KLOROFIL
FENOL KAP.
ANTIOK UL
Total Larut
Tidak Total
a b
Mmmg
1 0.0000 91.7621
60.0504 31.7117 0.2736 0.5326 0.1175
0.0608 0.0568
2.5995
0.2487
2 0.0000 90.3327
58.6604 31.6723 0.2686 0.5468 0.1174
0.0600 0.0574
2.5995
0.2446
1 0.0000 89.3467
57.6977 31.6490 0.2934 0.5462 0.1159
0.0603 0.0556
2.6968
0.2547
2 0.0000 91.0205
59.3887 31.6318 0.2846 0.5462 0.1160
0.0602 0.0558
2.6968
0.2392
RATA-RATA 0.0000
90.6155 58.9493
31.6662 0.2801 0.5430 0.1167 0.0603
0.0564 2.6482
0.2468
SD 0.0000 1.0277
1.0092 0.0346
0.0111 0.0069
0.0009 0.0003 0.0008
0.0562
0.0065
90.6155 2736.3748
5326.3148 1175.1386
607.8591 567.6410
2599.4683 2686.3783
5468.2131 1173.6563
599.5846 574.4347
2599.4683 2933.5941
5462.1579 1158.8886
603.0182 556.2257
2696.8566 2846.1807
5462.1579 1159.7754
601.8976 558.2338
2696.8566
mgKg mgKg mgKg mgKg
mgKg mg100g
RATA-RATA 2800.6320 5429.7109 1166.8647
603.0899 564.1338
2648.1625
SD 110.9602 68.9898 8.7266 3.4861
8.4805 56.2272
Lampiran 8 Rendemen bubuk gel, KPG dan kadar air Rendemen bubuk gel
Berat daun Pelarut + Daun
Gel W kering rendemen rendemen
Sampel Daun segar
Segar g ml
ml K.A 8
dr daun dr gel
U1 1 25.0
400 302
2.9526 11.8106
0.9777 2
25.2 400
304 2.9582
11.7389 0.9731
U2 1 25.0
400 310
2.8797 11.5189
0.9289 2
25.3 400
312 2.8482
11.2579 0.9129
Rata-rata 11.6437 0.9481
SD 0.2489 0.0321
Rendemen komponen pembentuk gel KPG Dalam 500 g gel segar
Dalam 100 g gel segar Gel g
Berat KPG g KA 6.6408
KPG bk g Gel
W KPG KA 6.6408
KPG bk 502.00 5.981 0.3971
5.5838 100.40 1.1962 0.0794 1.1167 504.00 5.997 0.3982
5.5987 100.80 1.1994 0.0796 1.1197 501.00 5.962 0.3959
5.5660 100.20 1.1924 0.0791 1.1132 501.00 6.033 0.4006
5.6323 100.20 1.2066 0.0801 1.1264
Rata-Rata 5.9932 0.3979 5.5952 Rata-Rata 1.1986 0.0796 1.1190
SD 0.0301 0.0019
0.0281 SD 0.0060 0.0004 0.0056
Kadar air bubuk gel setelah freeze dryer
NO UL
Cawan Cawan + Spl
Berat sampel BERAT
SELISIH KA
Kosong g g
B. AWAL g
