Formulasi dan Uji Efek Anti-Aging Sediaan Masker Sheet yang Mengandung Vitamin B3
Lampiran 1. Sertifikat analisis niasinamida
57
Universitas Sumatera Utara
Lampiran 2. Gambar bahan dan alat
A
B
C
Keterangan:
A. Vitamin B3 (niasinamida)
B. Viskometer Brookfield
C. pH meter
58
Universitas Sumatera Utara
Lampiran 2. (Lanjutan)
D
E
F
Keterangan:
D. Neraca analitik
E. Skin analyzer
F. Moisture checker
59
Universitas Sumatera Utara
Lampiran 2. (Lanjutan)
G
H
I
Keterangan:
G. Lembaran masker sheet
H. Foil bag
I. Alat penyegel
60
Universitas Sumatera Utara
Lampiran 3. Bagan pembuatan essence masker sheet blanko
Nipagin
Natrium Poliakrilat
← Ditambahkan butilen
glikol dan gliserin
hingga
← Digerus
homogen
← Dilarutkan dalam air
panas
← Diaduk hingga homogen
Campuran I
Larutan Nipagin
← Dicampur perlahan-lahan larutan
nipagin ke dalam campuran I
← Digerus homogen
Campuran II
← Ditambahkan PEG-40 HCO
← Digerus homogen
← Ditambahkan etanol dan parfum
← Digerus homogen
Essence Masker Sheet Blanko
61
Universitas Sumatera Utara
Lampiran 4. Bagan pembuatan essence masker sheet vitamin B3
Natrium Poliakrilat
Nipagin
← Dilarutkan dalam air
panas
← Diaduk hingga homogen
← Ditambahkan butilen
glikol dan gliserin
← Digerus
hingga
homogen
Campuran I
Larutan Nipagin
← Dicampur perlahan-lahan larutan
nipagin ke dalam campuran I
← Digerus homogen
Campuran II
Vitamin B3
← Ditambahkan
dengan
PEG-40 HCO
← Ditambahkan air suling
← Diaduk homogen
Campuran III
← Ditambahkan campuran III ke dalam
campuran II
← Digerus homogen
← Ditambahkan etanol dan parfum
← Digerus homogen
Essence Masker Sheet Vitamin B3
62
Universitas Sumatera Utara
Lampiran 5. Surat pernyataan persetujuan (informed consent)
63
Universitas Sumatera Utara
Lampiran 6. Gambar essence sediaan masker sheet
F0
F1
F3
F2
A
F0
F1
F2
F3
B
Keterangan:
A : Pada awal pembuatan
B : Setelah penyimpanan 12 minggu
F0 : Masker sheet formula blanko
F1 : Masker sheet formula I (konsentrasi vitamin B3 1%)
F2 : Masker sheet formula II (konsentrasi vitamin B3 3%)
F3 : Masker sheet formula III (konsentrasi vitamin B3 5%)
64
Universitas Sumatera Utara
Lampiran 7.Proses pengemasan masker sheet
65
Universitas Sumatera Utara
Lampiran 8.Pengujian masker sheetpada sukarelawan
B
A
Keterangan:
A. Uji iritasi
B. Aplikasi masker sheet pada sukarelawan
66
Universitas Sumatera Utara
Lampiran 9. Lampiran skin analyzer
− Kadar air (moisture)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
Perawatan minggu ke-3
Perawatan minggu ke-4
67
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
− Kehalusan/pori (evenness/pore)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
68
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
Perawatan minggu ke-3
Perawatan minggu-4
69
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
− Noda (spot)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
70
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
Perawatan minggu ke-3
Perawatan minggu ke-4
71
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
− Keriput (wrinkle)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
72
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
Perawatan minggu ke-3
Perawatan minggu ke-4
73
Universitas Sumatera Utara
Lampiran 10. Data hasil uji statistik
− Kadar air (Moisture)
1. Uji Normalitas
b,c,d,e
Tests of Normality
Formula
Kondisi Awal
F1
a
Kolmogorov-Smirnov
Statistic
.385
df
Shapiro-Wilk
3
Sig.
.
Statistic
.750
df
3
Sig.
.000
F2
F3
BLANKO
F1
F2
F3
F1
.385
.385
.385
.385
.175
.385
.385
3
3
3
3
3
3
3
.
.
.
.
.
.
.
.750
.750
.750
.750
1.000
.750
.750
3
3
3
3
3
3
3
.000
.000
.000
.000
1.000
.000
.000
F2
F3
BLANKO
F1
F2
F3
F2
.385
.385
.385
.385
.385
.175
.385
3
3
3
3
3
3
3
.
.
.
.
.
.
.
.750
.750
.750
.750
.750
1.000
.750
3
3
3
3
3
3
3
.000
.000
.000
.000
.000
1.000
.000
F3
.175
3
.
1.000
a. Lilliefors Significance Correction
b. Kondisi Awal is constant when Formula = BLANKO. It has been omitted.
c. Moisture M2 is constant when Formula = BLANKO. It has been omitted.
d. Moisture M4 is constant when Formula = BLANKO. It has been omitted.
e. Moisture M4 is constant when Formula = F1. It has been omitted.
3
1.000
Moisture M1
Moisture M2
Moisture M3
Moisture M4
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
Kondisi Awal
6.381
df
Asymp. Sig.
Moisture M1
9.339
Moisture M2
9.954
Moisture M3
10.311
Moisture M4
10.722
3
3
3
3
3
.094
.025
.019
.016
.013
a. Kruskal Wallis Test
b. Grouping Variable: Formula
74
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Mann-Whitney U
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
1.500
.000
.000
.000
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
7.500
-1.581
.114
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
.200
a
6.000
-2.023
.043
.100
6.000
-2.121
.034
a
.100
a
6.000
-2.023
.043
.100
a
6.000
-2.236
.025
.100
a
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Kondisi Awal Moisture M1 Moisture M2 Moisture M3
1.500
.000
.000
.000
7.500
6.000
6.000
6.000
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
-1.581
.114
a
.200
-1.993
.046
a
.100
-2.121
.034
a
.100
-2.023
.043
a
.100
Moisture
M4
.000
6.000
-2.121
.034
a
.100
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
.000
.000
.000
.000
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
6.000
6.000
6.000
6.000
6.000
-2.121
-2.023
-2.121
-1.993
-2.087
.034
.100
a
.043
.100
a
.034
.100
a
.046
.100
a
.037
.100
a
b. Grouping Variable: Formula
75
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
4.500
2.500
2.000
.000
.000
10.500
8.500
8.000
6.000
6.000
.000
-.943
-1.291
-2.023
-2.121
1.000
.346
.197
.043
.034
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
1.000
a
.400
a
.400
a
.100
a
.100
a
F1 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
2.000
.000
.000
.000
.000
8.000
6.000
6.000
6.000
6.000
-1.291
-2.023
-2.023
-1.993
-2.087
.197
.043
.043
.046
.037
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
.400
a
.100
a
.100
a
.100
a
.100
a
F2 dengan F3
b
Test Statistics
Mann-Whitney U
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
2.000
1.000
.500
.500
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
8.000
7.000
6.500
6.500
6.000
-1.291
-1.623
-1.826
-1.798
-1.993
.197
.105
.068
.072
.046
a
a
a
a
.400
.200
.100
.100
.100
a
b. Grouping Variable: Formula
76
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Kehalusan (Evenness)
1. Uji Normalitas
b
Tests of Normality
Formula
a
Kolmogorov-Smirnov
Kondisi Awal
BLANKO
Statistic
.196
Evenness M1
F1
F2
F3
BLANKO
Evenness M2
3
Sig.
.878
.750
1.000
.964
.996
3
3
3
3
.000
1.000
.637
.878
.
.
.
.
.964
.750
.893
.893
3
3
3
3
.637
.000
.363
.363
.
.
.
.
.
.
.
.750
.964
.750
.996
.964
.750
.923
3
3
3
3
3
3
3
.000
.637
.000
.878
.637
.000
.463
F1
.175
3
.
1.000
F2
.385
3
.
.750
F3
.385
3
.
.750
a. Lilliefors Significance Correction
b. Evenness M3 is constant when Formula = F1. It has been omitted.
3
3
3
1.000
.000
.000
Evenness M3
Evenness M4
df
Shapiro-Wilk
3
Sig.
.
Statistic
.996
.385
.175
.253
.196
3
3
3
3
.
.
.
.
F1
F2
F3
BLANKO
.253
.385
.314
.314
3
3
3
3
F1
F2
F3
BLANKO
F2
F3
BLANKO
.385
.253
.385
.196
.253
.385
.292
3
3
3
3
3
3
3
df
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
2.591
3.824
4.258
7.859
10.077
df
Asymp. Sig.
3
3
3
3
3
.459
.281
.235
.049
.018
a. Kruskal Wallis Test
b. Grouping Variable: Formula
77
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
3.000
4.000
3.500
3.000
.500
Wilcoxon W
9.000
10.000
9.500
9.000
6.500
Z
-.664
-.218
-.471
-.696
-1.771
Asymp. Sig. (2-tailed)
.507
.827
.637
.487
.077
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
1.000
.700
.700
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
3.000
3.000
2.500
1.000
.000
Wilcoxon W
9.000
9.000
8.500
7.000
6.000
Z
-.674
-.664
-.886
-1.528
-1.993
Asymp. Sig. (2-tailed)
.500
.507
.376
.127
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
.700
.400
.200
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F3
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
4.500
2.500
1.000
.000
.000
Wilcoxon W
10.500
8.500
7.000
6.000
6.000
Z
.000
-.886
-1.550
-1.993
-1.993
Asymp. Sig. (2-tailed)
1.000
.376
.121
.046
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
1.000
.400
.200
.100
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
78
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
3.500
3.500
3.000
1.500
.500
Wilcoxon W
9.500
9.500
9.000
7.500
6.500
Z
-.449
-.471
-.696
-1.549
-1.798
Asymp. Sig. (2-tailed)
.653
.637
.487
.121
.072
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
.700
.700
.200
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
1.000
1.500
1.000
.000
.000
Wilcoxon W
7.000
7.500
7.000
6.000
6.000
Z
-1.623
-1.328
-1.573
-2.121
-1.993
Asymp. Sig. (2-tailed)
.105
.184
.116
.034
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
.200
.200
.200
.100
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
1.500
.000
1.500
1.000
.000
7.500
6.000
7.500
7.000
6.000
-1.328
-1.993
-1.348
-1.623
-2.023
.184
.046
.178
.105
.043
a
a
a
a
a
.200
.100
.200
.200
.100
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
79
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Pori (Pore)
1. Uji Normalitas
b
Tests of Normality
Formula
a
Kolmogorov-Smirnov
Kondisi Awal
BLANKO
Statistic
.175
Pori M1
F1
F3
BLANKO
df
Shapiro-Wilk
3
Sig.
.
Statistic
1.000
.175
.385
.304
3
3
3
.
.
.
Pori M2
F1
F2
F3
BLANKO
.385
.385
.385
.253
3
3
3
3
Pori M3
F1
F2
F3
BLANKO
.175
.385
.385
.253
Pori M4
F1
F2
F3
BLANKO
df
3
Sig.
1.000
1.000
.750
.907
3
3
3
1.000
.000
.407
.
.
.
.
.750
.750
.750
.964
3
3
3
3
.000
.000
.000
.637
3
3
3
3
.
.
.
.
1.000
.750
.750
.964
3
3
3
3
1.000
.000
.000
.637
.385
.385
.385
.304
3
3
3
3
.
.
.
.
.750
.750
.750
.907
3
3
3
3
.000
.000
.000
.407
F1
.385
F2
.385
F3
.385
a. Lilliefors Significance Correction
3
3
3
.
.
.
.750
.750
.750
3
3
3
.000
.000
.000
b. Kondisi Awal is constant when Formula = F2. It has been omitted.
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
df
Asymp. Sig.
Kondisi Awal
.689
3
.876
Pori M1
3.089
3
.378
Pori M2
8.145
3
.043
Pori M3
10.001
3
.019
Pori M4
10.188
3
.017
a. Kruskal Wallis Test
b. Grouping Variable: Formula
80
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
4.500
10.500
.000
1.000
a
1.000
Pori M1
4.000
10.000
-.232
.817
a
1.000
Pori M2
3.000
9.000
-.674
.500
a
.700
Pori M3
1.000
7.000
-1.623
.105
a
.200
Pori M4
1.000
7.000
-1.623
.105
a
.200
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Kondisi Awal
4.500
Pori M1
3.500
Pori M2
1.000
Pori M3
.000
Pori M4
.000
Wilcoxon W
Z
10.500
.000
9.500
-.471
7.000
-1.623
6.000
-1.993
6.000
-1.993
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
1.000
a
1.000
.637
a
.700
.105
a
.200
.046
a
.100
.046
a
.100
Mann-Whitney U
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
3.500
Pori M1
2.500
Pori M2
.000
Pori M3
.000
Pori M4
.000
9.500
-.471
8.500
-.943
6.000
-1.993
6.000
-1.993
6.000
-1.993
.637
.700
.346
a
.400
a
.046
.100
a
.046
.100
a
.046
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
81
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
4.500
10.500
.000
1.000
a
1.000
Pori M1
2.000
8.000
-1.291
.197
a
.400
Pori M2
1.000
7.000
-1.623
.105
a
.200
Pori M3
.000
6.000
-2.023
.043
a
.100
Pori M4
.000
6.000
-2.023
.043
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
3.000
9.000
-.696
Pori M1
1.000
7.000
-1.650
Pori M2
.000
6.000
-1.993
Pori M3
.000
6.000
-2.023
Pori M4
.000
6.000
-2.023
.487
a
.700
.099
a
.200
.046
a
.100
.043
a
.100
.043
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
3.000
9.000
Pori M1
3.000
9.000
Pori M2
1.000
7.000
Pori M3
.500
6.500
Pori M4
.000
6.000
-1.000
.317
-.745
.456
-1.650
.099
-1.826
.068
-2.023
.043
.700
a
.700
a
.200
a
.100
a
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
82
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Noda (Spot)
1. Uji Normalitas
b
Tests of Normality
Formula
a
Kolmogorov-Smirnov
Kondisi Awal
BLANKO
Statistic
.385
Spot M1
F1
F2
F3
BLANKO
3
.
Statistic
.750
.253
.385
.385
.385
3
3
3
3
.
.
.
.
Spot M3
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
.253
.385
.385
.314
.292
.385
.385
.276
3
3
3
3
3
3
3
3
Spot M4
F1
F2
F3
BLANKO
.175
.385
.175
.314
3
3
3
3
Spot M2
df
Shapiro-Wilk
Sig.
3
Sig.
.000
.964
.750
.750
.750
3
3
3
3
.637
.000
.000
.000
.
.
.
.
.
.
.
.
.964
.750
.750
.893
.923
.750
.750
.942
3
3
3
3
3
3
3
3
.637
.000
.000
.363
.463
.000
.000
.537
.
.
.
.
1.000
.750
1.000
.893
3
3
3
3
1.000
.000
1.000
.363
.750
.750
3
3
.000
.000
F1
.385
3
.
F3
.385
3
.
a. Lilliefors Significance Correction
b. Spot M4 is constant when Formula = F2. It has been omitted.
df
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
df
Kondisi Awal
6.070
3
Spot M1
2.852
3
Spot M2
7.159
3
Spot M3
9.562
3
Spot M4
10.607
3
.108
.415
.067
.023
.014
Asymp. Sig.
a. Kruskal Wallis Test
b. Grouping Variable: Formula
83
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
2.500
8.500
-.899
.369
a
.400
Spot M1
3.000
9.000
-.664
.507
a
.700
Spot M2
2.500
8.500
-.886
.376
a
.400
Spot M3
3.000
9.000
-.674
.500
a
.700
Spot M4
.000
6.000
-1.993
.046
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Spot Sebelum
.500
Spot M1
3.000
Spot M2
2.500
Spot M3
.000
Spot M4
.000
6.500
-1.826
9.000
-.674
8.500
-.943
6.000
-1.993
6.000
-2.087
.068
a
.100
.500
a
.700
.346
a
.400
.046
a
.100
.037
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
1.000
Spot M1
3.000
Spot M2
.000
Spot M3
.000
Spot M4
.000
7.000
-1.573
9.000
-.674
6.000
-1.993
6.000
-1.964
6.000
-1.993
.116
.200
.500
a
.700
a
.046
.100
a
.050
.100
a
.046
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
84
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
.500
6.500
-1.798
.072
a
.100
Spot M1
2.000
8.000
-1.107
.268
a
.400
Spot M2
4.000
10.000
-.232
.817
a
1.000
Spot M3
.000
6.000
-1.993
.046
a
.100
Spot M4
.000
6.000
-2.121
.034
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
1.500
7.500
-1.348
Spot M1
3.500
9.500
-.471
Spot M2
.000
6.000
-1.993
Spot M3
.000
6.000
-1.964
Spot M4
.000
6.000
-2.023
.178
a
.200
.637
a
.700
.046
a
.100
.050
a
.100
.043
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
4.000
10.000
Spot M1
.000
6.000
Spot M2
.000
6.000
Spot M3
.000
6.000
Spot M4
.000
6.000
-.258
.796
-2.023
.043
-2.023
.043
-1.993
.046
-2.121
.034
1.000
a
.100
a
.100
a
.100
a
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
85
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Keriput (Wrinkle)
1. Uji Normalitas
Tests of Normality
Formula
a
Kolmogorov-Smirnov
3
.
Statistic
.976
.253
.175
.175
.211
.219
.253
.175
.187
.328
.385
.219
.219
.385
.385
.356
.204
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
F1
.385
F2
.385
F3
.175
a. Lilliefors Significance Correction
3
3
3
.
.
.
Kondisi Awal
Keriput M1
Keriput M2
Keriput M3
Keriput M4
BLANKO
Statistic
.238
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
df
Shapiro-Wilk
Sig.
df
3
Sig.
.702
.964
1.000
1.000
.991
.987
.964
1.000
.998
.871
.750
.987
.987
.750
.750
.818
.993
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
.637
1.000
1.000
.817
.780
.637
1.000
.915
.298
.000
.780
.780
.000
.000
.157
.843
.750
.750
1.000
3
3
3
.000
.000
1.000
Keriput M3
6.621
3
.085
Keriput M4
7.887
3
.048
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
df
Asymp. Sig.
Kondisi Awal
1.872
3
.599
Keriput M1
4.033
3
.258
Keriput M2
4.587
3
.205
a. Kruskal Wallis Test
b. Grouping Variable: Formula
86
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
Mann-Whitney U
2.000
2.000
3.500
4.000
3.000
Wilcoxon W
8.000
8.000
9.500
10.000
9.000
Z
-1.091
-1.091
-.443
-.221
-.664
Asymp. Sig. (2-tailed)
.275
.275
.658
.825
.507
a
a
a
a
a
Exact Sig. [2*(1-tailed
.400
.400
.700
1.000
.700
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
2.500
3.000
4.000
2.500
2.000
8.500
9.000
10.000
8.500
8.000
-.886
-.655
-.221
-.899
-1.159
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
.376
a
.400
.513
a
.700
.825
a
1.000
.369
a
.400
.246
a
.400
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
3.000
4.500
2.500
.000
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
9.000
-.655
.513
a
.700
10.500
.000
1.000
a
1.000
8.500
-.886
.376
a
.400
6.000
-1.964
.050
a
.100
6.000
-1.964
.050
a
.100
87
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
3.000
4.000
1.500
4.000
1.000
9.000
10.000
7.500
10.000
7.000
-.655
-.225
-1.348
-.225
-1.650
.513
.822
.178
.822
.099
a
a
a
a
a
.700
1.000
.200
1.000
.200
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
Mann-Whitney U
3.500
.500
.000
.000
.000
Wilcoxon W
9.500
6.500
6.000
6.000
6.000
Z
-.443
-1.771
-1.964
-1.993
-1.993
Asymp. Sig. (2-tailed)
.658
.077
.050
.046
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
.100
.100
.100
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
2.000
.500
1.000
.000
.000
8.000
6.500
7.000
6.000
6.000
-1.124
-1.771
-1.623
-1.993
-1.993
.261
.077
.105
.046
.046
a
a
a
a
a
.400
.100
.200
.100
.100
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
88
Universitas Sumatera Utara
57
Universitas Sumatera Utara
Lampiran 2. Gambar bahan dan alat
A
B
C
Keterangan:
A. Vitamin B3 (niasinamida)
B. Viskometer Brookfield
C. pH meter
58
Universitas Sumatera Utara
Lampiran 2. (Lanjutan)
D
E
F
Keterangan:
D. Neraca analitik
E. Skin analyzer
F. Moisture checker
59
Universitas Sumatera Utara
Lampiran 2. (Lanjutan)
G
H
I
Keterangan:
G. Lembaran masker sheet
H. Foil bag
I. Alat penyegel
60
Universitas Sumatera Utara
Lampiran 3. Bagan pembuatan essence masker sheet blanko
Nipagin
Natrium Poliakrilat
← Ditambahkan butilen
glikol dan gliserin
hingga
← Digerus
homogen
← Dilarutkan dalam air
panas
← Diaduk hingga homogen
Campuran I
Larutan Nipagin
← Dicampur perlahan-lahan larutan
nipagin ke dalam campuran I
← Digerus homogen
Campuran II
← Ditambahkan PEG-40 HCO
← Digerus homogen
← Ditambahkan etanol dan parfum
← Digerus homogen
Essence Masker Sheet Blanko
61
Universitas Sumatera Utara
Lampiran 4. Bagan pembuatan essence masker sheet vitamin B3
Natrium Poliakrilat
Nipagin
← Dilarutkan dalam air
panas
← Diaduk hingga homogen
← Ditambahkan butilen
glikol dan gliserin
← Digerus
hingga
homogen
Campuran I
Larutan Nipagin
← Dicampur perlahan-lahan larutan
nipagin ke dalam campuran I
← Digerus homogen
Campuran II
Vitamin B3
← Ditambahkan
dengan
PEG-40 HCO
← Ditambahkan air suling
← Diaduk homogen
Campuran III
← Ditambahkan campuran III ke dalam
campuran II
← Digerus homogen
← Ditambahkan etanol dan parfum
← Digerus homogen
Essence Masker Sheet Vitamin B3
62
Universitas Sumatera Utara
Lampiran 5. Surat pernyataan persetujuan (informed consent)
63
Universitas Sumatera Utara
Lampiran 6. Gambar essence sediaan masker sheet
F0
F1
F3
F2
A
F0
F1
F2
F3
B
Keterangan:
A : Pada awal pembuatan
B : Setelah penyimpanan 12 minggu
F0 : Masker sheet formula blanko
F1 : Masker sheet formula I (konsentrasi vitamin B3 1%)
F2 : Masker sheet formula II (konsentrasi vitamin B3 3%)
F3 : Masker sheet formula III (konsentrasi vitamin B3 5%)
64
Universitas Sumatera Utara
Lampiran 7.Proses pengemasan masker sheet
65
Universitas Sumatera Utara
Lampiran 8.Pengujian masker sheetpada sukarelawan
B
A
Keterangan:
A. Uji iritasi
B. Aplikasi masker sheet pada sukarelawan
66
Universitas Sumatera Utara
Lampiran 9. Lampiran skin analyzer
− Kadar air (moisture)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
Perawatan minggu ke-3
Perawatan minggu ke-4
67
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
− Kehalusan/pori (evenness/pore)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
68
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
Perawatan minggu ke-3
Perawatan minggu-4
69
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
− Noda (spot)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
70
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
Perawatan minggu ke-3
Perawatan minggu ke-4
71
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
− Keriput (wrinkle)
Kondisi awal
Perawatan minggu-1
Perawatan minggu ke-2
72
Universitas Sumatera Utara
Lampiran 9. (Lanjutan)
Perawatan minggu ke-3
Perawatan minggu ke-4
73
Universitas Sumatera Utara
Lampiran 10. Data hasil uji statistik
− Kadar air (Moisture)
1. Uji Normalitas
b,c,d,e
Tests of Normality
Formula
Kondisi Awal
F1
a
Kolmogorov-Smirnov
Statistic
.385
df
Shapiro-Wilk
3
Sig.
.
Statistic
.750
df
3
Sig.
.000
F2
F3
BLANKO
F1
F2
F3
F1
.385
.385
.385
.385
.175
.385
.385
3
3
3
3
3
3
3
.
.
.
.
.
.
.
.750
.750
.750
.750
1.000
.750
.750
3
3
3
3
3
3
3
.000
.000
.000
.000
1.000
.000
.000
F2
F3
BLANKO
F1
F2
F3
F2
.385
.385
.385
.385
.385
.175
.385
3
3
3
3
3
3
3
.
.
.
.
.
.
.
.750
.750
.750
.750
.750
1.000
.750
3
3
3
3
3
3
3
.000
.000
.000
.000
.000
1.000
.000
F3
.175
3
.
1.000
a. Lilliefors Significance Correction
b. Kondisi Awal is constant when Formula = BLANKO. It has been omitted.
c. Moisture M2 is constant when Formula = BLANKO. It has been omitted.
d. Moisture M4 is constant when Formula = BLANKO. It has been omitted.
e. Moisture M4 is constant when Formula = F1. It has been omitted.
3
1.000
Moisture M1
Moisture M2
Moisture M3
Moisture M4
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
Kondisi Awal
6.381
df
Asymp. Sig.
Moisture M1
9.339
Moisture M2
9.954
Moisture M3
10.311
Moisture M4
10.722
3
3
3
3
3
.094
.025
.019
.016
.013
a. Kruskal Wallis Test
b. Grouping Variable: Formula
74
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Mann-Whitney U
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
1.500
.000
.000
.000
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
7.500
-1.581
.114
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
.200
a
6.000
-2.023
.043
.100
6.000
-2.121
.034
a
.100
a
6.000
-2.023
.043
.100
a
6.000
-2.236
.025
.100
a
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Kondisi Awal Moisture M1 Moisture M2 Moisture M3
1.500
.000
.000
.000
7.500
6.000
6.000
6.000
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
-1.581
.114
a
.200
-1.993
.046
a
.100
-2.121
.034
a
.100
-2.023
.043
a
.100
Moisture
M4
.000
6.000
-2.121
.034
a
.100
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
.000
.000
.000
.000
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
6.000
6.000
6.000
6.000
6.000
-2.121
-2.023
-2.121
-1.993
-2.087
.034
.100
a
.043
.100
a
.034
.100
a
.046
.100
a
.037
.100
a
b. Grouping Variable: Formula
75
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
4.500
2.500
2.000
.000
.000
10.500
8.500
8.000
6.000
6.000
.000
-.943
-1.291
-2.023
-2.121
1.000
.346
.197
.043
.034
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
1.000
a
.400
a
.400
a
.100
a
.100
a
F1 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
2.000
.000
.000
.000
.000
8.000
6.000
6.000
6.000
6.000
-1.291
-2.023
-2.023
-1.993
-2.087
.197
.043
.043
.046
.037
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
.400
a
.100
a
.100
a
.100
a
.100
a
F2 dengan F3
b
Test Statistics
Mann-Whitney U
Kondisi Awal Moisture M1 Moisture M2 Moisture M3 Moisture M4
2.000
1.000
.500
.500
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
8.000
7.000
6.500
6.500
6.000
-1.291
-1.623
-1.826
-1.798
-1.993
.197
.105
.068
.072
.046
a
a
a
a
.400
.200
.100
.100
.100
a
b. Grouping Variable: Formula
76
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Kehalusan (Evenness)
1. Uji Normalitas
b
Tests of Normality
Formula
a
Kolmogorov-Smirnov
Kondisi Awal
BLANKO
Statistic
.196
Evenness M1
F1
F2
F3
BLANKO
Evenness M2
3
Sig.
.878
.750
1.000
.964
.996
3
3
3
3
.000
1.000
.637
.878
.
.
.
.
.964
.750
.893
.893
3
3
3
3
.637
.000
.363
.363
.
.
.
.
.
.
.
.750
.964
.750
.996
.964
.750
.923
3
3
3
3
3
3
3
.000
.637
.000
.878
.637
.000
.463
F1
.175
3
.
1.000
F2
.385
3
.
.750
F3
.385
3
.
.750
a. Lilliefors Significance Correction
b. Evenness M3 is constant when Formula = F1. It has been omitted.
3
3
3
1.000
.000
.000
Evenness M3
Evenness M4
df
Shapiro-Wilk
3
Sig.
.
Statistic
.996
.385
.175
.253
.196
3
3
3
3
.
.
.
.
F1
F2
F3
BLANKO
.253
.385
.314
.314
3
3
3
3
F1
F2
F3
BLANKO
F2
F3
BLANKO
.385
.253
.385
.196
.253
.385
.292
3
3
3
3
3
3
3
df
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
2.591
3.824
4.258
7.859
10.077
df
Asymp. Sig.
3
3
3
3
3
.459
.281
.235
.049
.018
a. Kruskal Wallis Test
b. Grouping Variable: Formula
77
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
3.000
4.000
3.500
3.000
.500
Wilcoxon W
9.000
10.000
9.500
9.000
6.500
Z
-.664
-.218
-.471
-.696
-1.771
Asymp. Sig. (2-tailed)
.507
.827
.637
.487
.077
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
1.000
.700
.700
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
3.000
3.000
2.500
1.000
.000
Wilcoxon W
9.000
9.000
8.500
7.000
6.000
Z
-.674
-.664
-.886
-1.528
-1.993
Asymp. Sig. (2-tailed)
.500
.507
.376
.127
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
.700
.400
.200
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F3
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
4.500
2.500
1.000
.000
.000
Wilcoxon W
10.500
8.500
7.000
6.000
6.000
Z
.000
-.886
-1.550
-1.993
-1.993
Asymp. Sig. (2-tailed)
1.000
.376
.121
.046
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
1.000
.400
.200
.100
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
78
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
3.500
3.500
3.000
1.500
.500
Wilcoxon W
9.500
9.500
9.000
7.500
6.500
Z
-.449
-.471
-.696
-1.549
-1.798
Asymp. Sig. (2-tailed)
.653
.637
.487
.121
.072
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
.700
.700
.200
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
Mann-Whitney U
1.000
1.500
1.000
.000
.000
Wilcoxon W
7.000
7.500
7.000
6.000
6.000
Z
-1.623
-1.328
-1.573
-2.121
-1.993
Asymp. Sig. (2-tailed)
.105
.184
.116
.034
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
.200
.200
.200
.100
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Kondisi Awal Evenness M1 Evenness M2 Evenness M3 Evenness M4
1.500
.000
1.500
1.000
.000
7.500
6.000
7.500
7.000
6.000
-1.328
-1.993
-1.348
-1.623
-2.023
.184
.046
.178
.105
.043
a
a
a
a
a
.200
.100
.200
.200
.100
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
79
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Pori (Pore)
1. Uji Normalitas
b
Tests of Normality
Formula
a
Kolmogorov-Smirnov
Kondisi Awal
BLANKO
Statistic
.175
Pori M1
F1
F3
BLANKO
df
Shapiro-Wilk
3
Sig.
.
Statistic
1.000
.175
.385
.304
3
3
3
.
.
.
Pori M2
F1
F2
F3
BLANKO
.385
.385
.385
.253
3
3
3
3
Pori M3
F1
F2
F3
BLANKO
.175
.385
.385
.253
Pori M4
F1
F2
F3
BLANKO
df
3
Sig.
1.000
1.000
.750
.907
3
3
3
1.000
.000
.407
.
.
.
.
.750
.750
.750
.964
3
3
3
3
.000
.000
.000
.637
3
3
3
3
.
.
.
.
1.000
.750
.750
.964
3
3
3
3
1.000
.000
.000
.637
.385
.385
.385
.304
3
3
3
3
.
.
.
.
.750
.750
.750
.907
3
3
3
3
.000
.000
.000
.407
F1
.385
F2
.385
F3
.385
a. Lilliefors Significance Correction
3
3
3
.
.
.
.750
.750
.750
3
3
3
.000
.000
.000
b. Kondisi Awal is constant when Formula = F2. It has been omitted.
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
df
Asymp. Sig.
Kondisi Awal
.689
3
.876
Pori M1
3.089
3
.378
Pori M2
8.145
3
.043
Pori M3
10.001
3
.019
Pori M4
10.188
3
.017
a. Kruskal Wallis Test
b. Grouping Variable: Formula
80
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
4.500
10.500
.000
1.000
a
1.000
Pori M1
4.000
10.000
-.232
.817
a
1.000
Pori M2
3.000
9.000
-.674
.500
a
.700
Pori M3
1.000
7.000
-1.623
.105
a
.200
Pori M4
1.000
7.000
-1.623
.105
a
.200
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Kondisi Awal
4.500
Pori M1
3.500
Pori M2
1.000
Pori M3
.000
Pori M4
.000
Wilcoxon W
Z
10.500
.000
9.500
-.471
7.000
-1.623
6.000
-1.993
6.000
-1.993
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
1.000
a
1.000
.637
a
.700
.105
a
.200
.046
a
.100
.046
a
.100
Mann-Whitney U
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
3.500
Pori M1
2.500
Pori M2
.000
Pori M3
.000
Pori M4
.000
9.500
-.471
8.500
-.943
6.000
-1.993
6.000
-1.993
6.000
-1.993
.637
.700
.346
a
.400
a
.046
.100
a
.046
.100
a
.046
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
81
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
4.500
10.500
.000
1.000
a
1.000
Pori M1
2.000
8.000
-1.291
.197
a
.400
Pori M2
1.000
7.000
-1.623
.105
a
.200
Pori M3
.000
6.000
-2.023
.043
a
.100
Pori M4
.000
6.000
-2.023
.043
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
3.000
9.000
-.696
Pori M1
1.000
7.000
-1.650
Pori M2
.000
6.000
-1.993
Pori M3
.000
6.000
-2.023
Pori M4
.000
6.000
-2.023
.487
a
.700
.099
a
.200
.046
a
.100
.043
a
.100
.043
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
3.000
9.000
Pori M1
3.000
9.000
Pori M2
1.000
7.000
Pori M3
.500
6.500
Pori M4
.000
6.000
-1.000
.317
-.745
.456
-1.650
.099
-1.826
.068
-2.023
.043
.700
a
.700
a
.200
a
.100
a
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
82
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Noda (Spot)
1. Uji Normalitas
b
Tests of Normality
Formula
a
Kolmogorov-Smirnov
Kondisi Awal
BLANKO
Statistic
.385
Spot M1
F1
F2
F3
BLANKO
3
.
Statistic
.750
.253
.385
.385
.385
3
3
3
3
.
.
.
.
Spot M3
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
.253
.385
.385
.314
.292
.385
.385
.276
3
3
3
3
3
3
3
3
Spot M4
F1
F2
F3
BLANKO
.175
.385
.175
.314
3
3
3
3
Spot M2
df
Shapiro-Wilk
Sig.
3
Sig.
.000
.964
.750
.750
.750
3
3
3
3
.637
.000
.000
.000
.
.
.
.
.
.
.
.
.964
.750
.750
.893
.923
.750
.750
.942
3
3
3
3
3
3
3
3
.637
.000
.000
.363
.463
.000
.000
.537
.
.
.
.
1.000
.750
1.000
.893
3
3
3
3
1.000
.000
1.000
.363
.750
.750
3
3
.000
.000
F1
.385
3
.
F3
.385
3
.
a. Lilliefors Significance Correction
b. Spot M4 is constant when Formula = F2. It has been omitted.
df
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
df
Kondisi Awal
6.070
3
Spot M1
2.852
3
Spot M2
7.159
3
Spot M3
9.562
3
Spot M4
10.607
3
.108
.415
.067
.023
.014
Asymp. Sig.
a. Kruskal Wallis Test
b. Grouping Variable: Formula
83
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
2.500
8.500
-.899
.369
a
.400
Spot M1
3.000
9.000
-.664
.507
a
.700
Spot M2
2.500
8.500
-.886
.376
a
.400
Spot M3
3.000
9.000
-.674
.500
a
.700
Spot M4
.000
6.000
-1.993
.046
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Spot Sebelum
.500
Spot M1
3.000
Spot M2
2.500
Spot M3
.000
Spot M4
.000
6.500
-1.826
9.000
-.674
8.500
-.943
6.000
-1.993
6.000
-2.087
.068
a
.100
.500
a
.700
.346
a
.400
.046
a
.100
.037
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
1.000
Spot M1
3.000
Spot M2
.000
Spot M3
.000
Spot M4
.000
7.000
-1.573
9.000
-.674
6.000
-1.993
6.000
-1.964
6.000
-1.993
.116
.200
.500
a
.700
a
.046
.100
a
.050
.100
a
.046
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
84
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
.500
6.500
-1.798
.072
a
.100
Spot M1
2.000
8.000
-1.107
.268
a
.400
Spot M2
4.000
10.000
-.232
.817
a
1.000
Spot M3
.000
6.000
-1.993
.046
a
.100
Spot M4
.000
6.000
-2.121
.034
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
1.500
7.500
-1.348
Spot M1
3.500
9.500
-.471
Spot M2
.000
6.000
-1.993
Spot M3
.000
6.000
-1.964
Spot M4
.000
6.000
-2.023
.178
a
.200
.637
a
.700
.046
a
.100
.050
a
.100
.043
a
.100
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed Sig.)]
Kondisi Awal
4.000
10.000
Spot M1
.000
6.000
Spot M2
.000
6.000
Spot M3
.000
6.000
Spot M4
.000
6.000
-.258
.796
-2.023
.043
-2.023
.043
-1.993
.046
-2.121
.034
1.000
a
.100
a
.100
a
.100
a
.100
a
a. Not corrected for ties.
b. Grouping Variable: Formula
85
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
− Keriput (Wrinkle)
1. Uji Normalitas
Tests of Normality
Formula
a
Kolmogorov-Smirnov
3
.
Statistic
.976
.253
.175
.175
.211
.219
.253
.175
.187
.328
.385
.219
.219
.385
.385
.356
.204
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
F1
.385
F2
.385
F3
.175
a. Lilliefors Significance Correction
3
3
3
.
.
.
Kondisi Awal
Keriput M1
Keriput M2
Keriput M3
Keriput M4
BLANKO
Statistic
.238
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
F1
F2
F3
BLANKO
df
Shapiro-Wilk
Sig.
df
3
Sig.
.702
.964
1.000
1.000
.991
.987
.964
1.000
.998
.871
.750
.987
.987
.750
.750
.818
.993
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
3
.637
1.000
1.000
.817
.780
.637
1.000
.915
.298
.000
.780
.780
.000
.000
.157
.843
.750
.750
1.000
3
3
3
.000
.000
1.000
Keriput M3
6.621
3
.085
Keriput M4
7.887
3
.048
2. Uji Kruskal Wallis
a,b
Test Statistics
Chi-square
df
Asymp. Sig.
Kondisi Awal
1.872
3
.599
Keriput M1
4.033
3
.258
Keriput M2
4.587
3
.205
a. Kruskal Wallis Test
b. Grouping Variable: Formula
86
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
3. Uji Mann-Whitney
Blanko dengan F1
b
Test Statistics
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
Mann-Whitney U
2.000
2.000
3.500
4.000
3.000
Wilcoxon W
8.000
8.000
9.500
10.000
9.000
Z
-1.091
-1.091
-.443
-.221
-.664
Asymp. Sig. (2-tailed)
.275
.275
.658
.825
.507
a
a
a
a
a
Exact Sig. [2*(1-tailed
.400
.400
.700
1.000
.700
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
Blanko dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
2.500
3.000
4.000
2.500
2.000
8.500
9.000
10.000
8.500
8.000
-.886
-.655
-.221
-.899
-1.159
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
.376
a
.400
.513
a
.700
.825
a
1.000
.369
a
.400
.246
a
.400
Blanko dengan F3
b
Test Statistics
Mann-Whitney U
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
3.000
4.500
2.500
.000
.000
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
9.000
-.655
.513
a
.700
10.500
.000
1.000
a
1.000
8.500
-.886
.376
a
.400
6.000
-1.964
.050
a
.100
6.000
-1.964
.050
a
.100
87
Universitas Sumatera Utara
Lampiran 10. (Lanjutan)
F1 dengan F2
b
Test Statistics
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
3.000
4.000
1.500
4.000
1.000
9.000
10.000
7.500
10.000
7.000
-.655
-.225
-1.348
-.225
-1.650
.513
.822
.178
.822
.099
a
a
a
a
a
.700
1.000
.200
1.000
.200
b. Grouping Variable: Formula
F1 dengan F3
b
Test Statistics
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
Mann-Whitney U
3.500
.500
.000
.000
.000
Wilcoxon W
9.500
6.500
6.000
6.000
6.000
Z
-.443
-1.771
-1.964
-1.993
-1.993
Asymp. Sig. (2-tailed)
.658
.077
.050
.046
.046
a
a
a
a
a
Exact Sig. [2*(1-tailed
.700
.100
.100
.100
.100
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
F2 dengan F3
b
Test Statistics
Kondisi Awal Keriput M1 Keriput M2 Keriput M3 Keriput M4
2.000
.500
1.000
.000
.000
8.000
6.500
7.000
6.000
6.000
-1.124
-1.771
-1.623
-1.993
-1.993
.261
.077
.105
.046
.046
a
a
a
a
a
.400
.100
.200
.100
.100
Mann-Whitney U
Wilcoxon W
Z
Asymp. Sig. (2-tailed)
Exact Sig. [2*(1-tailed
Sig.)]
a. Not corrected for ties.
b. Grouping Variable: Formula
88
Universitas Sumatera Utara