0.12 mg 0.02 mg 0.06 mg - PENGARUH JENIS KEMASAN (BOTOL PET DAN BLISTER) TERHADAP UMUR SIMPAN KAPSUL BUAH DAN SAYUR FREEZE DRIED: TINJAUAN SIFAT FISIK,VITAMIN A DAN VITAMIN C - Unika Repository

  Perpustakaan Unika

7. LAMPIRAN Lampiran 1. Daftar Komposisi Buah dan Sayur

  

Daftar Komposisi Buah dan Sayur (per 100 gram)

Nutrisi Melon Mangga Wortel Labu Bayam Ubi Jalar Labu Kedondong Brokoli

Kuning Merah Merah Siam

  Kalori 28 kal 59 kal. 42 kal. 29 kal. 51 kal. 47 kal. 23 kal. 59 kal. 25 kal. Protein 0,5 g 0,5 g 1.2 g 1.1 g 3.5 g 2.8 g 0.6 g 3.5 g 2.4 g Lemak 0,2 g 0,4 g 0.3 g 0.3 g 0.5 g 0.4 g 0.1 g 0.3 g 0.2 g Karbohidrat 6,9 g 15,1 g 9.3 g 6.6 g 6.5 g 10.4 g 6.7 g 13.4 g 4.9 g Kalsium 7 mg 12 mg 39 mg 45 mg 267 mg 79 mg 14 mg 540 mg 22 mg Fosfor 12 mg 11 mg 37 mg 64 mg 67 mg 66 mg 25 mg 82 mg 72 mg Besi 0,2 mg 0,4 mg 0.8 mg 1.4 mg 3.9 mg 10.0 mg 0.5 mg 6.2 mg 1.1 mg Vtamin A 590 S.I

85 S.I 12000 S.I 180 S.I 6090 S.I 6015 S.I

  20 S.I 2900 S.I

  90 S.I Vitamin B

  1 0,05 mg 0,06 mg 0.06 mg 0.08 mg 0.08 mg 0.12 mg 0.02 mg 0.06 mg 0.11 mg

  Vitamin C 6 mg 65 mg 6 mg 52 mg 80 mg 22 mg 18 mg 29 mg 69 mg Air 92,1 g 83,7 g 88.2 g 91.2 g 86.9 g 84.7 g 92.3 g 81.0 g 91.7 g Sumber : Direktorat Gizi Departemen Kesehatan Republik Indonesia (1996).

  47

  Lampiran 2. SNI 01-3710-1995 Buah Kering Buah Kering

1. Ruang lingkup

  Standar ini meliputi definisi, syarat mutu, cara pengambilan contoh, cara uji, cara pengemasan, dan syarat penandaan.

  2. Definisi Buah kering adalah produk makanan yang dibuat dari buah segar yang dikeringkan dengan atau tanpa penambahan gula, garam, bahan makanan lain, dan bahan tambahan makanan yang diizinkan.

  3. Syarat Mutu TABEL Syarat Mutu Buah Kering No. Kriteria Uji Satuan Persyaratan

1 Keadaan :

  1.1 Penampakan - Normal

  

1.2 Bau - Normal

  

1.3 Rasa - Normal

  

2 Air % Maks

  31

  3 Bahan tambahan makanan :

  3.1

• Pemanis buatan (sakarin, siklamat) Negatif

  3.2 Pewarna Sesuai SNI 01- 022211987

  3.3 Pengawet Sesuai SNI 01- 022211987

4 Cemaran logam :

  4.1 Timbal (Pb) mg/kg Maks. 2,0

  4.2 Tembaga (Cu) mg/kg Maks. 5,0

  4.3 Seng (Zn) mg/kg Maks. 40,0

  

4.4 Timah (Sc) mg/kg Maks. 40,0 / 250 **

  4.5 Raksa (Hg) mg/kg Maks. 0,03

  5 Cemaran arsen (As) mg/kg Maks. 1,0

  6 Cemaran mikroba :

6.1 E. coli APM / g < 3

• dan revisinya
• khusus untuk produk yang dikemas dalam kaleng

  Lampiran 3. SPSS One Way Anova One Way Anova Bobot Kemasan Blister Oneway Descriptives

  bobot 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0,blister

  20 .43735 .031140 .006963 .42278 .45192 .379 .486 hari 6, blister 20 .43900 .034253 .007659 .42297 .45503 .382 .481 hari 12, blister 20 .44780 .033075 .007396 .43232 .46328 .386 .496 hari 18, blister 20 .45765 .027878 .006234 .44460 .47070 .416 .516 hari 24, blister 20 .46170 .026294 .005880 .44939 .47401 .388 .502 hari 30, blister 20 .47135 .031928 .007139 .45641 .48629 .402 .522 hari 36, blister 20 .47635 .031928 .007139 .46141 .49129 .407 .527 hari 42, blister 20 .48420 .020806 .004652 .47446 .49394 .448 .514

  Total 160 .45943 .033475 .002646 .45420 .46465 .379 .527

  Test of Homogeneity of Variances

  bobot Levene Statistic df1 df2 Sig.

  1.549 7 152 .155

  ANOVA

  bobot Sum of Squares df Mean Square F Sig.

  Between Groups .042 7 .006 6.657 .000

  Within Groups .136 152 .001

  Total .178 159

  Post Hoc Tests Homogeneous Subsets bobot a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2

  3

  

4 hari 0,blister 20 .43735 hari 6, blister 20 .43900 hari 12, blister 20 .44780 .44780 hari 18, blister 20 .45765 .45765 .45765 hari 24, blister 20 .46170 .46170 hari 30, blister 20 .47135 .47135 hari 36, blister 20 .47635 .47635 hari 42, blister 20 .48420 Sig. .051 .169 .073 .204 One Way Anova Bobot Kemasan Botol Oneway

  

Descriptives

  bobot 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0, botol

  20 .43065 .028784 .006436 .41717 .44412 .379 .467 hari 6, botol 20 .44550 .027447 .006137 .43265 .45834 .389 .492 hari 12, botol 20 .45661 .023711 .005302 .44551 .46770 .401 .495 hari 18, botol 20 .46310 .031562 .007058 .44833 .47787 .373 .517 hari 24, botol 20 .46477 .028815 .006443 .45128 .47826 .408 .515 hari 30, botol 20 .46617 .026446 .005914 .45379 .47854 .407 .497 hari 36, botol 20 .47141 .027891 .006237 .45836 .48446 .402 .508 hari 42, botol 20 .46896 .032235 .007208 .45388 .48405 .423 .543

  Total 160 .45839 .030728 .002429 .45360 .46319 .373 .543

  Test of Homogeneity of Variances bobot Levene

  Statistic df1 df2 Sig.

  .250 7 152 .971 ANOVA

  bobot Sum of Squares df Mean Square F Sig.

  Between Groups .027 7 .004 4.735 .000

  Within Groups .123 152 .001

  Total .150 159

  Post Hoc Tests Homogeneous Subsets bobot a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2

  3 hari 0, botol 20 .43065 hari 6, botol 20 .44550 .44550 hari 12, botol 20 .45661 .45661 hari 18, botol 20 .46310 .46310 hari 24, botol 20 .46477 .46477 hari 30, botol 20 .46617 hari 42, botol 20 .46896 hari 36, botol 20 .47141 Sig.

  .101 .051 .156 One Way Anova Kelarutan Kemasan Blister Oneway Descriptives

  kelarutan 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0,blister

  10 5.6000 1.07497 .33993 4.8310 6.3690

  4.00

  7.00 hari 6, blister 10 21.3000 4.00139 1.26535 18.4376 24.1624

  15.00

  26.00 hari 12, blister 10 35.6000 5.50151 1.73973 31.6645 39.5355

  24.00

  46.00 hari 18, blister 10 42.4000 5.10338 1.61383 38.7493 46.0507

  33.00

  49.00 hari 24, blister 10 50.7000 4.29599 1.35851 47.6268 53.7732

  45.00

  57.00 hari 30, blister 10 55.7000 5.61842 1.77670 51.6808 59.7192

  48.00

  66.00 hari 36, blister 10 65.4000 9.26403 2.92954 58.7729 72.0271

  55.00

  81.00 hari 42, blister 10 72.4000 10.07968 3.18748 65.1894 79.6106

  59.00

  87.00 Total 80 43.6375 21.89748 2.44821 38.7645 48.5105

  4.00

  87.00 Test of Homogeneity of Variances

  kelarutan Levene Statistic df1 df2 Sig.

  6.656

  7 72 .000 ANOVA kelarutan Sum of

  Squares df Mean Square F Sig. Between Groups 35082.188

  7 5011.741 128.952 .000 Within Groups 2798.300 72 38.865 Total

  37880.488

79 Post Hoc Tests

  Homogeneous Subsets kelarutan a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2

  3

  4

  5

  6

  7 hari 0,blister 10 5.6000 hari 6, blister 10 21.3000 hari 12, blister 10 35.6000 hari 18, blister 10 42.4000 hari 24, blister 10 50.7000 hari 30, blister 10 55.7000 hari 36, blister

  10 65.4000 hari 42, blister

  10 72.4000 Sig.

  1.000 1.000 1.000 1.000 .077 1.000 1.000 One Way Anova Kelarutan Kemasan Botol Oneway

  

Descriptives

  kelarutan 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0, botol

  10 6.6000 1.17379 .37118 5.7603 7.4397

  5.00

  8.00 hari 6, botol 10 7.7000 1.15950 .36667 6.8705 8.5295

  6.00

  10.00 hari 12, botol 10 22.7000 6.86456 2.17077 17.7894 27.6106

  14.00

  34.00 hari 18, botol 10 27.7000 4.98999 1.57797 24.1304 31.2696

  21.00

  36.00 hari 24, botol 10 34.6000 4.42719 1.40000 31.4330 37.7670

  28.00

  40.00 hari 30, botol 10 42.5000 3.83695 1.21335 39.7552 45.2448

  35.00

  47.00 hari 36, botol 10 51.6000 3.89301 1.23108 48.8151 54.3849

  46.00

  58.00 hari 42, botol 10 61.0000 5.98145 1.89150 56.7211 65.2789

  50.00

  69.00 Total 80 31.8000 18.91513 2.11478 27.5906 36.0094

  5.00

  69.00 Test of Homogeneity of Variances

  kelarutan Levene Statistic df1 df2 Sig.

  5.885

  7 72 .000 ANOVA

  kelarutan Sum of Squares df Mean Square F Sig.

  Between Groups 26824.800 7 3832.114 191.606 .000

  Within Groups 1440.000 72 20.000

  Total 28264.800

79 Post Hoc Tests

  Homogeneous Subsets kelarutan a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2

  3

  4

  5

  6

  7 hari 0, botol 10 6.6000 hari 6, botol 10 7.7000 hari 12, botol 10 22.7000 hari 18, botol 10 27.7000 hari 24, botol 10 34.6000 hari 30, botol 10 42.5000 hari 36, botol

  10 51.6000 hari 42, botol

  10 61.0000 Sig.

  .584 1.000 1.000 1.000 1.000 1.000 1.000 One Way Anova Kadar Air Kemasan Blister Oneway

  

Descriptives

  6 19.6967

  9.894 40 .247 1039.953

  47 Between Groups Within Groups Total

  Sum of Squares df Mean Square F Sig.

  Post Hoc Tests Homogeneous Subsets

ka

  Duncan

  a

  6 7.3317 6 8.8233 6 14.3117 6 16.0483 6 17.7683

  6 18.4633

  6 20.7167

  ANOVA

  1.000 1.000 1.000 1.000 1.000 1.000 1.000 1.000 kombinasi hari 0,blister hari 6, blister hari 12, blister hari 18, blister hari 24, blister hari 30, blister hari 36, blister hari 42, blister Sig.

  N

  1

  2

  3

  4

  5

  6

  7

  ka 1030.059 7 147.151 594.919 .000

  7 40 .003 Levene Statistic df1 df2 Sig.

  ka 6 7.3317 .15917 .06498 7.1646 7.4987

  18.26 6 18.4633 .40322 .16461 18.0402 18.8865

  7.18

  7.58 6 8.8233 .19633 .08015 8.6173 9.0294

  8.49

  9.06 6 14.3117 .30314 .12376 13.9935 14.6298

  13.86

  14.69 6 16.0483 .21217 .08662 15.8257 16.2710

  15.65

  16.27 6 17.7683 .32799 .13390 17.4241 18.1125

  17.27

  17.95

  Test of Homogeneity of Variances ka 3.881

  18.94 6 19.6967 1.12906 .46094 18.5118 20.8815

  18.00

  20.98 6 20.7167 .48273 .19707 20.2101 21.2233

  19.98

  21.28 48 15.3950 4.70390 .67895 14.0291 16.7609

  7.18

  21.28 hari 0,blister hari 6, blister hari 12, blister hari 18, blister hari 24, blister hari 30, blister hari 36, blister hari 42, blister Total

  N Mean Std. Deviation Std. Error Lower Bound Upper Bound 95% Confidence Interval for

  Mean Minimum Maximum

  8 Subset for alpha = .05 Means for groups in homogeneous subsets are displayed. One Way Anova Kadar Air Kemasan Botol Oneway

  

Descriptives

  ka 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0, botol

  6 6.6183 .36641 .14959 6.2338 7.0029

  6.08

  7.05 hari 6, botol 6 8.2617 .13423 .05480 8.1208 8.4025

  8.13

  8.45 hari 12, botol 6 11.8100 .36222 .14787 11.4299 12.1901

  11.34

  12.15 hari 18, botol 6 13.4583 .32945 .13450 13.1126 13.8041

  13.09

  14.04 hari 24, botol 6 13.7367 .33560 .13701 13.3845 14.0889

  13.29

  14.07 hari 30, botol 6 14.9783 .37573 .15339 14.5840 15.3726

  14.54

  15.54 hari 36, botol 6 15.5983 .46145 .18839 15.1141 16.0826

  14.99

  16.24 hari 42, botol 6 16.4317 .39321 .16053 16.0190 16.8443

  15.77

  16.77 Total 48 12.6117 3.34077 .48220 11.6416 13.5817

  6.08

  16.77 Test of Homogeneity of Variances

  ka Levene Statistic df1 df2 Sig.

  .914

  7 40 .506 ANOVA

  ka Sum of Squares df Mean Square F Sig.

  Between Groups 519.488 7 74.213 585.870 .000

  Within Groups 5.067 40 .127

  Total 524.555

47 Post Hoc Tests

  Homogeneous Subsets ka a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2

  3

  4

  5

  6

  7 hari 0, botol 6 6.6183 hari 6, botol 6 8.2617 hari 12, botol 6 11.8100 hari 18, botol 6 13.4583 hari 24, botol 6 13.7367 hari 30, botol 6 14.9783 hari 36, botol

  6 15.5983 hari 42, botol

  6 16.4317 Sig.

  1.000 1.000 1.000 .183 1.000 1.000 1.000 One Way Anova Vitamin A Kemasan Blister Oneway Descriptives

  vitA 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0,blister

  6 341.0517 18.21927 7.43799 321.9317 360.1716 323.07 367.41 hari 6, blister 6 353.2133 23.57932 9.62622 328.4684 377.9583 330.62 385.14 hari 12, blister 6 345.0733 30.46965 12.43918 313.0974 377.0493 309.98 386.71 hari 18, blister 6 347.7883 9.46060 3.86228 337.8600 357.7166 339.02 359.85 hari 24, blister 6 325.6050 8.48788 3.46516 316.6975 334.5125 314.27 333.65 hari 30, blister 6 348.1017 32.35319 13.20813 314.1491 382.0543 311.33 389.72 hari 36, blister 6 347.2850 15.41804 6.29439 331.1048 363.4652 331.89 368.77 hari 42, blister 6 366.2683 7.87026 3.21302 358.0090 374.5277 356.74 375.38

  Total 48 346.7983 21.67022 3.12783 340.5060 353.0907 309.98 389.72

  Test of Homogeneity of Variances vitA Levene

  Statistic df1 df2 Sig.

  3.352

  7 40 .007 ANOVA

  vitA Sum of Squares df Mean Square F Sig.

  Between Groups 5449.836 7 778.548 1.874 .100

  Within Groups 16621.292 40 415.532 Total

  22071.127

47 Post Hoc Tests

  Homogeneous Subsets vitA a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2 hari 24, blister 6 325.6050 hari 0,blister 6 341.0517 341.0517 hari 12, blister 6 345.0733 345.0733 hari 36, blister 6 347.2850 347.2850 hari 18, blister 6 347.7883 347.7883 hari 30, blister 6 348.1017 348.1017 hari 6, blister 6 353.2133 hari 42, blister 6 366.2683

  Sig. .100 .069 One Way Anova Vitamin A Kemasan Botol Oneway

  

Descriptives

  vitA 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0, botol

  6 348.1667 37.69752 15.38995 308.6055 387.7278 314.37 404.86 hari 6, botol 6 353.8067 56.25627 22.96653 294.7693 412.8440 289.84 418.02 hari 12, botol 6 347.4250 13.32677 5.44063 333.4394 361.4106 331.65 365.76 hari 18, botol 6 346.7483 22.90853 9.35237 322.7073 370.7894 314.97 377.30 hari 24, botol 6 340.0433 25.58900 10.44667 313.1893 366.8973 314.72 377.07 hari 30, botol 6 334.6167 29.97541 12.23741 303.1594 366.0739 293.49 367.52 hari 36, botol 6 338.8550 5.68222 2.31976 332.8919 344.8181 332.29 347.91 hari 42, botol 6 357.8617 4.69224 1.91560 352.9375 362.7859 352.03 364.73

  Total 48 345.9404 28.06891 4.05140 337.7901 354.0908 289.84 418.02

  Test of Homogeneity of Variances

  vitA Levene Statistic df1 df2 Sig.

  4.595

  7 40 .001

  ANOVA

  vitA Sum of Squares df Mean Square F Sig.

  Between Groups 2550.078 7 364.297 .423 .882 Within Groups 34479.514 40 861.988 Total

  37029.592

47 Post Hoc Tests

  Homogeneous Subsets vitA a

  Duncan Subset for alpha

  = .05 kombinasi N 1 hari 30, botol

  6 334.6167 hari 36, botol 6 338.8550 hari 24, botol 6 340.0433 hari 18, botol 6 346.7483 hari 12, botol 6 347.4250 hari 0, botol 6 348.1667 hari 6, botol 6 353.8067 hari 42, botol 6 357.8617 Sig.

  .248 One Way Anova Vitamin C Kemasan Blister Oneway Descriptives

  vitc 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0,blister

  6 32.9967 .52435 .21407 32.4464 33.5469

  32.48

  33.53 hari 6, blister 6 31.7667 .52175 .21300 31.2191 32.3142

  31.18

  32.50 hari 12, blister 6 30.8350 .33709 .13762 30.4812 31.1888

  30.27

  31.12 hari 18, blister 6 29.9850 .38672 .15788 29.5792 30.3908

  29.49

  30.55 hari 24, blister 6 30.1967 .52435 .21407 29.6464 30.7469

  29.68

  30.73 hari 30, blister 6 31.8967 .90917 .37117 30.9426 32.8508

  31.02

  33.10 hari 36, blister 6 31.5933 .52279 .21343 31.0447 32.1420

  31.05

  32.20 hari 42, blister 6 30.7667 .52175 .21300 30.2191 31.3142

  30.18

  31.50 Total 48 31.2546 1.07290 .15486 30.9430 31.5661

  29.49

  33.53 Test of Homogeneity of Variances

  vitc Levene Statistic df1 df2 Sig.

  4.775

  7 40 .001 ANOVA

  vitc Sum of Squares df Mean Square F Sig.

  Between Groups 41.815 7 5.974 19.447 .000

  Within Groups 12.287 40 .307

  Total 54.103

47 Post Hoc Tests

  Homogeneous Subsets vitc a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2

  3

  4 hari 18, blister 6 29.9850 hari 24, blister 6 30.1967 30.1967 hari 42, blister 6 30.7667 hari 12, blister 6 30.8350 hari 36, blister 6 31.5933 hari 6, blister 6 31.7667 hari 30, blister 6 31.8967 hari 0,blister 6 32.9967

  Sig. .512 .065 .378 1.000 One Way Anova Vitamin C Kemasan Botol Oneway

  

Descriptives

  vitc 95% Confidence Interval for

  Mean N Mean Std. Deviation Std. Error Lower Bound Upper Bound Minimum Maximum hari 0, botol

  6 39.0383 .19457 .07943 38.8341 39.2425

  38.85

  39.34 hari 6, botol 6 37.1933 .20077 .08196 36.9826 37.4040

  37.06

  37.59 hari 12, botol 6 38.3833 .40297 .16451 37.9604 38.8062

  37.89

  38.78 hari 18, botol 6 40.3900 .65715 .26828 39.7004 41.0796

  39.39

  41.20 hari 24, botol 6 42.0033 .22232 .09076 41.7700 42.2366

  41.76

  42.35 hari 30, botol 6 41.8267 .68028 .27772 41.1128 42.5406

  40.85

  42.46 hari 36, botol 6 40.2350 .10387 .04241 40.1260 40.3440

  40.11

  40.36 hari 42, botol 6 42.3933 .27940 .11407 42.1001 42.6865

  42.01

  42.82 Total 48 40.1829 1.80407 .26039 39.6591 40.7068

  37.06

  42.82 Test of Homogeneity of Variances

  vitc Levene Statistic df1 df2 Sig.

  5.243

  7 40 .000 ANOVA

  vitc Sum of Squares df Mean Square F Sig.

  Between Groups 146.601 7 20.943 131.566 .000 Within Groups

  6.367 40 .159 Total

  152.969

47 Post Hoc Tests

  Homogeneous Subsets vitc a

  Duncan Subset for alpha = .05 kombinasi N

  1

  2

  3

  4

  5

  6 hari 6, botol 6 37.1933 hari 12, botol 6 38.3833 hari 0, botol 6 39.0383 hari 36, botol 6 40.2350 hari 18, botol 6 40.3900 hari 30, botol 6 41.8267 hari 24, botol 6 42.0033 42.0033 hari 42, botol

  6 42.3933 Sig.

  1.000 1.000 1.000 .505 .448 .098

  Lampiran 4. SPSS Normalitas Normalitas bobot

  Tests of Normality a

  Kolmogorov-Smirnov Shapiro-Wilk kombinasi Statistic df Sig. Statistic df Sig. bobot hari 0,blister .126 20 .200* .952 20 .395 hari 0, botol

  .165 20 .154 .906 20 .054 hari 6, blister .165 20 .160 .904 20 .048 hari 6, botol .116 20 .200* .966 20 .667 hari 12, blister .142 20 .200* .940 20 .237 hari 12, botol .158 20 .200* .950 20 .374 hari 18, blister .155 20 .200* .955 20 .456 hari 18, botol .184 20 .076 .928 20 .140 hari 24, blister .164 20 .163 .924 20 .119 hari 24, botol .157 20 .200* .963 20 .597 hari 30, blister .146 20 .200* .964 20 .634 hari 30, botol .143 20 .200* .897 20 .037 hari 36, blister .146

  20 .200* .964 20 .634 hari 36, botol .153 20 .200* .911 20 .066 hari 42, blister .131 20 .200* .931 20 .160 hari 42, botol .148 20 .200* .954 20 .438 *. This is a lower bound of the true significance.

  a.

  Lilliefors Significance Correction Normalitas Kadar Air

  Tests of Normality a

  Kolmogorov-Smirnov Shapiro-Wilk kombinasi Statistic df Sig. Statistic df Sig. ka hari 0,blister .270

  6 .196 .885 6 .290 hari 0, botol .201 6 .200* .946 6 .712 hari 6, blister .226 6 .200* .946 6 .710 hari 6, botol .253 6 .200* .887 6 .303 hari 12, blister .164 6 .200* .972 6 .905 hari 12, botol .255

  6 .200* .846 6 .145 hari 18, blister .280 6 .153 .855 6 .172 hari 18, botol .283 6 .144 .895 6 .343 hari 24, blister .177 6 .200* .979 6 .945 hari 24, botol

  .247 6 .200* .876 6 .249 hari 30, blister .230 6 .200* .918 6 .492 hari 30, botol .154 6 .200* .964 6 .848 hari 36, blister .190 6 .200* .931 6 .586 hari 36, botol .139 6 .200* .981 6 .957 hari 42, blister .154 6 .200* .964 6 .850 hari 42, botol .253

  6 .200* .870 6 .225 *. This is a lower bound of the true significance. Normalitas Kelarutan Kapsul Tests of Normality

  .245 10 .090 .892 10 .177 .195 10 .200* .878 10 .124 .170 10 .200* .900 10 .218 .227 10 .155 .916 10 .328 .231 10 .138 .900 10 .218 .135 10 .200* .950 10 .672 .116 10 .200* .966 10 .847 .127 10 .200* .946 10 .624 .154 10 .200* .934 10 .483 .141 10 .200* .920 10 .355 .122 10 .200* .969 10 .881 .152 10 .200* .928 10 .428 .183 10 .200* .916 10 .325 .161 10 .200* .954 10 .718 .211 10 .200* .884 10 .143 .192 10 .200* .939 10 .539 kombinasi hari 0,blister hari 0, botol hari 6, blister hari 6, botol hari 12, blister hari 12, botol hari 18, blister hari 18, botol hari 24, blister hari 24, botol hari 30, blister hari 30, botol hari 36, blister hari 36, botol hari 42, blister hari 42, botol kelarutan Statistic df Sig. Statistic df Sig.

  Kolmogorov-Smirnov a

  Shapiro-Wilk This is a lower bound of the true significance.

• .

  Lilliefors Significance Correction a.

  Normalitas Vitamin A Tests of Normality

  .270 6 .198 .875 6 .248 .275 6 .175 .857 6 .181 .285 6 .140 .840 6 .131 .205 6 .200* .870 6 .226 .194 6 .200* .935 6 .616 .183 6 .200* .944 6 .688 .282 6 .147 .835 6 .119 .152 6 .200* .979 6 .946 .285 6 .139 .834 6 .116 .196 6 .200* .908 6 .422 .195 6 .200* .908 6 .422 .193 6 .200* .919 6 .497 .254 6 .200* .877 6 .257 .215 6 .200* .949 6 .729 .216 6 .200* .889 6 .311 .193 6 .200* .962 6 .839 kombinasi hari 0,blister hari 0, botol hari 6, blister hari 6, botol hari 12, blister hari 12, botol hari 18, blister hari 18, botol hari 24, blister hari 24, botol hari 30, blister hari 30, botol hari 36, blister hari 36, botol hari 42, blister hari 42, botol vitA Statistic df Sig. Statistic df Sig.

  Kolmogorov-Smirnov

a

  Shapiro-Wilk Normalitas Vitamin C Tests of Normality

  Kolmogorov-Smirnov

a

  .303 6 .090 .756 6 .023 .323 6 .050 .850 6 .156 .189 6 .200* .926 6 .548 .320 6 .054 .712 6 .008 .257 6 .200* .864 6 .202 .238 6 .200* .852 6 .162 .156 6 .200* .975 6 .923 .148 6 .200* .980 6 .951 .303 6 .090 .756 6 .023 .191 6 .200* .937 6 .638 .275 6 .175 .836 6 .120 .233 6 .200* .870 6 .226 .276 6 .171 .819 6 .087 .224 6 .200* .886 6 .299 .189 6 .200* .926 6 .548 .176 6 .200* .975 6 .925 kombinasi hari 0,blister hari 0, botol hari 6, blister hari 6, botol hari 12, blister hari 12, botol hari 18, blister hari 18, botol hari 24, blister hari 24, botol hari 30, blister hari 30, botol hari 36, blister hari 36, botol hari 42, blister hari 42, botol vitc Statistic df Sig. Statistic df Sig.

  Shapiro-Wilk This is a lower bound of the true significance.

• .

  Lilliefors Significance Correction a.

  Lampiran 5. Perhitungan ASLT

Persamaan Arhennius digunakan untuk mengkonversi lamanya waktu penyimpanan,

maka kondisi normal (suhu kamar) umur simpan bahan pangan dapat diketahui dengan perhitungan di bawah ini :

  δT/10

  Q = ts (T )

  1

  ts (T

  2 ) δT/10

  dimana : Q = faktor percepatan ts (T ) = masa kadaluarsa jika disimpan pada suhu TºC

  1

  ts (T

  2 ) = masa kadaluarsa jika disimpan pada suhu T + 10ºC

  Dalam penelitian digunakan suhu 40ºC (kelembaban 90%) selama 42 hari, maka apabila dikonversikan pada suhu kamar (25ºC) menjadi :

  δT/10 δT/10

  Q = 4 ts (T

  1 ) = ts (T 2 ) x Q

  Suhu penelitian (T

  2 ) = 40ºC 15/10

  Suhu kamar (T ) = 25ºC = 42 x 4

  1 T 2 -T

  1

  δT = = 40ºC-25ºC = 336 hari = 48 minggu = 15ºC = 12 bulan

  Konversi Lama Penyimpanan ASLT (40

  C) Terhadap Lama Penyimpanan suhu ruang (25 C) Q = 4

10 T = 40ºC (hari) T = 25ºC (hari)

  Titik ke-0 (hari ke-0) Titik ke-1 (hari ke-6)

48 Titik ke-2 (hari ke-12)

  72 Titik ke-3 (hari ke-18) 144 Titik ke-4 (hari ke-24) 192 Titik ke-5 (hari ke-30) 240 Titik ke-6 (hari ke-36) 288 Titik ke-7 (hari ke-40) 336

  Lampiran 6. Perhitungan Harga Pokok Produk Kapsul Buah &amp; Sayur

PERHITUNGAN HPP per 1000 g Kapsul

JUMLAH

HARGA TOTAL HARGA (BERAT) BAHAN BAKU

  

Melon 1,536 kg 5000/ kg 7680

Mangga 1,536 kg 2500/ kg 3840

Wortel 1,536 kg 8000/ kg 12288

Brokoli 1,536 kg 6000/ kg 9216

Kedondong 1,536 kg 6000/ kg 9216

Labu Siam 1,536 kg 1000/ kg 1536

Labu Kuning 1,536 kg 3500/ kg 5376

Bayam Merah 1,536 kg 5000/ kg 7680

Ubi Jalar Merah 1,536 kg 2000/ kg 3072

Mg Stearat 8,64 g 14910/ kg 129

Aerosil 4,32 g 61154/ kg 264

Amilum 172,8 g 23379/ kg 4040

Kapsul 2192 buah 30/ kapsul 65760

KEMASAN

Botol PET @ 65 kapsul 16 buah 1700/ botol 27200

Blister @ 12 kapsul 96 buah 475/ blister 45600

LISTRIK

Freezer 3 kw 7 jam 800/ kw 16800

  5,5 kw 28 jam 800/ kw 123200 Freeze Dryer TOTAL BIAYA 1 kg

  342987

  Lampiran 7. Freeze Dry Log Sheet PRODUCT Ice Test

  : Fruits &amp; Vegetables BATCH No

  : 2 Hours start

  DATE : 2.10 pm at 12.02.08 : 12 February 2008

  Hours end

WEIGHT IN

  

: 06.00 pm at 13.02.08 : 42,685 kg

Total

WEIGHT OUT

  : 4,95 kg DATE TIME VACUUM STEP ACTUAL ACTUAL ICE PRODUCT TEMP PRESSURE TEMP SET (sv) SET (sv) READ (pv) T1 T2 T3

  12.02.08 14.10 20 mbar 1 -17,9 -16,1 -37,2 16.10 0,6 mbar 1 -9,3 10,0 -24,4 18.10 0,4 mbar 1 -0,2 -0,7 -23,1

  22.10 0.6 mbar 2 27,4 26,7 -19,8 13.02.08 02.10 0,4 mbar 2 54,8 54,1 -21,7

  10.10 0,2 mbar 3 55,0 54,1 -25,6 12.10 0,2 mbar 3 55,0 54,1 -34,3 15.10 0,2 mbar 4 50,2 50,9 -25,1

  18.10 VACUUM PUMP OIL :

  OBSEVATION &amp; COMMENTS :

  Start freezer = 07.00 am Stop freezer = 01.45 pm Start Mesin Freeze Dry = 12.00 pm (warming up + 105 menit) Buah dan Sayur masuk ke mesin = 02.00 pm

PROGRAM SET

  o o

  1. -18 C – 0 C = 4 hour

  o o

  2. 0 C – 55 C = 8 hour

  o

  3. 55 C = 10 hour

  o o

  4. 55 C – 45 C = 6 hour

  o

  5. 55 C = 12 hour

  0,3092 0,6052 1,1425 y = 0,2081x - 0,3416

  Lampiran 8. Kurva Standar Vitamin A standar hari 0 0,036 0,0724 0,1556

  1 1,2 1,4 3,125 6,25 12,5

  25 50 100 konsentrasi ab so rb a n s i absorbansi Linear (absorbansi) standar hari 12

• 0,2 0,2 0,4 0,6 0,8

• 0,2 0,2 0,4 0,6 0,8

  0,0286 0,0824 0,4312 0,6071 0,9171

  25 50 100 konsentrasi ab s o rb an s i absorbansi Linear (absorbansi) standar hari 36

  1 1,2 1,4 3,125 6,25 12,5

  1,2461 y = 0,2505x - 0,3247

  0,0294 0,0832 0,2326 0,4509

  25 50 100 konsentrasi ab so rb an si absorbansi Linear (absorbansi) standar hari 24

  1 1,2 1,4 3,125 6,25 12,5

  1,1461 y = 0,2075x - 0,3618

  0,0148 0,0631 0,13883 0,2692 0,5552

• 0,4
• 0,2 0,2 0,4 0,6 0,8
• 0,4
• 0,2 0,2 0,4 0,6 0,8

• 0,2 0,2 0,4 0,6 0,8
• 0,4
• 0,2 0,2 0,4 0,6 0,8

  1 1,2 1,4 3,125 6,25 12,5

  0,7176 1,2478 y = 0,2347x - 0,3611

  1,2468 y = 0,257x - 0,3369

  25 50 100 konsentrasi ab so rb an si absorbansi Linear (absorbansi)

  1,1461 y = 0,2079x - 0,3662

  standar hari 6 0,036 0,0719 0,1553

  0,3093 0,6047 1,1417 y = 0,208x - 0,3416

  1 1,2 1,4 3,125 6,25 12,5

  25 50 100 konsentrasi ab so rb an si absorbansi Linear (absorbansi) standar hari 18

  0,0132 0,0592 0,1331 0,2643 0,5531

  1 1,2 1,4 3,125 6,25 12,5

  1 1,2 1,4 3,125 6,25 12,5

  25 50 100 konsentrasi ab so rb an si absorbansi Linear (absorbansi)

  Standar hari 30 0,0281 0,0522 0,1823

  0,4457 0,7167 1,2468 y = 0,2386x - 0,3897

  1 1,2 1,4 3,125 6,25 12,5

  25 50 100 Konsentrasi A b so rb an si absorbansi Linear (absorbansi) standar hari 42

  0,0284 0,0816 0,352 0,751 0,9167

  25 50 100 konsentrasi ab so rb an si absorbansi Linear (absorbansi)

• 0,2 0,2 0,4 0,6 0,8
• 0,2 0,2 0,4 0,6 0,8