Studi Karakteristik Abu Sekam Padi Dengan Kitosan Molekul Tinggi Nanopartikel Sebagai Bahan Dentinogenesis Pada Kavitas Profunda (In Vitro)
Alur Penelitian
Lampiran 1
I
II
Pembuatan Abu Sekam Padi (ASP) merah
jambu nanopartikel
III
Persiapan sampel gigi P
Pembuatan Gel kitosan
nanopartikel
Penanaman sampel gigi P dalam pipa paralon
ASP 10 gr
grinding jar
Aplikasi Bahan Uji yang dibagi menjadi 3 kelompok,
masing-masing kelompok terdiri dari 8 sampel
1 gr kitosan + 100 ml
larutan asam asetat 1%
Diaduk pada kecepatan
200 rpm (± 30 menit)
Gel kitosan.
Kelompok III
Gel kitosan dimasukkan
dalam ultrasonic bath
Preparasi kavitas profunda klas I
ASP 10 gr
grinding jar
Planetary Ball Mills ( Retsch, PM
200), 2 jam, kecepatan 250 rpm
Kelompok I
Kelompok II
MTA
SIKMR
ASP Nanopartikel 20 gr
ASP nano + kitosan
molekul tinggi nano
Gel Kitosan blangkas
Sampel gigi P di bagi dua pada arah bukal-lingual dan di potong
pada daerah servikal gigi
Sampel dilakukan pemeriksaan dengan SEM-EDX
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Lampiran 2
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Lampiran 3
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Lampiran 4
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Lampiran 5
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Lampiran 6
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Lampiran 7
UJI NORMALITAS DATA
b,c
Tests of Normality
a
Kolmogorov-Smirnov
kelompok
C
O
*
.930
8
.515
.200
*
.921
8
.438
8
.095
.815
8
.051
8
*
.957
8
.779
*
.897
8
.274
*
.200
SIKMR
.189
8
MTA
.268
8
.200
.200
MTA
.218
8
.200
.873
8
.162
ASP + KITOSAN
.284
8
.056
.902
8
.304
8
*
.965
8
.859
*
.936
8
.574
*
.919
8
.422
*
.912
8
.368
*
.907
8
.334
*
.873
8
.160
*
MTA
MTA
ASP + KITOSAN
.148
.201
.173
.181
.204
.226
8
8
8
8
8
.200
.200
.200
.200
.200
.200
SIKMR
.137
8
.200
.964
8
.844
MTA
.306
8
.026
.745
8
.057
8
*
.897
8
.274
*
ASP + KITOSAN
.209
.200
SIKMR
.159
8
.200
.977
8
.949
MTA
.292
8
.044
.913
8
.372
8
*
.877
8
.176
*
.908
8
.343
*
ASP + KITOSAN
SIKMR
Si
.100
8
SIKMR
Ca
8
.198
.235
Sig.
.852
ASP + KITOSAN
.149
df
*
.200
ASP + KITOSAN
P
Statistic
8
SIKMR
N
Sig.
.209
SIKMR
Na
df
MTA
ASP + KITOSAN
F
Statistic
Shapiro-Wilk
.215
.238
8
.200
.200
MTA
.092
8
.200
.993
8
.998
ASP + KITOSAN
.303
8
.030
.769
8
.053
8
*
.848
8
.091
SIKMR
.238
.200
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Al
MTA
.172
8
.200
*
.954
8
.755
ASP + KITOSAN
.252
8
.143
.906
8
.328
SIKMR
.242
8
.185
.876
8
.172
a. Lilliefors Significance Correction
*. This is a lower bound of the true significance.
b. Bi is constant when kelompok = ASP + KITOSAN. It has been omitted.
c. Bi is constant when kelompok = SIKMR. It has been omitted.
Descriptive Statistics
N
Minimum
Bi
8
Valid N (listwise)
8
.80
Maximum
1.32
Mean
Std. Deviation
1.0950
.19849
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ONE WAY
Descriptives
C
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8 80.4450
1.14909
.40626
79.4843
81.4057
79.65
83.22
ASP +
8 67.6388
1.13839
.40248
66.6870
68.5905
65.90
69.86
2.9738
.19770
.06990
2.8085
3.1390
2.62
3.20
24 50.3525
34.64826
7.07255
35.7218
64.9832
2.62
83.22
KITOSAN
SIKMR
8
Total
Test of Homogeneity of Variances
C
Levene Statistic
2.138
df1
df2
2
Sig.
21
.143
ANOVA
C
Sum of Squares
Between Groups
27592.952
Df
Mean Square
2
13796.476
F
Sig.
15586.827
.000
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*Within Groups
Total
18.588
21
27611.539
23
.885
Post Hoc Tests
Multiple Comparisons
C
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
12.80625
SIKMR
77.47125
ASP + KITOSAN MTA
Std. Error
Sig.
Lower Bound
Upper Bound
*
.47041
.000
11.8280
13.7845
*
.47041
.000
76.4930
78.4495
*
.47041
.000
-13.7845
-11.8280
*
.47041
.000
63.6867
65.6433
*
.47041
.000
-78.4495
-76.4930
*
.47041
.000
-65.6433
-63.6867
-12.80625
SIKMR
SIKMR
Difference (I-J)
64.66500
MTA
-77.47125
ASP + KITOSAN
-64.66500
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
O
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
3.4013
.65743
.23244
2.8516
3.9509
2.77
4.86
ASP +
8
10.5562
.53984
.19086
10.1049
11.0076
9.77
11.66
8
21.8663
.28874
.10208
21.6249
22.1076
21.47
22.32
24
11.9412
7.78095
1.58828
8.6556
15.2269
2.77
22.32
KITOSAN
SIKMR
Total
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Test of Homogeneity of Variances
O
Levene Statistic
df1
.587
df2
Sig.
2
21
.565
ANOVA
O
Sum of Squares
Between Groups
Mean Square
F
1386.844
2
693.422
5.649
21
.269
1392.493
23
Within Groups
Total
Df
Sig.
2577.748
.000
Post Hoc Tests
Multiple Comparisons
O
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
SIKMR
ASP + KITOSAN MTA
Difference (I-J)
Std. Error
Sig.
Lower Bound
Upper Bound
*
.25933
.000
-7.6943
-6.6157
*
.25933
.000
-19.0043
-17.9257
*
.25933
.000
6.6157
7.6943
-7.15500
-18.46500
7.15500
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SIKMR
SIKMR
*
.25933
.000
-11.8493
-10.7707
*
.25933
.000
17.9257
19.0043
*
.25933
.000
10.7707
11.8493
-11.31000
MTA
18.46500
ASP + KITOSAN
11.31000
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
F
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.7338
.52334
.18503
.2962
1.1713
.12
1.40
ASP +
8
1.7913
.40951
.14478
1.4489
2.1336
1.14
2.12
8
7.4013
1.49124
.52723
6.1545
8.6480
5.00
8.76
24
3.3088
3.12155
.63718
1.9906
4.6269
.12
8.76
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
F
Levene Statistic
14.728
df1
df2
2
Sig.
21
.000
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ANOVA
F
Sum of Squares
Between Groups
Within Groups
Total
Df
Mean Square
F
205.456
2
102.728
18.658
21
.888
224.113
23
Sig.
115.625
.000
Post Hoc Tests
Multiple Comparisons
F
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
-1.05750
SIKMR
-6.66750
ASP + KITOSAN
MTA
SIKMR
SIKMR
MTA
ASP + KITOSAN
(I-J)
Std. Error
Sig.
Lower Bound
Upper Bound
*
.47129
.036
-2.0376
-.0774
*
.47129
.000
-7.6476
-5.6874
*
.47129
.036
.0774
2.0376
*
.47129
.000
-6.5901
-4.6299
*
.47129
.000
5.6874
7.6476
*
.47129
.000
4.6299
6.5901
1.05750
-5.61000
6.66750
5.61000
*. The mean difference is significant at the 0.05 level.
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Oneway
Descriptives
Na
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.4662
.13201
.04667
.3559
.5766
.23
.65
ASP +
8
1.3263
.18731
.06622
1.1697
1.4828
1.04
1.55
8
2.4463
.34247
.12108
2.1599
2.7326
2.05
2.92
24
1.4129
.85872
.17529
1.0503
1.7755
.23
2.92
F
Sig.
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
Na
Levene Statistic
5.342
df1
df2
2
Sig.
21
.013
ANOVA
Na
Sum of Squares
Between Groups
Within Groups
Total
df
Mean Square
15.772
2
7.886
1.189
21
.057
16.960
23
139.331
.000
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Post Hoc Tests
Multiple Comparisons
Na
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
Difference (I-J)
MTA
ASP + KITOSAN
Upper Bound
.000
-1.1074
-.6126
*
.11895
.000
-2.2274
-1.7326
*
.11895
.000
.6126
1.1074
*
.11895
.000
-1.3674
-.8726
*
.11895
.000
1.7326
2.2274
*
.11895
.000
.8726
1.3674
.86000
SIKMR
Lower Bound
.11895
-1.98000
ASP + KITOSAN MTA
Sig.
*
-.86000
SIKMR
SIKMR
Std. Error
-1.12000
MTA
1.98000
ASP + KITOSAN
1.12000
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
N
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.3737
.15611
.05519
.2432
.5043
.19
.61
ASP +
8
2.5388
.22681
.08019
2.3491
2.7284
2.24
2.89
8 24.8075
2.86019
1.01123
22.4163
27.1987
21.88
30.18
KITOSAN
SIKMR
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Descriptives
N
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.3737
.15611
.05519
.2432
.5043
.19
.61
ASP +
8
2.5388
.22681
.08019
2.3491
2.7284
2.24
2.89
8 24.8075
2.86019
1.01123
22.4163
27.1987
21.88
30.18
11.39166
2.32531
4.4297
14.0503
.19
30.18
KITOSAN
SIKMR
Total
24
9.2400
ANOVA
N
Sum of Squares
Between Groups
Within Groups
Total
Df
Mean Square
2926.914
2
1463.457
57.795
21
2.752
2984.709
23
F
531.748
Sig.
.000
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Post Hoc Tests
Multiple Comparisons
N
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
(I-J)
MTA
ASP + KITOSAN
SIKMR
Upper Bound
.016
-3.8900
-.4400
*
.82948
.000
-26.1588
-22.7087
*
.82948
.016
.4400
3.8900
*
.82948
.000
-23.9938
-20.5437
*
.82948
.000
22.7087
26.1588
*
.82948
.000
20.5437
23.9938
2.16500
SIKMR
Lower Bound
.82948
-24.43375
MTA
Sig.
*
-2.16500
SIKMR
ASP + KITOSAN
Std. Error
-22.26875
MTA
24.43375
ASP + KITOSAN
22.26875
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
P
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
3.3888
.35430
.12526
3.0925
3.6850
2.63
3.73
ASP +
8
1.6438
.31296
.11065
1.3821
1.9054
1.02
1.98
8 16.4513
1.72484
.60982
15.0092
17.8933
13.35
18.85
KITOSAN
SIKMR
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Total
24
7.1613
6.82138
1.39241
4.2808
10.0417
1.02
18.85
Test of Homogeneity of Variances
P
Levene Statistic
df1
7.589
df2
2
Sig.
21
.003
ANOVA
P
Sum of Squares
Between Groups
Mean Square
F
1047.829
2
523.915
22.390
21
1.066
1070.219
23
Within Groups
Total
df
Sig.
491.395
.000
Post Hoc Tests
Multiple Comparisons
P
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
Difference (I-J)
Std. Error
*
1.74500
.51628
Sig.
.003
Lower Bound
.6713
Upper Bound
2.8187
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SIKMR
ASP + KITOSAN MTA
.51628
.000
-14.1362
-11.9888
*
.51628
.003
-2.8187
-.6713
*
.51628
.000
-15.8812
-13.7338
*
.51628
.000
11.9888
14.1362
*
.51628
.000
13.7338
15.8812
-1.74500
SIKMR
SIKMR
*
-13.06250
-14.80750
MTA
13.06250
ASP + KITOSAN
14.80750
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
Ca
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
7.9413
.69372
.24527
7.3613
8.5212
7.35
9.38
ASP +
8
1.8775
.40138
.14191
1.5419
2.2131
1.41
2.41
8
5.6463
.16071
.05682
5.5119
5.7806
5.48
5.93
24
5.1550
2.59305
.52930
4.0601
6.2499
1.41
9.38
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
Ca
Levene Statistic
5.066
df1
df2
2
Sig.
21
.016
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ANOVA
Ca
Sum of Squares
Between Groups
Within Groups
Total
Df
Mean Square
149.972
2
74.986
4.677
21
.223
154.649
23
F
Sig.
336.676
.000
Post Hoc Tests
Multiple Comparisons
Ca
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
6.06375
SIKMR
2.29500
ASP + KITOSAN MTA
SIKMR
Difference (I-J) Std. Error
Lower Bound
Upper Bound
*
.23597
.000
5.5730
6.5545
*
.23597
.000
1.8043
2.7857
*
.23597
.000
-6.5545
-5.5730
*
.23597
.000
-4.2595
-3.2780
*
.23597
.000
-2.7857
-1.8043
*
.23597
.000
3.2780
4.2595
-6.06375
SIKMR
-3.76875
MTA
-2.29500
ASP + KITOSAN
Sig.
3.76875
*. The mean difference is significant at the 0.05 level.
Oneway
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Descriptives
Si
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
3.3775
.27855
.09848
3.1446
3.6104
3.03
3.78
ASP +
8 12.1463
.81054
.28657
11.4686
12.8239
11.30
13.29
8
5.2913
.19577
.06922
5.1276
5.4549
5.01
5.57
24
6.9383
3.87595
.79117
5.3017
8.5750
3.03
13.29
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
Si
Levene Statistic
15.002
df1
df2
2
Sig.
21
.000
ANOVA
Si
Sum of Squares
Between Groups
Within Groups
Total
df
Mean Square
340.119
2
170.059
5.410
21
.258
345.529
23
F
660.092
Sig.
.000
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Post Hoc Test
Multiple Comparisons
Si
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
(I-J)
MTA
ASP + KITOSAN
8.76875
SIKMR
6.85500
ASP + KITOSAN MTA
SIKMR
Std. Error
Sig.
Lower Bound
Upper Bound
*
.25379
.000
-9.2965
-8.2410
*
.25379
.000
-2.4415
-1.3860
*
.25379
.000
8.2410
9.2965
*
.25379
.000
6.3272
7.3828
*
.25379
.000
1.3860
2.4415
*
.25379
.000
-7.3828
-6.3272
1.91375
SIKMR
6.85500
MTA
1.91375
ASP + KITOSAN
8.76875
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
Al
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.4813
.20904
.07391
.3065
.6560
.24
.89
ASP +
8
.1837
.05317
.01880
.1393
.2282
.10
.26
8 13.0800
.88494
.31287
12.3402
13.8198
11.18
14.11
KITOSAN
SIKMR
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Descriptives
Al
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.4813
.20904
.07391
.3065
.6560
.24
.89
ASP +
8
.1837
.05317
.01880
.1393
.2282
.10
.26
8 13.0800
.88494
.31287
12.3402
13.8198
11.18
14.11
1.25746
1.9804
7.1829
.10
14.11
KITOSAN
SIKMR
Test of Homogeneity of Variances
Al
Levene Statistic
df1
df2
5.026
Total
2
24
Sig.
21
4.5817
.016
6.16026
ANOVA
Al
Sum of Squares
Between Groups
Within Groups
Df
Mean Square
867.014
2
433.507
5.807
21
.277
F
Sig.
1567.574
.000
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Total
872.822
23
Post Hoc Tests
Multiple Comparisons
Al
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
SIKMR
ASP + KITOSAN
MTA
SIKMR
SIKMR
(I-J)
Std. Error
Sig.
Lower Bound
Upper Bound
.29750
.26294
.271
-.2493
.8443
-12.59875
*
.26294
.000
-13.1456
-12.0519
-.29750
.26294
.271
-.8443
.2493
*
.26294
.000
-13.4431
-12.3494
*
.26294
.000
12.0519
13.1456
*
.26294
.000
12.3494
13.4431
-12.89625
MTA
12.59875
ASP + KITOSAN
12.89625
*. The mean difference is significant at the 0.05 level.
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Lampiran 8
MINERAL TRIOXIDE AGGREGATE ( MTA )
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MINERAL TRIOXIDE AGGREGATE ( MTA )
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ABU SEKAM PADI DENGAN KITOSAN
ABU SEKAM PADI DENGAN KITOSAN
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SEMEN IONOMER KACA MODIFIKASI RESIN (SIKMR)
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SEMEN IONOMER KACA MODIFIKASI RESIN (SIKMR)
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Lampiran 9
HASIL UJI XRD ABU SEKAM PADI
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Lampiran 1
I
II
Pembuatan Abu Sekam Padi (ASP) merah
jambu nanopartikel
III
Persiapan sampel gigi P
Pembuatan Gel kitosan
nanopartikel
Penanaman sampel gigi P dalam pipa paralon
ASP 10 gr
grinding jar
Aplikasi Bahan Uji yang dibagi menjadi 3 kelompok,
masing-masing kelompok terdiri dari 8 sampel
1 gr kitosan + 100 ml
larutan asam asetat 1%
Diaduk pada kecepatan
200 rpm (± 30 menit)
Gel kitosan.
Kelompok III
Gel kitosan dimasukkan
dalam ultrasonic bath
Preparasi kavitas profunda klas I
ASP 10 gr
grinding jar
Planetary Ball Mills ( Retsch, PM
200), 2 jam, kecepatan 250 rpm
Kelompok I
Kelompok II
MTA
SIKMR
ASP Nanopartikel 20 gr
ASP nano + kitosan
molekul tinggi nano
Gel Kitosan blangkas
Sampel gigi P di bagi dua pada arah bukal-lingual dan di potong
pada daerah servikal gigi
Sampel dilakukan pemeriksaan dengan SEM-EDX
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Lampiran 2
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Lampiran 3
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Lampiran 4
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Lampiran 5
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Lampiran 6
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Lampiran 7
UJI NORMALITAS DATA
b,c
Tests of Normality
a
Kolmogorov-Smirnov
kelompok
C
O
*
.930
8
.515
.200
*
.921
8
.438
8
.095
.815
8
.051
8
*
.957
8
.779
*
.897
8
.274
*
.200
SIKMR
.189
8
MTA
.268
8
.200
.200
MTA
.218
8
.200
.873
8
.162
ASP + KITOSAN
.284
8
.056
.902
8
.304
8
*
.965
8
.859
*
.936
8
.574
*
.919
8
.422
*
.912
8
.368
*
.907
8
.334
*
.873
8
.160
*
MTA
MTA
ASP + KITOSAN
.148
.201
.173
.181
.204
.226
8
8
8
8
8
.200
.200
.200
.200
.200
.200
SIKMR
.137
8
.200
.964
8
.844
MTA
.306
8
.026
.745
8
.057
8
*
.897
8
.274
*
ASP + KITOSAN
.209
.200
SIKMR
.159
8
.200
.977
8
.949
MTA
.292
8
.044
.913
8
.372
8
*
.877
8
.176
*
.908
8
.343
*
ASP + KITOSAN
SIKMR
Si
.100
8
SIKMR
Ca
8
.198
.235
Sig.
.852
ASP + KITOSAN
.149
df
*
.200
ASP + KITOSAN
P
Statistic
8
SIKMR
N
Sig.
.209
SIKMR
Na
df
MTA
ASP + KITOSAN
F
Statistic
Shapiro-Wilk
.215
.238
8
.200
.200
MTA
.092
8
.200
.993
8
.998
ASP + KITOSAN
.303
8
.030
.769
8
.053
8
*
.848
8
.091
SIKMR
.238
.200
Universitas Sumatera Utara
Al
MTA
.172
8
.200
*
.954
8
.755
ASP + KITOSAN
.252
8
.143
.906
8
.328
SIKMR
.242
8
.185
.876
8
.172
a. Lilliefors Significance Correction
*. This is a lower bound of the true significance.
b. Bi is constant when kelompok = ASP + KITOSAN. It has been omitted.
c. Bi is constant when kelompok = SIKMR. It has been omitted.
Descriptive Statistics
N
Minimum
Bi
8
Valid N (listwise)
8
.80
Maximum
1.32
Mean
Std. Deviation
1.0950
.19849
Universitas Sumatera Utara
ONE WAY
Descriptives
C
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8 80.4450
1.14909
.40626
79.4843
81.4057
79.65
83.22
ASP +
8 67.6388
1.13839
.40248
66.6870
68.5905
65.90
69.86
2.9738
.19770
.06990
2.8085
3.1390
2.62
3.20
24 50.3525
34.64826
7.07255
35.7218
64.9832
2.62
83.22
KITOSAN
SIKMR
8
Total
Test of Homogeneity of Variances
C
Levene Statistic
2.138
df1
df2
2
Sig.
21
.143
ANOVA
C
Sum of Squares
Between Groups
27592.952
Df
Mean Square
2
13796.476
F
Sig.
15586.827
.000
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*Within Groups
Total
18.588
21
27611.539
23
.885
Post Hoc Tests
Multiple Comparisons
C
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
12.80625
SIKMR
77.47125
ASP + KITOSAN MTA
Std. Error
Sig.
Lower Bound
Upper Bound
*
.47041
.000
11.8280
13.7845
*
.47041
.000
76.4930
78.4495
*
.47041
.000
-13.7845
-11.8280
*
.47041
.000
63.6867
65.6433
*
.47041
.000
-78.4495
-76.4930
*
.47041
.000
-65.6433
-63.6867
-12.80625
SIKMR
SIKMR
Difference (I-J)
64.66500
MTA
-77.47125
ASP + KITOSAN
-64.66500
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
O
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
3.4013
.65743
.23244
2.8516
3.9509
2.77
4.86
ASP +
8
10.5562
.53984
.19086
10.1049
11.0076
9.77
11.66
8
21.8663
.28874
.10208
21.6249
22.1076
21.47
22.32
24
11.9412
7.78095
1.58828
8.6556
15.2269
2.77
22.32
KITOSAN
SIKMR
Total
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Test of Homogeneity of Variances
O
Levene Statistic
df1
.587
df2
Sig.
2
21
.565
ANOVA
O
Sum of Squares
Between Groups
Mean Square
F
1386.844
2
693.422
5.649
21
.269
1392.493
23
Within Groups
Total
Df
Sig.
2577.748
.000
Post Hoc Tests
Multiple Comparisons
O
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
SIKMR
ASP + KITOSAN MTA
Difference (I-J)
Std. Error
Sig.
Lower Bound
Upper Bound
*
.25933
.000
-7.6943
-6.6157
*
.25933
.000
-19.0043
-17.9257
*
.25933
.000
6.6157
7.6943
-7.15500
-18.46500
7.15500
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SIKMR
SIKMR
*
.25933
.000
-11.8493
-10.7707
*
.25933
.000
17.9257
19.0043
*
.25933
.000
10.7707
11.8493
-11.31000
MTA
18.46500
ASP + KITOSAN
11.31000
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
F
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.7338
.52334
.18503
.2962
1.1713
.12
1.40
ASP +
8
1.7913
.40951
.14478
1.4489
2.1336
1.14
2.12
8
7.4013
1.49124
.52723
6.1545
8.6480
5.00
8.76
24
3.3088
3.12155
.63718
1.9906
4.6269
.12
8.76
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
F
Levene Statistic
14.728
df1
df2
2
Sig.
21
.000
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ANOVA
F
Sum of Squares
Between Groups
Within Groups
Total
Df
Mean Square
F
205.456
2
102.728
18.658
21
.888
224.113
23
Sig.
115.625
.000
Post Hoc Tests
Multiple Comparisons
F
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
-1.05750
SIKMR
-6.66750
ASP + KITOSAN
MTA
SIKMR
SIKMR
MTA
ASP + KITOSAN
(I-J)
Std. Error
Sig.
Lower Bound
Upper Bound
*
.47129
.036
-2.0376
-.0774
*
.47129
.000
-7.6476
-5.6874
*
.47129
.036
.0774
2.0376
*
.47129
.000
-6.5901
-4.6299
*
.47129
.000
5.6874
7.6476
*
.47129
.000
4.6299
6.5901
1.05750
-5.61000
6.66750
5.61000
*. The mean difference is significant at the 0.05 level.
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Oneway
Descriptives
Na
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.4662
.13201
.04667
.3559
.5766
.23
.65
ASP +
8
1.3263
.18731
.06622
1.1697
1.4828
1.04
1.55
8
2.4463
.34247
.12108
2.1599
2.7326
2.05
2.92
24
1.4129
.85872
.17529
1.0503
1.7755
.23
2.92
F
Sig.
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
Na
Levene Statistic
5.342
df1
df2
2
Sig.
21
.013
ANOVA
Na
Sum of Squares
Between Groups
Within Groups
Total
df
Mean Square
15.772
2
7.886
1.189
21
.057
16.960
23
139.331
.000
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Post Hoc Tests
Multiple Comparisons
Na
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
Difference (I-J)
MTA
ASP + KITOSAN
Upper Bound
.000
-1.1074
-.6126
*
.11895
.000
-2.2274
-1.7326
*
.11895
.000
.6126
1.1074
*
.11895
.000
-1.3674
-.8726
*
.11895
.000
1.7326
2.2274
*
.11895
.000
.8726
1.3674
.86000
SIKMR
Lower Bound
.11895
-1.98000
ASP + KITOSAN MTA
Sig.
*
-.86000
SIKMR
SIKMR
Std. Error
-1.12000
MTA
1.98000
ASP + KITOSAN
1.12000
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
N
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.3737
.15611
.05519
.2432
.5043
.19
.61
ASP +
8
2.5388
.22681
.08019
2.3491
2.7284
2.24
2.89
8 24.8075
2.86019
1.01123
22.4163
27.1987
21.88
30.18
KITOSAN
SIKMR
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Descriptives
N
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.3737
.15611
.05519
.2432
.5043
.19
.61
ASP +
8
2.5388
.22681
.08019
2.3491
2.7284
2.24
2.89
8 24.8075
2.86019
1.01123
22.4163
27.1987
21.88
30.18
11.39166
2.32531
4.4297
14.0503
.19
30.18
KITOSAN
SIKMR
Total
24
9.2400
ANOVA
N
Sum of Squares
Between Groups
Within Groups
Total
Df
Mean Square
2926.914
2
1463.457
57.795
21
2.752
2984.709
23
F
531.748
Sig.
.000
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Post Hoc Tests
Multiple Comparisons
N
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
(I-J)
MTA
ASP + KITOSAN
SIKMR
Upper Bound
.016
-3.8900
-.4400
*
.82948
.000
-26.1588
-22.7087
*
.82948
.016
.4400
3.8900
*
.82948
.000
-23.9938
-20.5437
*
.82948
.000
22.7087
26.1588
*
.82948
.000
20.5437
23.9938
2.16500
SIKMR
Lower Bound
.82948
-24.43375
MTA
Sig.
*
-2.16500
SIKMR
ASP + KITOSAN
Std. Error
-22.26875
MTA
24.43375
ASP + KITOSAN
22.26875
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
P
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
3.3888
.35430
.12526
3.0925
3.6850
2.63
3.73
ASP +
8
1.6438
.31296
.11065
1.3821
1.9054
1.02
1.98
8 16.4513
1.72484
.60982
15.0092
17.8933
13.35
18.85
KITOSAN
SIKMR
Universitas Sumatera Utara
Total
24
7.1613
6.82138
1.39241
4.2808
10.0417
1.02
18.85
Test of Homogeneity of Variances
P
Levene Statistic
df1
7.589
df2
2
Sig.
21
.003
ANOVA
P
Sum of Squares
Between Groups
Mean Square
F
1047.829
2
523.915
22.390
21
1.066
1070.219
23
Within Groups
Total
df
Sig.
491.395
.000
Post Hoc Tests
Multiple Comparisons
P
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
Difference (I-J)
Std. Error
*
1.74500
.51628
Sig.
.003
Lower Bound
.6713
Upper Bound
2.8187
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SIKMR
ASP + KITOSAN MTA
.51628
.000
-14.1362
-11.9888
*
.51628
.003
-2.8187
-.6713
*
.51628
.000
-15.8812
-13.7338
*
.51628
.000
11.9888
14.1362
*
.51628
.000
13.7338
15.8812
-1.74500
SIKMR
SIKMR
*
-13.06250
-14.80750
MTA
13.06250
ASP + KITOSAN
14.80750
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
Ca
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
7.9413
.69372
.24527
7.3613
8.5212
7.35
9.38
ASP +
8
1.8775
.40138
.14191
1.5419
2.2131
1.41
2.41
8
5.6463
.16071
.05682
5.5119
5.7806
5.48
5.93
24
5.1550
2.59305
.52930
4.0601
6.2499
1.41
9.38
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
Ca
Levene Statistic
5.066
df1
df2
2
Sig.
21
.016
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ANOVA
Ca
Sum of Squares
Between Groups
Within Groups
Total
Df
Mean Square
149.972
2
74.986
4.677
21
.223
154.649
23
F
Sig.
336.676
.000
Post Hoc Tests
Multiple Comparisons
Ca
LSD
95% Confidence Interval
Mean
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
6.06375
SIKMR
2.29500
ASP + KITOSAN MTA
SIKMR
Difference (I-J) Std. Error
Lower Bound
Upper Bound
*
.23597
.000
5.5730
6.5545
*
.23597
.000
1.8043
2.7857
*
.23597
.000
-6.5545
-5.5730
*
.23597
.000
-4.2595
-3.2780
*
.23597
.000
-2.7857
-1.8043
*
.23597
.000
3.2780
4.2595
-6.06375
SIKMR
-3.76875
MTA
-2.29500
ASP + KITOSAN
Sig.
3.76875
*. The mean difference is significant at the 0.05 level.
Oneway
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Descriptives
Si
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
3.3775
.27855
.09848
3.1446
3.6104
3.03
3.78
ASP +
8 12.1463
.81054
.28657
11.4686
12.8239
11.30
13.29
8
5.2913
.19577
.06922
5.1276
5.4549
5.01
5.57
24
6.9383
3.87595
.79117
5.3017
8.5750
3.03
13.29
KITOSAN
SIKMR
Total
Test of Homogeneity of Variances
Si
Levene Statistic
15.002
df1
df2
2
Sig.
21
.000
ANOVA
Si
Sum of Squares
Between Groups
Within Groups
Total
df
Mean Square
340.119
2
170.059
5.410
21
.258
345.529
23
F
660.092
Sig.
.000
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Post Hoc Test
Multiple Comparisons
Si
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
(I-J)
MTA
ASP + KITOSAN
8.76875
SIKMR
6.85500
ASP + KITOSAN MTA
SIKMR
Std. Error
Sig.
Lower Bound
Upper Bound
*
.25379
.000
-9.2965
-8.2410
*
.25379
.000
-2.4415
-1.3860
*
.25379
.000
8.2410
9.2965
*
.25379
.000
6.3272
7.3828
*
.25379
.000
1.3860
2.4415
*
.25379
.000
-7.3828
-6.3272
1.91375
SIKMR
6.85500
MTA
1.91375
ASP + KITOSAN
8.76875
*. The mean difference is significant at the 0.05 level.
Oneway
Descriptives
Al
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.4813
.20904
.07391
.3065
.6560
.24
.89
ASP +
8
.1837
.05317
.01880
.1393
.2282
.10
.26
8 13.0800
.88494
.31287
12.3402
13.8198
11.18
14.11
KITOSAN
SIKMR
Universitas Sumatera Utara
Descriptives
Al
95% Confidence Interval for
Mean
Std.
N
Mean
Deviation
Std. Error Lower Bound Upper Bound Minimum Maximum
MTA
8
.4813
.20904
.07391
.3065
.6560
.24
.89
ASP +
8
.1837
.05317
.01880
.1393
.2282
.10
.26
8 13.0800
.88494
.31287
12.3402
13.8198
11.18
14.11
1.25746
1.9804
7.1829
.10
14.11
KITOSAN
SIKMR
Test of Homogeneity of Variances
Al
Levene Statistic
df1
df2
5.026
Total
2
24
Sig.
21
4.5817
.016
6.16026
ANOVA
Al
Sum of Squares
Between Groups
Within Groups
Df
Mean Square
867.014
2
433.507
5.807
21
.277
F
Sig.
1567.574
.000
Universitas Sumatera Utara
Total
872.822
23
Post Hoc Tests
Multiple Comparisons
Al
LSD
95% Confidence Interval
Mean Difference
(I) kelompok
(J) kelompok
MTA
ASP + KITOSAN
SIKMR
ASP + KITOSAN
MTA
SIKMR
SIKMR
(I-J)
Std. Error
Sig.
Lower Bound
Upper Bound
.29750
.26294
.271
-.2493
.8443
-12.59875
*
.26294
.000
-13.1456
-12.0519
-.29750
.26294
.271
-.8443
.2493
*
.26294
.000
-13.4431
-12.3494
*
.26294
.000
12.0519
13.1456
*
.26294
.000
12.3494
13.4431
-12.89625
MTA
12.59875
ASP + KITOSAN
12.89625
*. The mean difference is significant at the 0.05 level.
Universitas Sumatera Utara
Lampiran 8
MINERAL TRIOXIDE AGGREGATE ( MTA )
Universitas Sumatera Utara
MINERAL TRIOXIDE AGGREGATE ( MTA )
Universitas Sumatera Utara
ABU SEKAM PADI DENGAN KITOSAN
ABU SEKAM PADI DENGAN KITOSAN
Universitas Sumatera Utara
Universitas Sumatera Utara
SEMEN IONOMER KACA MODIFIKASI RESIN (SIKMR)
Universitas Sumatera Utara
SEMEN IONOMER KACA MODIFIKASI RESIN (SIKMR)
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Lampiran 9
HASIL UJI XRD ABU SEKAM PADI
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara