Keterangan : Kodok Purwodadi : Kodok Demak : Kodok Semarang

  

Perpustakaan Unika

  Perpustakaan Unika

Lampiran 1. Jadwal Pengambilan Sampel

  Bulan Febuari 2007

  Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 Pengambilan dan pengeringan sampel Powder sampel dan kadar air Destruksi sampel Bulan

  Maret 2007 Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 Pengambilan dan pengeringan sampel Powder sampel dan kadar air Destruksi sampel

  Perpustakaan Unika

  Bulan Apr-07

  Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 Pengambilan dan pengeringan sampel Powder sampel dan kadar air Destruksi sampel Bulan

  Mei-07 Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 Pengambilan dan pengeringan sampel Powder sampel dan kadar air Destruksi sampel

  Keterangan : Kodok Purwodadi : Kodok Demak : Kodok Semarang

  Perpustakaan Unika Lampiran 2. Peta Lokasi Pengambilan Sampel Kode Berat cawan

  Sampel basah Berat cawan dan sampel basah

  Sampel kering Berat cawan dan sampel kering Berat awal

  Berat akhir Kadar air

  Paha 1 40,236 21,159 61,395 5,431 45,667 21,159 5,431 74,3324 Paha 2 40,253 35,63 75,883 6,703 46,956 35,63 6,703 81,1872 Paha 3 39,014 30,102 69,116 5,6 44,614 30,102 5,6 81,3966 Paha 4 46,769 31,375 78,144 6,134 52,903 31,375 6,134 80,4494 Paha 5 31,012 27,745 58,757 5,438 36,45 27,745 5,438 80,4001 Sisa 1 39,625 25,595 65,22 4,878 44,503 25,595 4,878 80,9416 Sisa 2 44,992 32,33 77,322 6,148 51,14 32,33 6,148 80,9836 Sisa 3 44,67 30,109 74,779 5,497 50,167 30,109 5,497 81,743 Sisa 4 43,74 33,741 77,481 6,778 50,518 33,741 6,778 79,9117 Sisa 5 33,521 28,777 62,298 5,32 38,841 28,777 5,32 81,513 Jeroan 1 47,772 2,364 50,136 0,474 48,246 2,364 0,474 79,9492 Jeroan 2 32,284 2,536 34,82 0,404 32,688 2,536 0,404 84,0694 Jeroan 3 42,297 2,712 45,009 0,508 42,805 2,712 0,508 81,2684 Jeroan 4 47,184 2,706 49,89 0,51 47,694 2,706 0,51 81,153 Jeroan 5 19,902 2,26 22,162 0,472 20,374 2,26 0,472 79,115 Avarage 20,6094 60,1608 43,57106667 20,6094 80,5609

  Perpustakaan Unika

Lampiran 3. Hasil Pengukuran kadar air dan AAS Pengukuran Kadar air Kodok (Pakai Tulang) Semarang

  Kode Berat cawan

  Sampel basah Berat cawan dan sampel basah

  Sampel kering Berat cawan dan sampel kering Berat awal

  Berat akhir Kadar air

  Paha 1 31,169 17,876 49,045 2,926 34,095 17,876 2,926 83,6317 Paha 2 33,548 15,515 49,063 2,493 36,041 15,515 2,493 83,9317 Paha 3 21,973 17,479 39,452 2,885 24,858 17,479 2,885 83,4945 Sisa 1 27,54 5,382 32,922 0,739 28,279 5,382 0,739 86,269 Sisa 2 32,695 5,231 37,926 0,718 33,413 5,231 0,718 86,2741 Sisa 3 19,315 5,142 24,457 0,683 19,998 5,142 0,683 86,7172 Jeroan 1 26,354 2,255 28,609 0,452 26,806 2,255 0,452 79,9557 Jeroan 3 29,855 2,902 32,757 0,539 30,394 2,902 0,539 81,4266

  Perpustakaan Unika

Pengukuran Kadar air Kodok (Tanpa Tulang) Semarang

Pengukuran Logam Kodok (Pakai Tulang) Semarang

  5 Sisa 3 1,706 5 81,743 0,44 1,114 0,2033 13,43 33,37 6,092 1,8 26,38 4,816

  Perpustakaan Unika

  11,29 2,1622 73,71 14,18 34,15 6,479

  169,4 32,433 1106 212,7 512,2 97,18 Avarage

  0,6 Sum

  5 Blanko 0,06

  5 Jeroan 5 0,358 5 79,115 2,24 30,45 6,3588 2,462 34,39 7,181 0,8 55,87 11,67

  5 Jeroan 4 0,314 5 81,153 3,31 51,59 9,7236 3,663 46,1 8,688 1,1 87,58 16,51

  5 Jeroan 3 0,302 5 81,268 3,26 11,42 2,1399 2,547 9,321 1,746 1 82,78 15,51

  5 Jeroan 2 0,345 5 84,069 3,2 22,46 3,5786 3,119 8,014 1,277 0,7 50,72 8,081

  5 Jeroan 1 0,31 5 79,949 2,92 44,68 8,9582 3,309 53,37 10,7 0,7 56,45 11,32

  5 Sisa 5 1,76 5 81,513 1,3 3,125 0,5777 10,72 304,5 56,3 10 2,3 32,67 6,04

  5 Sisa 4 1,7 5 79,912 0,69 1,765 0,3545 10,06 295,9 59,44 10 2,2 32,35 6,499

  Kode Berat distruksi Volume dilution

  Kadar air Cu (AAS)

  5 Sisa 2 1,776 5 80,984 0,37 0,732 0,1392 9,34 263

  5 Paha 5 1,724 5 80,4 0,21 0,435 0,0853 2,59 7,512 1,472 1,4 2,32 0,455 Sisa 1 1,713 5 80,942 0,39 0,788 0,1502 12,05 32,22 6,141 1,8 26,27 5,007

  5 Paha 4 1,669 5 80,449 0,16 0,479 0,0937 2,95 8,838 1,728 1,1 16,48 3,221

  Paha 1 1,682 5 1 74,332 0,08 0,059 0,0153 1,143 3,398 0,872 0,9 0,892 0,229 Paha 2 1,722 5 10 81,187 0,02 0,058 0,0109 0,741 2,152 0,405 2,1 4,355 0,819 Paha 3 1,688 5 81,397 0,08 0,237 0,0441 1,219 3,611 0,672 0,7 10,37 1,929

  Zn sampel basah Dilution

  Kadar Zn

  Zn (AAS)

  Fe sampel basah Dilution

  Kadar Fe

  Fe (AAS)

  Cu sampel basah

  Kadar Cu

  50 10 1,9 26,75 5,086

Kodok (Tanpa Tulang) Semarang

  5 Paha 3 1,184 5 83,494 1,34 5,659 0,934 2,044 146 24,1 0,6 12,669 24,1

  Perpustakaan Unika

  75,31 13,629 616,9 93 178,92 93,01 Avarage 8,367 1,5143 68,54 19,879 10,33

  0,6 Sum

  5 Jeroan 3 0,315 5 81,427 0,07 0,159 0,0295 0,768 12,19 2,26 0,9 4,7619 2,264 Blanko 0,06

  5 Jeroan 1 0,319 5 79,956 1,65 24,92 4,9954 2,566 40,22 8,06 0,6 47,022 8,062

  5 Sisa 3 0,521 5 86,717 0,15 0,864 0,1147 6,308 60,54 8,04 0,5 23,992 8,041

  5 Sisa 1 0,525 5 86,269 0,09 0,857 0,1177 2,957 246,4 33,8 1,1 4,7619 33,84 Sisa 2 0,531 5 86,274 0,2 1,883 0,2585 7,677 72,29 9,92 0,6 28,249 9,922

  Kode Berat distruksi Volume

  Kadar air Cu (AAS)

  Zn sampel basah Dilution

  Kadar Zn

  Zn (AAS)

  Fe sampel basah

  Kadar Fe

  Fe (AAS)

  Cu sampel basah

  Kadar Cu

  Paha 1 1,158 5 83,632 0,12 0,259 0,0424 1,011 3,064 0,5 1,5 3,886 0,501 Paha 2 1,132 5 83,932 0,11 0,221 0,0355 2,14 4,163 0,67 0,6 13,251 0,669

  Kode Berat cawan

  Sampel basah Berat cawan dan sampel basah

  Sampel kering Berat cawan dan sampel kering

  Kadar air Paha 1 42,29 42,686 84,976 7,403 49,693 82,6571 Paha 2 60,502 42,27 102,772 7,471 67,973 82,3255 Paha 3 44,681 42,456 87,137 7,455 52,136 82,4406 Paha 4 45,548 44,721 90,269 7,625 53,173 82,9498 Paha 5 50,077 45,472 95,549 8,62 58,697 81,0433 Sisa 1 39,63 32,418 72,048 5,985 45,615 81,538 Sisa 2 32,663 33,812 66,475 6,117 38,78 81,9088 Sisa 4 43,745 30,304 74,049 5,544 49,289 81,7054 Sisa 5 33,404 19,855 53,259 3,35 36,754 83,1277 Jeroan 1 47,779 2,174 49,953 0,384 48,163 82,3367 Jeroan 2 32,288 1,504 33,792 0,248 32,536 83,5106 Jeroan 3 42,304 1,117 43,421 0,18 42,484 83,8854 Jeroan 4 47,194 1,277 48,471 0,243 47,437 80,971 Jeroan 5 19,904 1,796 21,7 0,289 20,193 83,9087 Avarage 24,8093

  Perpustakaan Unika

Pengukuran Kadar Air Kodok (Pakai Tulang) Demak

  Kode Berat cawan

  Sampel basah Berat cawan dan sampel basah

  Sampel kering Berat cawan dan sampel kering Kadar air

  Paha 1 31,083 11,151 42,234 1,72 32,803 84,5754 Paha 2 33,449 12,227 45,676 2,015 35,464 83,5201 Paha 3 21,9 11,905 33,805 1,901 23,801 84,0319 Sisa 1 27,509 4,564 32,073 0,522 28,031 88,5627 Sisa 2 44,998 4,429 49,427 0,696 45,694 84,2854 Sisa 3 19,304 4,772 24,076 0,651 19,955 86,3579 Jeroan 1 26,359 1,297 27,656 0,233 26,592 82,0355 Jeroan 3 29,857 2,544 32,401 0,586 30,443 76,9654

  Perpustakaan Unika

Pengukuran Kadar Air Kodok (Tanpa Tulang) Demak

Pengukuran Logam Kodok (Pakai Tulang) Demak

  2 Sisa 2 1,713 5 81,9088 0,09 0,0876 0,0158 2,6 6,1588 1,1142 0,9 13,1349 2,3763

  Perpustakaan Unika

  Avarage 16,346 2,7893 19,72 3,3747 38,8825 6,7275

  Sum 245,19 41,84 295,79 50,621 583,237 100,91

  5 Blanko 0,06 0,6

  5 Jeroan 5 0,258 5 83,9087 2,66 51,55 8,2951 3,15 61,047 9,8232 0,8 77,5194 12,474

  5 Jeroan 4 0,248 5 80,971 2,97 58,669 11,164 3,47 69,96 13,313 0,9 90,7258 17,264

  5 Jeroan 3 0,183 5 83,8854 2,09 57,104 9,202 3,52 51,366 8,2774 0,6 81,9672 13,209

  5 Jeroan 2 0,253 5 83,5106 2,59 50 8,2447 3,85 76,087 12,546 1,1 108,696 17,923

  5 Jeroan 1 0,393 5 82,3367 1,99 24,555 4,3372 4,21 16,158 2,854 1,1 69,9746 12,36

  5 Sisa 5 1,58 5 83,1277 0,14 0,2532 0,0427 0,55 0,538 0,0908 1,2 18,9873 3,2036

  5 Sisa 4 1,59 5 81,7054 0,13 0,4088 0,0748 0,58 0,0943 0,0173 0,9 14,1509 2,5889

  5 Sisa 3 1,654 5 81,6203 0,2 0,6046 0,1111 0,94 0,9976 0,1834 1,9 28,7183 5,2783

  Kode Berat distruksi Volume

  Kadar air Cu (AAS)

  2 Paha 5 1,655 5 81,0433 0,17 0,5136 0,0974 0,76 2,2961 0,4353 1,4 21,148 4,009

  5 Paha 4 1,684 5 82,9498 0,1 0,1188 0,0202 0,67 1,9893 0,3392 1,3 7,71971 1,3162

  5 Paha 3 1,721 5 82,4406 0,09 0,2615 0,0459 0,42 1,2202 0,2143 0,8 11,6212 2,0406

  5 Paha 2 1,737 5 82,3255 0,17 0,4893 0,0865 1,01 2,9073 0,5139 1,1 15,8319 2,7982

  Paha 1 1,681 5 82,6571 0,16 0,2974 0,0516 0,58 1,7252 0,2992 1,1 16,3593 2,8372

  Zn sampel basah Dilution

  Kadar Zn

  Zn (AAS)

  Fe sampel basah

  Kadar Fe

  Fe (AAS)

  Cu sampel basah

  Kadar Cu

  5 Sisa 1 1,646 5 81,538 0,09 0,2734 0,0505 1,07 3,2503 0,6001 1,1 6,68287 1,2338

  Perpustakaan Unika

Kodok (tanpa Tulang) Demak

  Cu Zn

  Berat Kadar Cu Kadar sampel Fe Kadar Fe sampel Zn Kadar sampel Kode distruksi Volume air (AAS) Cu basah (AAS) Fe basah (AAS) Zn basah Dilution Paha 1 1,482 5 84,5754 0,34 0,9447 0,1457 2,61 8,8057 1,3582 0,7 11,8084 1,8214

  5 Paha 2 1,461 5 83,5201 0,47 1,4031 0,2312 2,48 8,4873 1,3987 0,8 13,6893 2,256

  5 Paha 3 1,541 5 84,0319 0,53 1,7197 0,2746 0,49 1,5899 0,2539 0,8 12,9786 2,0724

  5 Sisa 1 0,521 5 88,5627 0,16 1,5355 0,1756 0,61 5,8541 0,6696 1,2 57,5816 6,5858

  5 Sisa 2 0,55 5 84,2854 0,21 1,9091 0,3 0,55 5 0,7857 1 45,4545 7,143

  5 Sisa 3 0,51 5 86,3579 0,1 0,9804 0,1337 0,38 3,7255 0,5082 1 49,0196 6,6873

  5 Jeroan 1 0,231 5 82,0355 3,45 74,675 13,415 2,94 63,636 11,432 0,8 86,5801 15,554

  5 Jeroan 3 0,25 5 76,9654 1,76 35,2 8,1082 1,64 32,8 7,5553 1 100 23,035

  5 Blanko 0,06 0,6

  Sum 752,379 8,47 144,45 27,467 221,63 40,432 476,033 82,916

  45 avarage 16,05 3,0519 24,625 4,4924 52,8925 9,2129

  5 Kode Berat cawan

  Sampel basah Berat cawan dan sampel basah

  Sampel kering Berat cawan dan sampel kering

  Kadar air Paha 1 40,226 40,566 80,792 10,263 50,489 74,7005 Paha 2 40,244 47,786 88,03 10,374 50,618 78,2907 Paha 3 44,653 44,462 89,115 10,341 54,994 76,7419 Paha 4 46,759 48,157 94,916 11,68 58,439 75,746 Paha 5 30,812 43,078 73,89 9,371 40,183 78,2464 Sisa 1 39,617 43,609 83,226 9,395 49,012 78,4563 Sisa 2 44,983 42,706 87,689 8,37 53,353 80,4009 Sisa 4 43,73 44,016 87,746 9,006 52,736 79,5393 Sisa 5 33,38 45,687 79,067 9,415 42,795 79,3924 Jeroan 1 47,765 3,322 51,087 0,605 48,37 81,7881 Jeroan 2 32,28 2,754 35,034 0,517 32,797 81,2273 Jeroan 3 42,29 2,856 45,146 0,512 42,802 82,0728 Jeroan 4 47,176 2,589 49,765 0,479 47,655 81,4986 Jeroan 5 19,891 2,045 21,936 0,389 20,28 80,978

  Perpustakaan Unika

Pengukuran Kadar Air Kodok (Pakai Tulang) Purwodadi

  Kode Berat cawan

  Sampel basah Berat cawan dan sampel basah

  Sampel kering Berat cawan dan sampel kering

  Kadar air Paha 1 31,054 11,613 42,667 2,112 33,166 81,8135 Paha 2 33,368 11,857 45,225 2,246 35,614 81,0576 Paha 3 21,881 12,512 34,393 2,538 24,419 79,7155 Sisa 1 27,491 3,655 31,146 0,5 27,991 86,3201 Sisa 2 32,646 3,048 35,694 0,431 33,077 85,8596 Sisa 3 19,29 2,706 21,996 0,375 19,665 86,1419 Jeroan 1 26,345 1,611 27,956 0,27 26,615 83,2402 Jeroan 3 29,845 1,791 31,636 0,305 30,15 82,9704

  Perpustakaan Unika

Pengukuran Kadar Air Kkodok (Tanpa Tulang) Purwodadi

Pengukuran Logam Kodok (Pakai Tulang) Purwodadi

  5 Sisa 2 1,649 5 80,4009 0,44 1,152 0,2258 8,41 23,893 4,6829 0,8 24,25713 4,7542

  Perpustakaan Unika

  Avarage 10,53 1,9615 30,984 5,8459 34,54463 6,7031

  Sum 157,9 29,422 464,77 87,688 518,1694 100,55

  5 Blanko 0,06 0,6

  5 Jeroan 5 0,314 5 80,978 1,25 19,9 3,7862 5,49 87,42 16,629 0,8 63,69427 12,116

  5 Jeroan 4 0,335 5 81,4986 1,76 25,37 4,6944 7,53 112,39 20,793 0,9 67,16418 12,426

  5 Jeroan 3 0,315 5 82,0728 2 31,75 5,6912 6,87 59,683 10,699 0,8 63,49206 11,382

  5 Jeroan 2 0,356 5 81,2273 3,89 53,79 10,098 9,32 89,045 16,716 1,2 84,26966 15,82

  10 Jeroan 1 0,309 5 81,7881 1,27 19,58 3,5658 5,84 34,628 6,3064 0,9 72,81553 13,261

  5 Sisa 5 1,69 5 79,3924 0,45 1,154 0,2378 0,41 1,213 0,25 1 29,5858 6,0969

  10 Sisa 4 1,652 5 79,5393 0,24 0,726 0,1486 6,5 16,858 3,4493 1 15,13317 3,0964

  10 Sisa 3 1,735 5 80,7503 0,43 1,239 0,2385 8,5 22,882 4,4047 0,6 17,29107 3,3285

  Kode Berat distruksi Volume

  Kadar air Cu (AAS)

  5 Paha 5 1,729 5 78,2464 0,26 0,752 0,1636 1,02 2,9497 0,6417 1,4 20,24291 4,4036

  5 Paha 4 1,741 5 75,746 0,1 0,115 0,0279 0,5 1,436 0,3483 0,6 8,615738 2,0897

  5 Paha 3 1,661 5 76,7419 0,22 0,662 0,154 0,86 2,5888 0,6021 1,2 18,06141 4,2007

  5 Paha 2 1,725 5 78,2907 0,17 0,493 0,107 0,46 1,3333 0,2895 0,7 10,14493 2,2024

  Paha 1 1,725 5 74,7005 0,17 0,319 0,0807 0,51 1,4783 0,374 0,6 8,695652 2,2

  Zn sampel basah Dilution

  Zn (AAS) Kadar Zn

  Fe sampel basah

  Kadar Fe

  Fe (AAS)

  Cu sampel basah

  Kadar Cu

  5 Sisa 1 1,7 5 78,4563 0,32 0,941 0,2028 2,77 6,9706 1,5017 1 14,70588 3,1682

  Perpustakaan Unika

Kodok (Tanpa Tulang) Purwodadi

  Cu Fe Zn Berat Kadar Cu Kadar sampel Fe Kadar sampel Zn sampel

  Kode distruksi Volume air (AAS) Cu basah (AAS) Fe basah (AAS) Kadar Zn basah Dilution Paha 1 1,13 5 81,8135 0,14 0,354 0,0644 1,63 7,2124 1,3117 1,9 5,752212 1,0461 Paha 2 1,185 5 81,0576 0,09 0,38 0,0719 0,4 1,6878 0,3197 1,6 6,751055 1,2788 Paha 3 1,124 5 79,7155 0,18 0,801 0,1624 0,53 2,3577 0,4782 0,9 4,003559 0,8121

  5 Sisa 1 0,512 5 86,3201 0,18 1,758 0,2405 0,56 5,4688 0,7481 0,7 6,835938 0,9351 Sisa 2 0,514 5 85,8596 0,17 1,654 0,2338 0,93 9,0467 1,2792 0,6 5,836576 0,8253

  5 Sisa 3 0,499 5 86,1419 0,1 1,002 0,1389 0,64 6,4128 0,8887 0,5 5,01002 0,6943

  5 Jeroan 1 0,219 5 83,2402 1,57 35,84 6,0075 3,7 84,475 14,158 0,8 18,26484 3,0611 Jeroan 3 0,205 5 82,9704 3,78 92,2 15,7 3,11 75,854 12,918 0,8 19,5122 3,3228 Blanko 0,06

  0,6 Sum

  172,8 28,2 14,48 260,55 41,883 92,51434 14,93 Avarage

  19,2 3,1334 28,95 4,6537 10,27937 1,6589

  49 Perpustakaan Unika

  Lampiran 4. Hasil Perhitungan MCL MCL berdasarkan Perhitungan Cu ULSR pria = 12 mg/hari ULSR wanita =10mg/hari = 12mg x 7 = 10mg x 7 = 84 mg/minggu = 70mg/minggu MCL Cu untuk pria:

  84 mg / min ggu Semarang = 2 , 162 µ g / g = 0,04g/minggu

  84 mg / min ggu Demak = 2 , 789 g / g µ

  = 0,03g/minggu 84 mg / min ggu Purwodadi = 1 , 961 µ g / g = 0,04g/minggu MCL Cu untuk wanita:

  70 mg / min ngu Semarang = 2 , 162 µ g / g = 0,03g/minggu

  70 mg / min ggu Demak = 2 , 789 µ g / g = 0,02g/minggu

  50 Perpustakaan Unika

  MCL berdasarkan perhitungan Zn ULSR pria = 45mg/hari ULSR wanita = 35mg/hari = 45mg x7 = 35mg x7 = 315mg/minggu = 245mg/minggu MCL Zn pria: 315 mg / min ggu Semarang = 6 , 478 µ g / g = 0,04g/minggu 315 mg / min ggu Demak = 6 , 727 g / g

  µ = 0,05g/minggu 315 mg / min ggu Purwodadi =

  6 , 703 µ g / g = 0,05g/minggu MCL Zn wanita: 245 mg / min ggu Semarang = 6 , 478 µ g / g = 0,03g/minggu 245 mg / min ggu Demak = 6 , 727 µ g / g = 0,04g/minggu