Time Scan: Instrument Tab

F.2.1 Time Scan: Instrument Tab

Parameter Name

Setting Range

Data mode

%T, Abs, E(S), E(R), %R (U-1900: %T, Abs E(S) and E(R) alone) (U-5100: %T and Abs alone)

Wavelength

Input range

U-1900/2900/2910/

190.00 to

1100.00 nm U-4100/UH4150 175.00 to

3900/3900H/5100

3300.00 nm

Scan time

Input range

U-

60 to 99999 s

1900/2900/2910/5100 U-3900/3900H

60 to 99990 s

U-4100/UH4150

60 to 18400 s

High Resolution (with U-

On, Off

3900/3900H/4100/UH4150) Response (with

Fast, Medium, Slow

U-1900/2900/ 2910/5100)

Delay

0 to 3600 s

Auto Zero before each run

ON, OFF When turned ON (checked), auto zero

measurement (100%T set in transmittance mode, 0 Abs set in absorbance mode) is carried out by using the measuring wavelength before each measurement.

Lamp change mode (for

Auto, D2 only, WI only

other than U-5100) Lamp change wavelength

325.00 to 370.00 nm

(for other than U-5100)

WI Lamp (for other than

On, Off

U-5100) D2 lamp (for other than U-

On, Off

Parameter Name

Setting Range

Slit width (nm)

Model U-3900/3900H

Input range

U-1900

: Fixed at 4 nm U-2900/2910 : Fixed at 1.5 nm U-5100

: Fixed at 5 nm

U-4100

: Select a slit width in the ultraviolet/visible region. It is recommended to fix the slit width for ordinary measurement.

Auto : The slit width is automatically controlled according to the optical energy level under a specified photomultiplier voltage. Concretely, the slit width is widened at a low optical energy level and narrowed at a high optical energy level. In other words, this is a function depending mainly on the S/N ratio (signal-to-noise ratio). In this mode, the slit width automatically changes in a range of about 0.01 to 14 nm. This mode cannot be set simultaneously with PMT mode “Auto”.

Fixed : The slit width is selectable in a range of 0.1 to 8.0 nm in 0.01 (0.02) nm steps. (The parenthesized step corresponds to slit width 2.4 nm or wider.)

PMT mode (for

Auto, Fixed

U-3900/3900H/

When “Fixed” is selected, the photomultiplier voltage

4100/UH4150)

is settable.

PMT voltage (for

0 to 1000 V

U-3900/3900H/ 4100/UH4150)

Sampling interval

Refer to APPENDIX G.2.

(s) Path correct

ON, OFF When turned ON (checked), cell length correction is

effective.

Path Length

0.1 to 100.0 mm

Parameter Name

Setting Range

Attenuation (with

The beam attenuator is inserted on the reference

U-4100/UH4150)

side. Set the attenuation ratio of the attenuator. This setting is usable for a sample whose absorbance and transmittance/reflectance are 4 Abs or more and 0.1%T or less, respectively. For usage, select the Attenuation command from the Spectrophotometer menu after baseline measurement. Then, carry out sample measurement.

None 1/10 1/100

Detector change

A function for automatically correcting the difference

correct (with

in photometric value between the detector

U-4100/UH4150)

changeover points in the near infrared and visible regions.

On Off

Detector change

Set up a wavelength for changeover between the

wavelength (with

detectors for the ultraviolet/visible and near infrared

U-4100/UH4150)

regions. Input range: 700.0 to 900.0 nm

Scan speed (with

Set up a scan speed in the near infrared region.

U-4100/UH4150)

0.75 nm/min 7.5 37.5 75 150 300 750 1500 3000 6000

Parameter Name

Setting Range

Slit width (with

Set up a slit width in the near infrared region.

U-4100/UH4150)

Fixed : Input range: 0.1 to 20.0 nm, in steps of

0.1 nm

Auto : The slit width is automatically controlled according to the optical energy level. This function is intended to keep the S/N ratio (signal-to-noise ratio) constant in the measuring wavelength range as far as possible. In this mode, the slit width automatically changes in a range of about

0.1 to 36 nm. This mode cannot be set simultaneously with Light control mode “Auto”.

PbS Gain (with

Specify a sensitivity level of the detector for the near

U-4100/UH4150)

infrared region. The PbS sensitivity is settable at four levels. Level 1 is used as a reference. Levels 2, 3 and 4 are 2, 4 and 8 times as high as level 1, i.e., the sensitivity rises in the order of 1, 2, 4 and 8 (times). For high resolution measurement in the near infrared region, use a higher sensitivity (PbS sensitivity level 3 or 4). However, use of a high sensitivity inevitably entails an increase in noise level. Therefore, PbS sensitivity level 2 is generally recommended. Use Pbs sensitivity level 1 for measuring quite a flat spectrum with no large absorbance change or checking spectral features alone with minimum noise.

Light control mode

A mode for controlling the light quantity in the near

(with U-4100/

infrared region.

UH4150)

Fixed : Used for ordinary measurement. Auto : Used when measurement cannot be

performed with the slit width fixed because the light quantity in the near infrared region is excessive.