A Photometry: Instrument Tab (Measurement type: Wavelength, Ratio)

F.3.2A Photometry: Instrument Tab (Measurement type: Wavelength, Ratio)

Parameter Name

Setting Range

Wavelength 1 to 6

Model Input range

U-1900/2900/2910/

190.00 to 1100.00 nm

3900/3900H/5100 U-4100/UH4150

Delay

0 to 3600 s

Lamp change

Auto, D2 only, WI only

mode (for other than U-5100)

Lamp change

325.00 to 370.00 nm

wavelength (for other than U-5100)

WI Lamp (for

On, Off

other than U-5100)

D2 lamp (for other

On, Off

than U-5100) Slit width (nm)

Model U-3900/3900H

Input range

U-1900

: Fixed at 4 nm

U-2900/2910 : Fixed at 1.5 nm U-5100

: Fixed at 5 nm

U-4100/UH4150 : Select a slit width in the ultraviolet/visible region. It is recommended to fix the slit width for ordinary measurement.

Auto : The slit width is automatically controlled according to the optical energy level under a specified photomultiplier voltage. Concretely, the slit width is widened at a low optical energy level and narrowed at a high optical energy level. In other words, this is a function depending mainly on the S/N ratio (signal-to-noise ratio). In this mode, the slit width automatically changes in a range of about 0.01 to 14 nm. This mode cannot be set simultaneously with PMT mode “Auto”.

Parameter Name

Setting Range

Slit width (nm)

Fixed : The slit width is selectable in a range of 0.1 to 8.0 nm in 0.01 (0.02) nm steps. (The parenthesized step corresponds to slit width 2.4 nm or wider.)

PMT mode (with

Auto, Fixed

U-3900/3900H/

When “Fixed” is selected, the photomultiplier voltage

is settable.

PMT voltage (with

0 to 1000 V

U-3900/3900H/ 4100/UH4150)

Integration time

0.5 to 10.0 s

(with U- 3900/3900H

Replicates (STD)

0 to 20

Replicates (UNK)

0 to 20 Effective when “Use Sample Table” on the General

tab page is turned ON. Statistics ON, OFF Statistics Number

2 to 4000 Effective when “Statistics” is turned ON.

NOTE: If “Replicates (UNK)” ≥ 2, this parameter is settable in a range of

1 to 4000.

Path correct

ON, OFF When turned ON (checked), cell length correction is

effective.

Path Length

0.1 to 100.0 mm

Parameter Name Setting Range

Attenuation (with The beam attenuator is inserted on the reference U-4100/UH4150)

side. Set the attenuation ratio of the attenuator. This setting is usable for a sample whose absorbance and transmittance/reflectance are 4 Abs or more and 0.1%T or less, respectively. For usage, select the Attenuation command from the Spectrophotometer menu after baseline measurement. Then, carry out sample measurement.

None 1/10 1/100

Detector change A function for automatically correcting the difference correct (with

in photometric value between the detector U-4100/UH4150)

changeover points in the near infrared and visible regions.

On Off

Detector change Set up a wavelength for changeover between the wavelength (with

detectors for the ultraviolet/visible and near infrared U-4100/UH4150)

regions. Input range: 700.0 to 900.0 nm

Scan speed (with Set up a scan speed in the near infrared region. U-4100/UH4150)

0.75 nm/min

Parameter Name

Setting Range

Slit width (with

Set up a slit width in the near infrared region.

U-4100/UH4150)

Fixed : Input range: 0.1 to 20.0 nm in steps of

0.1 nm

Auto : The slit width is automatically controlled according to the optical energy level. This function is intended to keep the S/N ratio (signal-to-noise ratio) constant in the measuring wavelength range as far as possible. In this mode, the slit width automatically changes in a range of about

0.1 to 36 nm. This mode cannot be set simultaneously with Light control mode “Auto”.

PbS Gain (with

Specify a sensitivity level of the detector for the near

U-4100/UH4150)

infrared region. The PbS sensitivity is settable at four levels. Level 1 is used as a reference. Levels 2, 3 and 4 are 2, 4 and 8 times as high as level 1, i.e., the sensitivity rises in the order of 1, 2, 4 and 8 (times). For high resolution measurement in the near infrared region, use a higher sensitivity (PbS sensitivity level 3 or 4). However, use of ahigh sensitivity inevitably entails an increase in noise level. Therefore, PbS sensitivity level 2 is generally recommended. Use Pbs sensitivity level 1 for measuring quite a flat spectrum with no large absorbance change or checking spectral features alone with minimum noise.

Light control mode

A mode for controlling the light quantity in the near

(with U-4100/

infrared region.

UH4150)

Fixed : Used for ordinary measurement. Auto : Used when measurement cannot be

performed with the slit width fixed because the light quantity in the near infrared region is excessive.