1.1.1 Edible Film Kontrol pH 4 Suhu 75o C dengan Larutan yang Mengandung Lemak - 11.70.0127 Mutiara Aletheia Handoko LAMPIRAN

1.1. Persen Kelarutan Edible Film

• – Total berat akhir

  41 LAMPIRAN 1. Perhitungan

  Rumus : Total Berat Awal = Berat kertas saring awal + berat sampel awal Berat Sisa Sampel akhir = Total berat awal

  Persen Kelarutan = 100%

1.1.1 Edible Film Kontrol pH 4 Suhu 75 o C dengan Larutan yang Mengandung Lemak

  Ulangan Kertas Saring Awal

  (gram) Sampel

  Awal (gram)

  Total Berat Awal (gram)

  Total Berat Akhir (gram)

  Sampel Akhir (gram)

  Kelarutan (%) 1 0,5312 0,0513 0,5825 0,5391 0,0434 84,6003 2 0,5912 0,0504 0,6416 0,5994 0,0422 83,7301 3 0,5304 0,0501 0,5805 0,5378 0,0427 85,2295 4 0,5505 0,0442 0,5947 0,5571 0,0376 85,0678 5 0,5045 0,0504 0,5549 0,5107 0,0442 87,6984 6 0,5212 0,0505 0,5717 0,5295 0,0422 83,5643

  42

  1.1.3. Edible Film Kontrol pH 7 Suhu 75 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5412 0,0524 0,5936 0,5492 0,0444 84,7328 2 0,5035 0,0429 0,5464 0,5101 0,0363 84,6153 3 0,5221 0,0451 0,5672 0,5283 0,0389 86,2527 4 0,5204 0,0524 0,5728 0,5275 0,0453 86,4503 5 0,4901 0,0521 0,5422 0,4981 0,0441 84,6449 6 0,5111 0,0605 0,5716 0,5202 0,0514 84,9586

  1.1.2. Edible Film Kontrol pH 4 Suhu 75 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,577 0,0513 0,6283 0,5854 0,0429 83,6257 2 0,4756 0,0611 0,5367 0,4852 0,0515 84,2880 3 0,5443 0,0578 0,6021 0,5549 0,0472 81,6608 4 0,5103 0,0532 0,5635 0,5201 0,0434 81,5789 5 0,5841 0,0512 0,6353 0,5932 0,0421 82,2265 6 0,524 0,0515 0,5755 0,5327 0,0428 83,1067

  43

  1.1.5. Edible Film Kontrol pH 10 Suhu 75 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,59 0,0495 0,6395 0,5991 0,0404 81,6161 2 0,5032 0,0523 0,5555 0,5121 0,0434 82,9827 3 0,5641 0,0545 0,6186 0,5742 0,0444 81,4678 4 0,5023 0,0466 0,5489 0,5101 0,0388 83,2618 5 0,5153 0,0432 0,5585 0,5231 0,0354 81,9444 6 0,5272 0,0477 0,5749 0,5357 0,0392 82,1802

  1.1.4. Edible Film Kontrol pH 7 Suhu 75 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,505 0,062 0,567 0,5162 0,0508 81,9354 2 0,5123 0,0521 0,5644 0,5221 0,0423 81,1900 3 0,5263 0,056 0,5823 0,5358 0,0465 83,0357 4 0,5307 0,0494 0,5801 0,5381 0,042 85,0202 5 0,5258 0,0591 0,5849 0,5381 0,0468 79,1878 6 0,5974 0,058 0,6554 0,6031 0,0523 90,1724

  44

  1.1.7. Edible Film Kontrol pH 4 Suhu 100 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,523 0,0571 0,5801 0,5307 0,0494 86,5148 2 0,5011 0,0542 0,5553 0,5101 0,0452 83,3948 3 0,5424 0,0495 0,5919 0,5511 0,0408 82,4242 4 0,5601 0,0601 0,6202 0,5702 0,05 83,1946 5 0,5353 0,0491 0,5844 0,5432 0,0412 83,9103 6 0,543 0,0532 0,5962 0,5512 0,045 84,5864

  1.1.6. Edible Film Kontrol pH 10 Suhu 75 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,4991 0,0571 0,5562 0,5037 0,0525 91,9439 2 0,5421 0,0551 0,5972 0,5465 0,0507 92,0145 3 0,5901 0,0592 0,6493 0,5952 0,0541 91,3851 4 0,5133 0,0601 0,5734 0,5171 0,0563 93,6772 5 0,5112 0,0578 0,569 0,5172 0,0518 89,6193 6 0,5303 0,0543 0,5846 0,5342 0,0504 92,8176

  45

1.1.8. Edible Film Kontrol pH 4 Suhu 100 o C Tanpa Larutan yang Mengandung Lemak

  (gram) Sampel

  Awal (gram)

  Total Berat Awal (gram)

  Total Berat Akhir (gram)

  Sampel Akhir (gram)

  Kelarutan (%) 1 0,5115 0,0523 0,5638 0,5158 0,048 91,7782 2 0,529 0,0486 0,5776 0,5321 0,0455 93,6213 3 0,512 0,0496 0,5616 0,516 0,0456 91,9354 4 0,5461 0,058 0,6041 0,5497 0,0544 93,7931 5 0,5132 0,0542 0,5674 0,5171 0,0503 92,8044 6 0,5111 0,0611 0,5722 0,5165 0,0557 91,1620 1.1.9.

  Ulangan Kertas Saring Awal

  Ulangan Kertas Saring Awal

  (gram) Sampel

  Awal (gram)

  Total Berat Awal (gram)

  Total Berat Akhir (gram)

  Sampel Akhir (gram)

  Kelarutan (%) 1 0,5227 0,0503 0,573 0,5294 0,0436 86,6799 2 0,5711 0,0601 0,6312 0,5761 0,0551 91,6805 3 0,547 0,0537 0,6007 0,5531 0,0476 88,6405 4 0,5557 0,0532 0,6089 0,5613 0,0476 89,4736 5 0,534 0,0515 0,5855 0,5401 0,0454 88,1553 6 0,5301 0,0501 0,5802 0,5371 0,0431 86,0279

   Edible Film Kontrol pH 7 Suhu 100 o C dengan Larutan yang Mengandung Lemak

  46

1.1.10. Edible Film Kontrol pH 7 Suhu 100 o C Tanpa Larutan yang Mengandung Lemak

  (gram) Sampel

  Awal (gram)

  Total Berat Awal (gram)

  Total Berat Akhir (gram)

  Sampel Akhir (gram)

  Kelarutan (%) 1 0,545 0,0477 0,5927 0,5495 0,0432 90,5660 2 0,5482 0,0556 0,6038 0,553 0,0508 91,3669 3 0,5931 0,0631 0,6562 0,6001 0,0561 88,9064 4 0,582 0,0494 0,6314 0,5864 0,045 91,0931 5 0,5463 0,0561 0,6024 0,5512 0,0512 91,2655 6 0,5123 0,0513 0,5636 0,5164 0,0472 92,0077 1.1.11.

  Ulangan Kertas Saring Awal

  Ulangan Kertas Saring Awal

  (gram) Sampel

  Awal (gram)

  Total Berat Awal (gram)

  Total Berat Akhir (gram)

  Sampel Akhir (gram)

  Kelarutan (%) 1 0,5901 0,054 0,6441 0,5956 0,0485 89,8148 2 0,5223 0,0571 0,5794 0,5283 0,0511 89,4921 3 0,5321 0,058 0,5901 0,5373 0,0528 91,0344 4 0,5283 0,0593 0,5876 0,5333 0,0543 91,568 5 0,5278 0,0532 0,581 0,5341 0,0469 88,1578 6 0,5201 0,0495 0,5696 0,5254 0,0442 89,2929

   Edible Film Kontrol pH 10 Suhu 100 o C dengan Larutan yang Mengandung Lemak

  47

  1.1.13. Edible Film Gliserol pH 4 Suhu 75 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5014 0,0541 0,5555 0,5065 0,049 90,5730 2 0,5908 0,0495 0,6403 0,5961 0,0442 89,2929 3 0,555 0,0605 0,6155 0,5608 0,0547 90,4132 4 0,6016 0,0473 0,6489 0,6061 0,0428 90,4862 5 0,5445 0,0477 0,5922 0,5493 0,0429 89,9371 6 0,5321 0,0523 0,5844 0,5365 0,0479 91,5869

  1.1.12. Edible Film Kontrol pH 10 Suhu 100 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,517 0,0521 0,5691 0,5239 0,0452 86,7562 2 0,5231 0,0501 0,5732 0,5306 0,0426 85,0299 3 0,5187 0,0497 0,5684 0,5275 0,0409 82,2937 4 0,5107 0,0661 0,5768 0,5217 0,0551 83,3585 5 0,5452 0,0563 0,6015 0,5521 0,0494 87,7442 6 0,5207 0,0436 0,5643 0,5275 0,0368 84,4036

  48

  1.1.15. Edible Film Gliserol pH 7 Suhu 75 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5152 0,053 0,5682 0,5228 0,0454 85,6603 2 0,543 0,0479 0,5909 0,5501 0,0408 85,1774 3 0,5302 0,0465 0,5767 0,5379 0,0388 83,4408 4 0,5142 0,0524 0,5666 0,5208 0,0458 87,4045 5 0,553 0,0549 0,6079 0,5602 0,0477 86,8852 6 0,5202 0,0515 0,5717 0,5268 0,0449 87,1844

  1.1.14. Edible Film Gliserol pH 4 Suhu 75 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5545 0,0495 0,604 0,5635 0,0405 81,8181 2 0,5017 0,0561 0,5578 0,5101 0,0477 85,0267 3 0,5226 0,0508 0,5734 0,5303 0,0431 84,8425 4 0,5123 0,0532 0,5655 0,5221 0,0434 81,5789 5 0,5874 0,0521 0,6395 0,5978 0,0417 80,0383 6 0,5236 0,0564 0,58 0,533 0,047 83,3333

  49

  1.1.17. Edible Film Gliserol pH 10 Suhu 75 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,518 0,0487 0,5667 0,5273 0,0394 80,9034 2 0,5421 0,0433 0,5854 0,5491 0,0363 83,8337 3 0,5011 0,0495 0,5506 0,5101 0,0405 81,8181 4 0,538 0,0498 0,5878 0,5461 0,0417 83,7349 5 0,543 0,0523 0,5953 0,552 0,0433 82,7915 6 0,5281 0,0535 0,5816 0,5381 0,0435 81,3084

  1.1.16. Edible Film Gliserol pH 7 Suhu 75 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5657 0,0573 0,623 0,5768 0,0462 80,6282 2 0,5552 0,0543 0,6095 0,5634 0,0461 84,8987 3 0,5212 0,0567 0,5779 0,5322 0,0457 80,5996 4 0,5477 0,0543 0,602 0,5578 0,0442 81,3996 5 0,5322 0,0578 0,59 0,5437 0,0463 80,1038 6 0,5262 0,0592 0,5854 0,5351 0,0503 84,9662

  50

  1.1.19. Edible Film Gliserol pH 4 Suhu 100 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,532 0,0567 0,5887 0,5424 0,0463 81,6578 2 0,5481 0,0404 0,5885 0,5559 0,0326 80,6930 3 0,5523 0,0442 0,5965 0,5594 0,0371 83,9366 4 0,5226 0,0541 0,5767 0,5327 0,044 81,3308 5 0,5391 0,057 0,5961 0,5483 0,0478 83,8596 6 0,5433 0,0497 0,593 0,5524 0,0406 81,6901

  1.1.18. Edible Film Gliserol pH 10 Suhu 75 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5323 0,0497 0,582 0,5355 0,0465 93,5613 2 0,512 0,0491 0,5611 0,5161 0,045 91,6496 3 0,5211 0,0542 0,5753 0,5242 0,0511 94,2804 4 0,5332 0,0508 0,584 0,5358 0,0482 94,8818 5 0,5012 0,0455 0,5467 0,5038 0,0429 94,2857 6 0,5203 0,0602 0,5805 0,5251 0,0554 92,0265

  51

  1.1.21. Edible Film Gliserol pH 7 Suhu 100 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5441 0,0501 0,5942 0,547 0,0472 94,2115 2 0,5361 0,0476 0,5837 0,539 0,0447 93,9075 3 0,5212 0,0487 0,5699 0,524 0,0459 94,2505 4 0,545 0,0541 0,5991 0,5497 0,0494 91,3123 5 0,5291 0,0496 0,5787 0,5323 0,0464 93,5483 6 0,5032 0,0517 0,5549 0,507 0,0479 92,6499

  1.1.20. Edible Film Gliserol pH 4 Suhu 100 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5867 0,0523 0,639 0,5904 0,0486 92,9254 2 0,5192 0,0517 0,5709 0,5238 0,0471 91,1025 3 0,5231 0,057 0,5801 0,5289 0,0512 89,8245 4 0,5437 0,0493 0,593 0,5471 0,0459 93,1034 5 0,5212 0,0516 0,5728 0,5248 0,048 93,0232 6 0,5371 0,057 0,5941 0,5425 0,0516 90,5263

  52

  1.1.23. Edible Film Gliserol pH 10 Suhu 100 o C dengan Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,537 0,0601 0,5971 0,5434 0,0537 89,3510 2 0,549 0,056 0,605 0,5531 0,0519 92,6785 3 0,5221 0,0423 0,5644 0,527 0,0374 88,4160 4 0,529 0,0591 0,5881 0,5354 0,0527 89,1708 5 0,5471 0,0547 0,6018 0,5523 0,0495 90,4936 6 0,5231 0,0601 0,5832 0,529 0,0542 90,1830

  1.1.22. Edible Film Gliserol pH 7 Suhu 100 o C Tanpa Larutan yang Mengandung Lemak

  Sampel Akhir (gram)

  Total Berat Akhir (gram)

  Total Berat Awal (gram)

  Awal (gram)

  (gram) Sampel

  Ulangan Kertas Saring Awal

  Kelarutan (%) 1 0,5116 0,0543 0,5659 0,5164 0,0495 91,1602 2 0,5213 0,0562 0,5775 0,5261 0,0514 91,4590 3 0,5128 0,0537 0,5665 0,5172 0,0493 91,8063 4 0,519 0,0473 0,5663 0,5233 0,043 90,9090 5 0,5281 0,0502 0,5783 0,5327 0,0456 90,8366 6 0,531 0,0521 0,5831 0,5361 0,047 90,2111

  53

1.1.24. Edible Film Gliserol pH 10 Suhu 100 o C Tanpa Larutan yang Mengandung Lemak

  Ulangan Kertas Saring Awal

  (gram) Sampel

  Awal (gram)

  Total Berat Awal (gram)

  Total Berat Akhir (gram)

  Sampel Akhir (gram)

  Kelarutan (%) 1 0,5354 0,0443 0,5797 0,5402 0,0395 89,1647 2 0,532 0,0405 0,5725 0,5362 0,0363 89,6296 3 0,5311 0,0453 0,5764 0,5348 0,0416 91,8322 4 0,5534 0,0543 0,6077 0,5581 0,0496 91,3443 5 0,5034 0,0535 0,5569 0,5081 0,0488 91,2149 6 0,5302 0,0495 0,5797 0,5352 0,0445 89,8989

1.2. Perhitungan Water Vapour Transmission Rate (WVTR) Edible Film

  Nilai WVTR edible film terhadap uap air akan diperoleh menggunakan rumus : Keterangan simbol: n : Water lost / air yang berdifusi melewati film (gram) t : Waktu (jam) a : Luas area (m

  2

  )

  1.2.1. WVTR Edible Film Kontrol

  1.2.1.1 WVTR Edible Film Kontrol Setelah 1 Jam

  Batch 1 0,05

  24 505,3483

  =

  0,002375

  1 Rata-rata = 507,0328 Batch 2

  0,0503

  24

  508,7173 =

  0,002375

  1

  1.2.1.2 WVTR Edible Film Kontrol Setelah 2 Jam

  Batch 1 0,1043

  24

  527,2467 =

  0,002375

  2 Rata-rata = 538,1959 Batch 2

  0,1086

  24 549,1451

  =

  0,002375

  2

  1.2.1.3 WVTR Edible Film Kontrol Setelah 3 Jam

  Batch 1 0,1042

  24 478,3964

  =

  0,002375

  3 Rata-rata = 491,3108 Batch 2

  0,1496

  24 504,2253

  =

  0,002375

  3

  1.2.1.4 WVTR Edible Film Kontrol Setelah 4 Jam

  Batch 1 0,1673

  24 422,8081

  =

  0,002375

  4 Rata-rata = 466,1838

  Batch 2 0,2016

  24 509,5595

  =

  0,002375

  4

1.2.1.5 WVTR Edible Film Kontrol Setelah 5 Jam

  Batch 1 0,2016

  24

  407,6476 =

  0,002375

5 Rata-rata = 456,161

  Batch 2 0,2496

  24

  504,6745 =

  0,002375

  5

1.2.1.6 WVTR Edible Film Kontrol Setelah 6 Jam

  Batch 1 0,2443

  24

  411,5781 =

  0,002375

6 Rata-rata = 453,4097

  Batch 2 0,249

  24

  495,2413 =

  0,002375

  6

1.2.1.7 WVTR Edible Film Kontrol Setelah 7 Jam

  Batch 1 0,293

  24

  423,53 = Rata-rata = 453,3696

  0,002375

7 Batch 2

  0,3346

  24

  483,2092 =

  0,002375

  7

  1.2.1.8 WVTR Edible Film Kontrol Setelah 8 Jam

  Batch 1 0,3216

  24

  406,3842 =

  0,002375

  8 Rata-rata = 433,5467 Batch 2

  0,3646

  24

  460,7092 =

  0,002375

  8

  1.2.1.9 WVTR Edible Film Kontrol Setelah 9 Jam

  Batch 1 0,3543

  24

  397,915 =

  0,002375

  9 Rata-rata = 419,8134 Batch 2

  0,3933

  24

  441,7118 =

  0,002375

  9

  1.2.1.10 WVTR Edible Film Kontrol Setelah 10 Jam

  Batch 1 0,388

  24

  392,1503 =

  0,002375

  10 Rata-rata = 412,7011 Batch 2

  0,4866

  24

  433,2519 =

  0,002375

  10

  1.2.1.11 WVTR Edible Film Kontrol Setelah 11 Jam

  Batch 1 0,4243

  24

  389,8838 =

  0,002375

  11 Batch 2 0,4656

  24

  441,7118 =

  0,002375

  11

1.2.1.12 WVTR Edible Film Kontrol Setelah 12 Jam

  Batch 1 0,4586

  24

  386,3107 =

  0,002375

12 Rata-rata = 404,419

  Batch 2 0,5016

  24

  422,5273 =

  0,002375

  12 1.2.2.

   WVTR Edible Film Dengan Penambahan Gliserol

1.2.2.1. WVTR Edible Film Gliserol Setelah 1 Jam

  Batch 1 0,118

  24

  1192,622 =

  0,002375

1 Rata-rata = 1167,355

  Batch 2 0,113

  24

  1142,087 =

  0,002375

  1

1.2.2.2.WVTR Edible Film Gliserol Setelah 2 Jam

  Batch 1 0,192

  24

  970,2687 =

  0,002375

2 Rata-rata = 1023,33

  Batch 2 0,213

  24

  1076,392 =

  0,002375

  2

  1.2.2.3.WVTR Edible Film Gliserol Setelah 3 Jam

  Batch 1 0,25

  24

  842,2471 =

  0,002375

  3 Rata-rata = 843,9316 Batch 2

  0,251

  24

  845,6161 =

  0,002375

  3

  1.2.2.4.WVTR Edible Film Gliserol Setelah 4 Jam

  Batch 1 0,285

  24

  720,1213 =

  0,002375

  4 Rata-rata = 728,9649 Batch 2

  0,292

  24

  737,8085 =

  0,002375

  4

  1.2.2.5.WVTR Edible Film Gliserol Setelah 5 Jam

  Batch 1 0,323

  24

  652,91 =

  0,002375

  5 Rata-rata = 664,0276 Batch 2

  0,334

  24

  675,1453 =

  0,002375

  5

  1.2.2.6.WVTR Edible Film Gliserol Setelah 6 Jam

  Batch 1 0,366

  24

  616,5249 =

  0,002375

  6 Batch 2 0,349

  24

  587,8885 =

  0,002375

  6

1.2.2.7.WVTR Edible Film Gliserol Setelah 7 Jam

  Batch 1 0,387

  24

  558,7708 =

  0,002375

7 Rata-rata = 542,1665

  Batch 2 0,364

  24

  525,5622 =

  0,002375

  7

1.2.2.8.WVTR Edible Film Gliserol Setelah 8 Jam

  Batch 1 0,438

  24

  553,3564 =

  0,002375

8 Rata-rata = 537,5642

  Batch 2 0,413

  24

  521,7721 =

  0,002375

  8

1.2.2.9.WVTR Edible Film Gliserol Setelah 9 Jam

  Batch 1 0,498

  24

  559,2521 =

  0,002375

9 Rata-rata = 533,9847

  Batch 2 0,453

  24

  508,7173 =

  0,002375

  9

1.2.2.10. WVTR Edible Film Gliserol Setelah 10 Jam

  Batch 1 0,548

  24

  553,8617 =

  0,002375

10 Rata-rata = 530,1103

  Batch 2 0,501

  24

  506,359 =

  0,002375

  10

1.2.2.11. WVTR Edible Film Gliserol Setelah 11 Jam

  Batch 1 0,598

  24

  549,4514 =

  0,002375

  11 Rata-rata = 533,3721 Batch 2

  0,563

  24

  517,2929 =

  0,002375

  11 1.2.2.12.

   WVTR Edible Film Gliserol Setelah 12 Jam

  Batch 1 0,638

  24

  537,3537 =

  0,002375

  12 Rata-rata = 528,9312 Batch 2

  0,618

  24

  520,5087 =

  12 0,002375

  LAMPIRAN 2. Output SPSS

2.1. Output SPSS uji One Way Anova, Pos Hoc Duncan o

2.1.1. Kelarutan Edible Film yang Dilarutkan pada pH 4 dan Berbagai Suhu (75 C

  o dan 100

C) Tests of Normal ity

  a Kolmogorov -Smirnov Shapiro-Wilk

Stat is tic df Sig. Stat is tic df Sig.

kelarutan1 ,103

  48 ,200* ,923 48 ,004 *. This is a lower bound of t he t rue signif icance.

  a.

  Lillief ors Signif ic ance Correct ion ANOVA kelarutan Sum of

  

Squares df Mean Square F Sig.

Between Groups 690,119

  7 98, 588 50, 837 ,000 Within Groups 77, 573

40 1, 939

Tot al

  767,692

  47 kel arutan a

  Duncan Subset f or alpha = .05 perlakuan N

  1

  2 gliserol+lemak 75oC 6 84, 9311 kontrol+lemak 75oC 6 84, 9818 kontrol tanpa lemak 75oC 6 85, 2758 gliserol t anpa lemak 6 85, 9588 75oC kontrol+lemak 100oC

6 91, 9096

kontrol tanpa lemak

6 92, 5158

100oC gliserol t anpa lemak

  

6 93, 3134

100oC gliserol+lemak100oC

6 93, 4476

Sig.

  ,252 ,087 Means f or groups in homogeneous subsets are display ed.

  a.

  Uses Harmonic Mean Sample Size = 6, 000. o

2.1.2. Kelarutan Edible Film yang dilarutkan pada pH 7 dan Berbagai Suhu (75 C

  o dan 100

  C)

  Tests of Normal ity a

  Kolmogorov -Smirnov Shapiro-Wilk

Stat is tic df Sig. Stat is tic df Sig.

kelarutan2 ,119

  48 ,086 ,907 48 ,001 a. Lillief ors Signif ic ance Correct ion

  ANOVA kelarutan Sum of

  

Squares df Mean Square F Sig.

Between Groups 755,239

  7 107,891 51, 480 ,000 Within Groups 83, 831

40 2, 096

Tot al

  839,070

  47 kel arutan a

  Duncan Subset f or alpha = .05 perlakuan N

  1

  2

  3 kontrol tanpa lemak 75oC 6 82, 2422 gliserol t anpa lemak 6 82, 3984 75oC kontrol+lemak 75oC 6 82, 7478 gliserol+lemak 75oC 6 82, 7730 kontrol+lemak 100oC

6 88, 4430

gliserol t anpa lemak 6 90, 0489 90, 0489 100oC kontrol tanpa lemak

  6 90, 8677 100oC gliserol+lemak100oC 6 91, 7509 Sig. ,569 ,062 ,060 Means f or groups in homogeneous subsets are display ed.

  a.

  Uses Harmonic Mean Sample Size = 6, 000. o

2.1.3. Kelarutan Edible Film yang dilarutkan pada pH 10 dan Berbagai Suhu (75 C

  o dan 100

C) Tests of Normali ty

  a

Kolmogorov -Smirnov Shapiro-Wilk

Stat is tic df Sig. Stat is tic df Sig. kelarutansin ,152

  

48 ,007 ,913

48 ,002 a. Lillief ors Signif ic ance Correction

  ANOVA kelarutan Sum of

  

Squares df Mean Square F Sig.

Between Groups 700,844

  7 100,121 29, 489 ,000 Within Groups 135,807 40 3, 395 Tot al 836,650

  47 kel arutan a

  Duncan

Subset f or alpha = .05

perlakuan N

  1

  2 gliserol+lemak 75oC 6 82, 0994 gliserol t anpa lemak 6 82, 1947 75oC kontrol+lemak 75oC 6 83, 4236 kontrol tanpa lemak 75oC 6 84, 0042 kontrol+lemak 100oC

6 89, 8934

kontrol tanpa lemak

6 90, 3816

100oC gliserol t anpa lemak

  

6 90, 5142

100oC gliserol+lemak100oC

6 91, 0638

Sig.

  ,109 ,324 Means f or groups in homogeneous subsets are display ed.

  a.

  Uses Harmonic Mean Sample Size = 6, 000. o

  

2.1.4. Kelarutan Edible Film yang dilarutkan pada suhu 75 C dan Berbagai pH

( 4, 7, 10) Tests of Normal ity a

  Kolmogorov -Smirnov Shapiro-Wilk Stat is tic df Sig. Stat is tic df Sig. kelarutan ,083

  72 ,200* ,978 72 ,230 *. This is a lower bound of t he true signif icance.

  a.

  Lillief ors Signif ic ance Correct ion

  ANOVA kelarutan Sum of

  

Squares df Mean Square F Sig.

Between Groups 127,019

  11 11, 547 3, 446 ,001 Within Groups 201,057

60 3, 351

Tot al 328,077

  71 kel arutan a

  Duncan Subset f or alpha = .05 perlakuan N

  1

  2

  3

  4 gliserol + lemak pH 10 6 82, 0994 gliserol t anpa lemak 6 82, 1947 pH10 kontrol tanpa lemak pH7 6 82, 2422 gliserol t anpa lemak pH7 6 82, 3984 kontrol+lemak pH 7

6 82, 7478 82, 7478

gliserol+lemak pH7

  

6 82, 7730 82, 7730

kontrol+lemak pH 10 6 83, 4236 83, 4236 83, 4236 kontrol tanpa lemak pH10 6 84, 0042 84, 0042 84, 0042 84, 0042 gliserol+lemak pH4 6 84, 9311 84, 9311 84, 9311 kontrol+lemak pH 4 6 84, 9818 84, 9818 84, 9818 kontrol tanpa lemak pH4 6 85, 2758 85, 2758 gliserol t anpa lemak pH4 6 85, 9588 Sig. ,129 ,067 ,124 ,104

  Means f or groups in homogeneous s ubsets are display ed.

  a.

  Uses Harmonic Mean Sample Size = 6, 000. o

2.1.5. Kelarutan Edible Film yang dilarutkan pada suhu 100 C dan Berbagai pH (4,7,10) Tests of Normal ity

  a Kolmogorov -Smirnov Shapiro-Wilk Stat is tic df Sig. Stat is tic df Sig. kelarutan ,072

  72 ,200* ,984 72 ,484 *. This is a lower bound of t he true signif icance.

  a.

  Lillief ors Signif ic ance Correct ion

  ANOVA kelarutan Sum of

  

Squares df Mean Square F Sig.

Between Groups 143,723

  11 13, 066 8, 153 ,000 Within Groups 96, 153

60 1, 603

Tot al 239,876

  71 _a

kel arutan

Duncan

  Subset f or alpha = .05 perlakuan N

  1

  2

  3

  4

  5

  6 kontrol+lemak pH7 6 88, 4430 kontrol+lemak pH10 6 89, 8934 89, 8934 gliserol t anpa lemak pH 7 6 90, 0489 kontrol tanpa lemak pH10

6 90, 3816 90, 3816

gliserol t anpa lemak

6 90, 5142 90, 5142

pH10 kontrol tanpa lemak pH7

6 90, 8677 90, 8677

gliserol + lemak pH 10

  6 91, 0638 91, 0638 91, 0638 gliserol+lemak pH7 6 91, 7509 91, 7509 91, 7509 kontrol+lemak pH4 6 91, 9096 91, 9096 91, 9096 91, 9096 kontrol tanpa lemak pH4 6 92, 5158 92, 5158 92, 5158 gliserol t anpa lemak pH 4 6 93, 3134 93, 3134 gliserol+lemak pH4

  6 93, 4476

Sig. ,052 ,168 ,070 ,073 ,054 ,058

  Means f or groups in homogeneous s ubset s are display ed.

  a.

  Uses Harmonic Mean Sample Size = 6,000.

2.1.6. Kelarutan Edible Film yang dilarutkan pada Larutan yang Mengandung o o Lemak pada Berbagai Suhu (75 C dan 100

  C) Tests of Normal ity a

  

Kolmogorov -Smirnov Shapiro-Wilk

Stat is tic df Sig. Stat is tic df Sig. kelarutansinn ,094

72 ,186 ,929

72 ,001 a.

  Lillief ors Signif ic ance Correct ion

  ANOVA kelarutan Sum of

  

Squares df Mean Square F Sig.

Between Groups 1171,943

  11 106,540 29, 805 ,000 Within Groups 214,477

60 3, 575

Tot al 1386,420

  71

kel arutan

a

  Duncan Subset f or alpha = .05 perlakuan N

  1

  2

  3

  4

  5 gliserol pH10 75oC 6 82, 0994 kontrol pH7 75oC 6 82, 7478 82, 7478 gliserol pH 7 75oC 6 82, 7730 82, 7730 kontro pH 10 75oC 6 83, 4236 83, 4236 gliserol pH 4 75oC 6 84, 9311 kontrol pH4 75oC 6 84, 9818 kontrol pH7 100oC 6 88, 4430 kontrol pH10 100oC 6 89, 8934 89, 8934 gliserol pH 10 100oC 6 91, 0638 gliserol pH 7 100oC 6 91, 7509 91, 7509 kontrol pH4 100oC 6 91, 9096 91, 9096 gliserol pH 4 100oC

  6 93, 4476

Sig. ,276 ,072 ,189 ,096 ,148

  Means f or groups in homogeneous s ubsets are display ed.

  a.

  Uses Harmonic Mean Sample Size = 6, 000.

2.1.7. Kelarutan Edible Film yang dilarutkan pada Larutan Tanpa Lemak pada o o Berbagai Suhu (75 C dan 100

C) Tests of Normali ty

  a

Kolmogorov -Smirnov Shapiro-Wilk

Stat is tic df Sig. Stat is tic df Sig. kelarutansin ,128

  

72 ,005 ,918

72 ,000 a. Lillief ors Signif ic ance Correction

  ANOVA kelarutan Sum of

  Squares df Mean Square F Sig. Between Groups 1173,195

  11 106,654 77, 348 ,000 Within Groups 82, 733 60 1, 379 Tot al

  1255,929

  71

kel arutan

a

  Duncan Subset f or alpha = .05 perlakuan N

  1

  2

  3

  4

  5 gliserol pH10 75oC 6 82, 1947 kontrol pH7 75oC 6 82, 2422 gliserol pH 7 75oC 6 82, 3984 kontro pH 10 75oC 6 84, 0042 kontrol pH4 75oC 6 85, 2758 85, 2758 gliserol pH 4 75oC 6 85, 9588 gliserol pH 7 100oC 6 90, 0489 kontrol pH10 100oC 6 90, 3816 gliserol pH 10 100oC 6 90, 5142 kontrol pH7 100oC 6 90, 8677 kontrol pH4 100oC

  6 92, 5158 gliserol pH 4 100oC

  6 93, 3134 Sig.

  ,780 ,066 ,318 ,279 ,244 Means f or groups in homogeneous s ubsets are display ed.

  a.

  Uses Harmonic Mean Sample Size = 6, 000.

2.2. Uji SPSS Independent Sampels T-Test

  2.2.1. Uji Kuat Tarik (Tensile Strength) _{Independent Samples Test TensileStrength Equal v ariances Equality of Varianc es t-test f or Equality of Means} Lev ene's Test f or _{F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper 3, 369 ,096 19, 908 10 ,000 11, 86406 ,59593 10, 53625 13, 19188 Mean Std. Error 95% Conf idenc e Interv al of the Dif f erence not as sumed Equal v ariances} ass umed _{19, 908 7, 235 ,000 11, 86406 ,59593 10, 46414 13, 26398}

  2.2.2. Uji Pemanjangan (Elongasi)

  _{Equality of Varianc es t-test f or Equality of Means Lev ene's Test f or} Independent Samples Test _{Mean Std. Error 95% Conf idence Interv al of the Dif f erence elongasi Equal v ariances not as sumed Equal v ariances ass umed 3, 333 ,098 -19,174} F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper _{-19,174 6, 372 ,000 -57,03447 2, 97460 -64,21124 -49,85769 10 ,000 -57,03447 2, 97460 -63,66229 -50,40665}

2.2.3. Uji WVTR

  2.2.3.1. Uji WVTR Setelah 1 Jam _{Equality of Varianc es t-test f or Equality of Means Lev ene's Test f or Independent Samples Test WVTR Equal v ariances Equal v ariances ass umed 3E+017 ,000 -26,075 F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper 2 ,001 -660,32174 25, 32350 -769,280 -551,364 Mean Std. Error} 95% Conf idenc e _{Interv al of the Dif f erence not as sumed} -26,075 1, 009 ,024 -660,32174 25, 32350 -975,465 -345,179

  2.2.3.2. Uji WVTR Setelah 2 Jam

_{Equality of Varianc es t-test f or Equality of Means}

_{Lev ene's Test f or}

_{Independent Samples Test}

_{WVTR Equal v ariances Equal v ariances ass umed 5E+017 ,000 -8,954 F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper 2 ,012 -485,13434 54, 17947 -718,250 -252,019 Mean Std. Error} 95% Conf idenc e _{Interv al of the Dif f erence not as sumed} -8,954 1, 085 ,060 -485,13434 54, 17947 -1058, 31 88, 04043

  2.2.3.3. Uji WVTR Setelah 3 Jam

_{Equality of Varianc es t-test f or Equality of Means}

_{Lev ene's Test f or}

_{Independent Samples Test}

_{WVTR Equal v ariances ass umed 2E+018 ,000 -27,075 F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper 2 ,001 -352,62079 13, 02385 -408,658 -296,584 Mean Std. Error} 95% Conf idenc e _{Interv al of the Dif f erence not as sumed} Equal v ariances _{-27,075 1, 034 ,021 -352,62079 13, 02385 -505,778 -199,463}

  2.2.3.4. Uji WVTR Setelah 4 Jam

  2.2.3.5. Uji WVTR Setelah 5 Jam

  2.2.3.6. Uji WVTR Setelah 6 Jam

  2.2.3.7. Uji WVTR Setelah 7 Jam

  2.2.3.8. Uji WVTR Setelah 8 Jam

^{Independent Samples Test}

^{3E+017 ,000 -5,936 2 ,027 -262,78110 44, 26808 -453,251 -72,31093 -5,936 1, 083 ,093 -262,78110 44, 26808 -732,960 207,39809 Equal v ariances ass umed Equal v ariances not as sumed WVTR F Sig. Lev ene's Test f or Equality of Varianc es t df Sig. (2-t ailed) Mean Dif f erence Std. Error Dif f erence Lower Upper 95% Conf idenc e Interv al of the Dif f erence t-test f or Equality of Means}

^{Independent Samples Test}

^{4E+016 ,000 -4,176 2 ,053 -207,86659 49, 77103 -422,014 6, 28088 -4,176 1, 105 ,131 -207,86659 49, 77103 -714,775 299,04155 Equal v ariances ass umed Equal v ariances not as sumed WVTR F Sig. Lev ene's Test f or Equality of Varianc es t df Sig. (2-t ailed) Mean Dif f erence Std. Error Dif f erence Lower Upper 95% Conf idenc e Interv al of the Dif f erence t-test f or Equality of Means}

^{Independent Samples Test}

^{2E+016 ,000 -3,365 2 ,078 -148,79699 44, 21419 -339,035 41, 44130 -3,365 1, 231 ,145 -148,79699 44, 21419 -513,564 215,96980 Equal v ariances ass umed Equal v ariances not as sumed WVTR F Sig. Lev ene's Test f or Equality of Varianc es t df Sig. (2-t ailed) Mean Dif f erence Std. Error Dif f erence Lower Upper 95% Conf idenc e Interv al of the Dif f erence t-test f or Equality of Means}

^{Independent Samples Test}

^{5E+015 ,000 -2,600 2 ,122 -88,79691 34, 14828 -235,725 58, 13129 -2,600 1, 565 ,155 -88,79691 34, 14828 -282,704 105,11030 Equal v ariances ass umed Equal v ariances not as sumed WVTR F Sig. Lev ene's Test f or Equality of Varianc es t df Sig. (2-t ailed) Mean Dif f erence Std. Error Dif f erence Lower Upper 95% Conf idenc e Interv al of the Dif f erence t-test f or Equality of Means}

  

_{Equality of Varianc es t-test f or Equality of Means}

_{Lev ene's Test f or}

Independent Samples Test

_{Mean Std. Error 95% Conf idenc e Interv al of the Dif f erence WVTR Equal v ariances not as sumed Equal v ariances ass umed 2E+017 ,000 -3,311} F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper _{-3,311 1, 607 ,107 -104,01752 31, 41960 -276,438 68, 40275 2 ,080 -104,01752 31, 41960 -239,205 31, 17011}

  2.2.3.9. Uji WVTR Setelah 9 Jam

_{Equality of Varianc es t-test f or Equality of Means}

_{Lev ene's Test f or}

_{Independent Samples Test}

_{WVTR Equal v ariances Equal v ariances ass umed 2E+014 ,000 -3,415 F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper 2 ,076 -114,17128 33, 43626 -258,036 29, 69332 Mean Std. Error} 95% Conf idenc e _{Interv al of the Dif f erence not as sumed} -3,415 1, 960 ,078 -114,17128 33, 43626 -260,857 32, 51459

  2.2.3.10. Uji WVTR Setelah 10 Jam

_{Equality of Varianc es t-test f or Equality of Means}

_{Lev ene's Test f or}

_{Independent Samples Test}

_{WVTR Equal v ariances Equal v ariances ass umed 4E+014 ,000 -3,738 F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper 2 ,065 -117,40925 31, 40803 -252,547 17, 72858 Mean Std. Error} 95% Conf idenc e _{Interv al of the Dif f erence not as sumed} -3,738 1, 960 ,067 -117,40925 31, 40803 -255,258 20, 43968

  2.2.3.11. Uji WVTR Setelah 11 Jam

_{Equality of Varianc es t-test f or Equality of Means}

_{Lev ene's Test f or}

_{Independent Samples Test}

_{WVTR Equal v ariances Equal v ariances ass umed 4E+016 ,000 -4,176 F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper 2 ,053 -207,86659 49, 77103 -422,014 6, 28088 Mean Std. Error} 95% Conf idenc e _{Interv al of the Dif f erence not as sumed} -4,176 1, 105 ,131 -207,86659 49, 77103 -714,775 299,04155

  2.2.3.12. Uji WVTR Setelah 12 Jam

  _{Equality of Varianc es t-test f or Equality of Means Lev ene's Test f or}

Independent Samples Test

_{Mean Std. Error 95% Conf idenc e Interv al of the Dif f erence WVTR Equal v ariances not as sumed Equal v ariances ass umed 9E+015 ,000 -6,235} F Sig. t df Sig. (2-t ailed) Dif f erence Dif f erence Lower Upper _{-6,235 1, 413 ,054 -124,51220 19, 97120 -255,556 6, 53127 2 ,025 -124,51220 19, 97120 -210,441 -38,58304}