Pembuatan Nanosilikon Dari Pasir Alam Secara Magnesiotermik Dengan Penambahan Kalium Klorida
LAMPIRAN
Universitas Sumatera Utara
62
Lampiran 1. Data JCPDS Silikat (Morris,1976)
Universitas Sumatera Utara
63
Lampiran 2. Data JCPDS Silikon (Morris,1976)
Universitas Sumatera Utara
64
Lampiran 3. Difraktogram Silika Hasil Pemurnian dari Pasir Kuarsa
tion
Analysis date
2016/03/28 11:23:32
Sample name
Spl SiO2
Measurement date
2016/03/28 11:11:14
File name
171-xrd-2016.ras
Operator
administrator
Comment
Universitas Sumatera Utara
65
Lampiran 4. Puncak Difraktogram Silika Hasil Pemurnian dari Pasir Kuarsa
No.
2-theta(deg)
d(ang.)
Height(counts
)
FWHM(deg)
Int. I(counts
deg)
Int. W(deg)
Asym
.
factor
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
5.71(5)
13.442(13)
20.733(15)
22.482(7)
23.340(4)
23.434(4)
24.123(13)
24.327(12)
26.249(13)
26.415(6)
26.538(2)
26.937(5)
27.336(10)
27.463(7)
27.592(6)
27.801(14)
30.134(19)
30.479(7)
30.829(2)
35.03(4)
36.339(9)
36.906(15)
39.223(4)
40.070(17)
41.325(8)
41.993(15)
42.51(4)
45.33(2)
45.693(7)
47.88(6)
49.560(6)
50.001(3)
52.403(13)
54.704(18)
57.815(13)
58.163(13)
59.840(4)
60.531(17)
61.858(15)
65.39(4)
67.587(12)
67.939(4)
69.367(8)
72.708(13)
73.324(8)
73.457(8)
74.625(5)
78.638(8)
79.66(3)
81.16(10)
83.645(10)
87.206(6)
15.46(13)
6.582(7)
4.281(3)
3.9515(11)
3.8082(6)
3.7931(6)
3.6863(19)
3.6558(18)
3.3923(17)
3.3715(7)
3.3561(3)
3.3072(6)
3.2598(12)
3.2451(8)
3.2302(7)
3.2064(15)
2.9633(18)
2.9305(7)
2.8981(2)
2.559(3)
2.4703(6)
2.4336(10)
2.2950(2)
2.2484(9)
2.1830(4)
2.1498(7)
2.1247(19)
1.9991(9)
1.9839(3)
1.898(2)
1.8378(2)
1.82265(12)
1.7446(4)
1.6765(5)
1.5935(3)
1.5848(3)
1.54433(10)
1.5283(4)
1.4987(3)
1.4261(8)
1.3849(2)
1.37860(7)
1.35366(14)
1.2995(2)
1.29008(13)
1.28806(12)
1.27078(8)
1.21567(11)
1.2027(4)
1.1841(12)
1.15517(11)
1.11692(6)
42(7)
73(9)
185(14)
425(21)
65(8)
393(20)
111(11)
285(17)
197(14)
229(15)
676(26)
395(20)
104(10)
228(15)
413(20)
145(12)
20(4)
174(13)
125(11)
14(4)
117(11)
27(5)
107(10)
55(7)
102(10)
58(8)
39(6)
43(7)
334(18)
10(3)
44(7)
834(29)
55(7)
71(8)
50(7)
54(7)
184(14)
34(6)
43(7)
10(3)
54(7)
455(21)
107(10)
70(8)
256(16)
169(13)
361(19)
47(7)
29(5)
12(3)
56(7)
30(5)
0.74(15)
0.11(4)
0.13(3)
0.099(5)
0.042(18)
0.063(5)
0.09(3)
0.110(16)
0.321(15)
0.063(8)
0.060(3)
0.100(5)
0.128(15)
0.09(6)
0.09(3)
0.157(13)
0.22(6)
0.121(10)
0.055(4)
0.67(11)
0.110(10)
0.075(18)
0.119(12)
0.13(3)
0.069(9)
0.168(18)
0.40(4)
0.10(3)
0.083(7)
0.53(16)
0.09(2)
0.104(3)
0.07(2)
0.117(18)
0.102(11)
0.106(11)
0.083(7)
0.13(2)
0.20(3)
0.71(13)
0.122(14)
0.093(4)
0.114(7)
0.115(12)
0.135(17)
0.113(13)
0.107(5)
0.069(12)
0.18(3)
0.37(9)
0.133(15)
0.11(2)
42(7)
15.9(16)
45(2)
46.4(15)
4.1(16)
36(2)
11(3)
37(4)
72(4)
17(2)
50(3)
47.3(13)
17(2)
24(21)
45(24)
26.9(16)
6.4(12)
26.7(11)
9.5(4)
12.0(17)
15.7(8)
2.6(6)
15.6(10)
11.2(9)
10.2(7)
10.7(9)
17.1(13)
5.6(11)
36.0(18)
6(2)
4.8(9)
110(2)
6.4(7)
12.1(9)
5.5(5)
6.2(6)
25.4(9)
7.1(8)
11.3(9)
7.6(16)
8.8(8)
57.5(13)
14.1(7)
9.3(8)
40(4)
22(4)
52.1(13)
4.2(6)
7.1(8)
4.6(10)
9.5(7)
3.6(6)
1.0(3)
0.22(5)
0.24(3)
0.109(9)
0.06(3)
0.091(10)
0.10(4)
0.13(2)
0.36(5)
0.075(15)
0.073(7)
0.120(9)
0.16(4)
0.11(10)
0.11(6)
0.19(3)
0.31(13)
0.154(18)
0.076(10)
0.9(4)
0.134(19)
0.10(4)
0.15(2)
0.20(4)
0.100(16)
0.18(4)
0.43(10)
0.13(4)
0.108(11)
0.6(4)
0.11(4)
0.132(7)
0.11(3)
0.17(3)
0.11(3)
0.12(3)
0.138(15)
0.21(6)
0.26(6)
0.8(4)
0.16(4)
0.126(9)
0.132(19)
0.13(3)
0.16(3)
0.13(4)
0.144(11)
0.09(3)
0.25(7)
0.4(2)
0.17(4)
0.12(4)
0.6(7)
0.4(3)
1.0(5)
0.8(2)
3(12)
1.3(3)
0.4(3)
1.4(7)
0.30(
6)
0.9(3)
1.28(
19)
1.05(
19)
3.5(1
5)
0.4(4)
1.4(8)
0.7(2)
0.6(7)
1.9(6)
0.82(
13)
1.2(1
0)
0.9(3)
1.3(1
1)
0.3(3)
0.9(5)
1.1(6)
4(2)
2.0(9)
1.1(1
1)
1.4(7)
0.9(1
4)
0.2(2)
1.22(
18)
1.0(9)
1.0(8)
1.9(1
0)
1.2(6)
1.0(2)
1.2(6)
2.2(8)
5(7)
1.8(7)
1.4(2)
1.0(3)
1.1(5)
1.0(4)
0.6(3)
0.89(
18)
2.1(1
1)
0.4(5)
1.6(1
6)
1.0(3)
0.3(4)
Peak
Universitas Sumatera Utara
66
Lampiran 5. Difraktogram Nanosilikon Hasil Pemurnian Metode Pertama
Analysis date
2016/08/31 10:46:15
Sample name
Si-KCl (S)
Measurement date
2016/08/31 10:35:51
File name
625-XRD-2016.ras
Operator
administrator
Comment
Measurement profile
Measurement Profile
Measurement Profile
Meas. data:625-XRD-2016/Data 1
BG data:625-XRD-2016/Data 1
Calc. data:625-XRD-2016/Data 1
15000
Intensity (cps)
10000
5000
0
20
40
60
2-theta (deg)
Peak List
No.
2theta(deg)
d(ang.)
Height(cps
)
FWHM(de
g)
Int. I(cps
deg)
Int. W(deg)
Asym.
factor
1
20.578(10)
4.313(2)
1465(110)
0.060(12)
126(11)
0.086(14)
1.5(15)
2
26.388(7)
3.3748(9)
3726(176)
0.110(14)
681(22)
0.183(15)
1.6(5)
3
28.192(5)
3.1628(5)
2715(27)
0.250(9)
1.50(14)
36.59(3)
2.4540(18)
10871(301
)857(85)
0.199(3)
4
0.20(3)
250(11)
0.29(4)
1.3(8)
5
44.53(2)
2.0330(10)
540(67)
0.18(3)
136(9)
0.25(5)
0.8(5)
6
47.057(6)
1.9296(2)
6257(228)
0.199(5)
1523(18)
0.243(12)
1.34(15)
7
55.867(6)
3561(172)
0.183(7)
862(13)
0.242(15)
1.13(15)
8
59.10(4)
1.64437(16
)1.5620(11)
284(49)
0.26(6)
104(12)
0.36(10)
1.5(13)
9
64.981(19)
1.4340(4)
605(71)
0.16(2)
160(8)
0.26(4)
1.4(8)
10
67.36(3)
1.3890(5)
307(51)
0.16(4)
76(8)
0.25(7)
0.7(6)
11
68.889(11)
0.165(11)
266(9)
0.23(3)
1.1(4)
76.146(8)
1.36188(19
)1.24913(11
1161(98)
12
1719(120)
0.180(8)
417(10)
0.24(2)
1.3(3)
)
Universitas Sumatera Utara
67
Lampiran 6. Hasil Analisa Kuantitatif Nanosilikon Hasil Pemurnian Metode
PertamaGeneral information
Analysis date
2016/09/21 13:35:26
Sample name
Si-KCl (S)
Measurement date
File name
625-XRD-2016.asc
Operator
2016/08/31 10:44:00
Comment
Qualitative analysis results
Phase name
Formul
a
Figure of
merit
Phase reg. detail
DB card number
Silicon
Si
0.493
User (COD)
9013108
Quartz low
Si O2
1.955
01-070-2540
Silicon
Oxide
Quartz, syn
Si O2
1.101
Si O2
1.165
ICDD (PDF-2/Release
2012 RDB)
ICDD (PDF-2/Release
2012 RDB)
ICDD (PDF-2/Release
2012 RDB)
01-075-3165
01-088-2487
Weight ratio
625-XRD-2016
100
90
Phase name
Content(%)
-
Silicon
40.4(4)
-
Quartz low
38(2)
-
Silicon Oxide
6.7(3)
-
Quartz, syn
15.4(4)
80
70
60
50
40
30
20
10
0
625-XRD-2016
Silicon(%)
Quartz low(%)
Silicon Oxide(%)
Quartz, syn(%)
Measurement profile
Meas. data:625-XRD-2016/Data 1
15000
Intensity (cps)
10000
5000
0
Silicon
Quartz low
Silicon Oxide
Quartz, syn
20
40
60
2-theta (deg)
Universitas Sumatera Utara
68
Lampiran 7. Difraktogram Nanosilikon Hasil Pemurnian Metode Kedua
General information
Analysis date
2016/09/30 10:08:57
Sample name
Si KCl (dJ )
Measurement date
2016/09/30 09:29:21
File name
690-xrd-2016.ras
Operator
Administrator
Comment
Measurement profile
40000
Meas. data:690-xrd-2016/Data 1
BG data:690-xrd-2016/Data 1
Calc. data:690-xrd-2016/Data 1
30000
Intensity (cps)
20000
10000
0
20
40
60
2-theta (deg)
Peak list
No.
2theta(deg)
d(ang.)
Height(cps)
FWHM(deg
)
Int. I(cps
deg)
Int. W(deg)
Asym.
Factor
1
28.386(5)
3.1416(5)
24765(454)
0.212(4)
6243(69)
0.252(7)
4.4(7)
2
36.678(15)
2.4482(10)
493(64)
0.24(2)
177(10)
0.36(7)
0.59(12)
3
42.297(6)
2.1351(3)
873(85)
0.070(9)
88(5)
0.101(16)
0.4(2)
4
44.67(5)
2.027(2)
283(49)
0.27(7)
116(9)
0.41(10)
1.0(9)
5
47.186(5)
15127(355)
0.188(4)
3609(34)
0.239(8)
1.53(15)
6
56.013(4)
1.92459(17
)1.64042(11
8513(266)
0.199(4)
2091(21)
0.246(10)
1.56(13)
7
59.18(4)
)
1.5601(9)
194(40)
0.27(5)
71(8)
0.37(12)
0.5(4)
8
65.159(13)
1.4305(3)
387(57)
0.24(2)
120(7)
0.31(6)
3.1(8)
9
69.001(8)
0.201(9)
510(11)
0.26(2)
1.18(19)
76.235(5)
1.35995(13
)1.24790(7)
1980(128)
10
3486(170)
0.168(5)
786(12)
0.225(15)
1.10(16)
Universitas Sumatera Utara
69
Lampiran 8. Hasil Analisa Kuantitatif Nanosilikon Hasil Pemurnian Metode Kedua
neral information
Analysis date
2016/10/10 11:47:04
Sample name
Si KCl (dJ )
Measurement date
File name
690-xrd-2016.asc
Operator
2016/09/30 09:39:00
Comment
Qualitative analysis results
Phase name
Formul
a
Figure of
merit
Phase reg. Detail
DB card
number
Silicon
Silicon Oxide
Quartz alpha, alphaSi
O2
Stishovite
Quartz low
Si
Si O2
Si O2
Si O2
Si O2
0.156
1.281
1.335
3.673
1.867
User (COD)
ICDD (PDF2/Release
2012 RDB)
ICDD (PDF2/Release
2012 RDB)
ICDD (PDF2/Release
2012 RDB)
ICDD
(PDF2/Release 2012 RDB)
9013104
01-075-3165
01-089-8937
01-072-2310
01-070-2540
Weight ratio
70
65
690-xrd-2016
60
55
50
45
40
Content(%)
64.7(6)
3.0(3)
1.7(3)
9(2)
22(4)
35
30
25
20
15
10
5
0
690-xrd-2016
Silicon(%)
Silicon Oxide(%)
Quartz a...Si O2(%)
Stishovite(%)
Quartz low(%)
Measurement profile
40000
Meas. data:690-xrd-2016/Data 1
30000
20000
Intensity (cps)
-
Phase name
Silicon
Silicon Oxide
Quartz alpha, alpha-Si O2
Stishovite
Quartz low
10000
0
Silicon
Silicon Oxide
Quartz alpha, alpha-Si O2
Stishovite
Quartz low
20
30
40
50
60
70
2-theta (deg)
Universitas Sumatera Utara
Universitas Sumatera Utara
62
Lampiran 1. Data JCPDS Silikat (Morris,1976)
Universitas Sumatera Utara
63
Lampiran 2. Data JCPDS Silikon (Morris,1976)
Universitas Sumatera Utara
64
Lampiran 3. Difraktogram Silika Hasil Pemurnian dari Pasir Kuarsa
tion
Analysis date
2016/03/28 11:23:32
Sample name
Spl SiO2
Measurement date
2016/03/28 11:11:14
File name
171-xrd-2016.ras
Operator
administrator
Comment
Universitas Sumatera Utara
65
Lampiran 4. Puncak Difraktogram Silika Hasil Pemurnian dari Pasir Kuarsa
No.
2-theta(deg)
d(ang.)
Height(counts
)
FWHM(deg)
Int. I(counts
deg)
Int. W(deg)
Asym
.
factor
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
5.71(5)
13.442(13)
20.733(15)
22.482(7)
23.340(4)
23.434(4)
24.123(13)
24.327(12)
26.249(13)
26.415(6)
26.538(2)
26.937(5)
27.336(10)
27.463(7)
27.592(6)
27.801(14)
30.134(19)
30.479(7)
30.829(2)
35.03(4)
36.339(9)
36.906(15)
39.223(4)
40.070(17)
41.325(8)
41.993(15)
42.51(4)
45.33(2)
45.693(7)
47.88(6)
49.560(6)
50.001(3)
52.403(13)
54.704(18)
57.815(13)
58.163(13)
59.840(4)
60.531(17)
61.858(15)
65.39(4)
67.587(12)
67.939(4)
69.367(8)
72.708(13)
73.324(8)
73.457(8)
74.625(5)
78.638(8)
79.66(3)
81.16(10)
83.645(10)
87.206(6)
15.46(13)
6.582(7)
4.281(3)
3.9515(11)
3.8082(6)
3.7931(6)
3.6863(19)
3.6558(18)
3.3923(17)
3.3715(7)
3.3561(3)
3.3072(6)
3.2598(12)
3.2451(8)
3.2302(7)
3.2064(15)
2.9633(18)
2.9305(7)
2.8981(2)
2.559(3)
2.4703(6)
2.4336(10)
2.2950(2)
2.2484(9)
2.1830(4)
2.1498(7)
2.1247(19)
1.9991(9)
1.9839(3)
1.898(2)
1.8378(2)
1.82265(12)
1.7446(4)
1.6765(5)
1.5935(3)
1.5848(3)
1.54433(10)
1.5283(4)
1.4987(3)
1.4261(8)
1.3849(2)
1.37860(7)
1.35366(14)
1.2995(2)
1.29008(13)
1.28806(12)
1.27078(8)
1.21567(11)
1.2027(4)
1.1841(12)
1.15517(11)
1.11692(6)
42(7)
73(9)
185(14)
425(21)
65(8)
393(20)
111(11)
285(17)
197(14)
229(15)
676(26)
395(20)
104(10)
228(15)
413(20)
145(12)
20(4)
174(13)
125(11)
14(4)
117(11)
27(5)
107(10)
55(7)
102(10)
58(8)
39(6)
43(7)
334(18)
10(3)
44(7)
834(29)
55(7)
71(8)
50(7)
54(7)
184(14)
34(6)
43(7)
10(3)
54(7)
455(21)
107(10)
70(8)
256(16)
169(13)
361(19)
47(7)
29(5)
12(3)
56(7)
30(5)
0.74(15)
0.11(4)
0.13(3)
0.099(5)
0.042(18)
0.063(5)
0.09(3)
0.110(16)
0.321(15)
0.063(8)
0.060(3)
0.100(5)
0.128(15)
0.09(6)
0.09(3)
0.157(13)
0.22(6)
0.121(10)
0.055(4)
0.67(11)
0.110(10)
0.075(18)
0.119(12)
0.13(3)
0.069(9)
0.168(18)
0.40(4)
0.10(3)
0.083(7)
0.53(16)
0.09(2)
0.104(3)
0.07(2)
0.117(18)
0.102(11)
0.106(11)
0.083(7)
0.13(2)
0.20(3)
0.71(13)
0.122(14)
0.093(4)
0.114(7)
0.115(12)
0.135(17)
0.113(13)
0.107(5)
0.069(12)
0.18(3)
0.37(9)
0.133(15)
0.11(2)
42(7)
15.9(16)
45(2)
46.4(15)
4.1(16)
36(2)
11(3)
37(4)
72(4)
17(2)
50(3)
47.3(13)
17(2)
24(21)
45(24)
26.9(16)
6.4(12)
26.7(11)
9.5(4)
12.0(17)
15.7(8)
2.6(6)
15.6(10)
11.2(9)
10.2(7)
10.7(9)
17.1(13)
5.6(11)
36.0(18)
6(2)
4.8(9)
110(2)
6.4(7)
12.1(9)
5.5(5)
6.2(6)
25.4(9)
7.1(8)
11.3(9)
7.6(16)
8.8(8)
57.5(13)
14.1(7)
9.3(8)
40(4)
22(4)
52.1(13)
4.2(6)
7.1(8)
4.6(10)
9.5(7)
3.6(6)
1.0(3)
0.22(5)
0.24(3)
0.109(9)
0.06(3)
0.091(10)
0.10(4)
0.13(2)
0.36(5)
0.075(15)
0.073(7)
0.120(9)
0.16(4)
0.11(10)
0.11(6)
0.19(3)
0.31(13)
0.154(18)
0.076(10)
0.9(4)
0.134(19)
0.10(4)
0.15(2)
0.20(4)
0.100(16)
0.18(4)
0.43(10)
0.13(4)
0.108(11)
0.6(4)
0.11(4)
0.132(7)
0.11(3)
0.17(3)
0.11(3)
0.12(3)
0.138(15)
0.21(6)
0.26(6)
0.8(4)
0.16(4)
0.126(9)
0.132(19)
0.13(3)
0.16(3)
0.13(4)
0.144(11)
0.09(3)
0.25(7)
0.4(2)
0.17(4)
0.12(4)
0.6(7)
0.4(3)
1.0(5)
0.8(2)
3(12)
1.3(3)
0.4(3)
1.4(7)
0.30(
6)
0.9(3)
1.28(
19)
1.05(
19)
3.5(1
5)
0.4(4)
1.4(8)
0.7(2)
0.6(7)
1.9(6)
0.82(
13)
1.2(1
0)
0.9(3)
1.3(1
1)
0.3(3)
0.9(5)
1.1(6)
4(2)
2.0(9)
1.1(1
1)
1.4(7)
0.9(1
4)
0.2(2)
1.22(
18)
1.0(9)
1.0(8)
1.9(1
0)
1.2(6)
1.0(2)
1.2(6)
2.2(8)
5(7)
1.8(7)
1.4(2)
1.0(3)
1.1(5)
1.0(4)
0.6(3)
0.89(
18)
2.1(1
1)
0.4(5)
1.6(1
6)
1.0(3)
0.3(4)
Peak
Universitas Sumatera Utara
66
Lampiran 5. Difraktogram Nanosilikon Hasil Pemurnian Metode Pertama
Analysis date
2016/08/31 10:46:15
Sample name
Si-KCl (S)
Measurement date
2016/08/31 10:35:51
File name
625-XRD-2016.ras
Operator
administrator
Comment
Measurement profile
Measurement Profile
Measurement Profile
Meas. data:625-XRD-2016/Data 1
BG data:625-XRD-2016/Data 1
Calc. data:625-XRD-2016/Data 1
15000
Intensity (cps)
10000
5000
0
20
40
60
2-theta (deg)
Peak List
No.
2theta(deg)
d(ang.)
Height(cps
)
FWHM(de
g)
Int. I(cps
deg)
Int. W(deg)
Asym.
factor
1
20.578(10)
4.313(2)
1465(110)
0.060(12)
126(11)
0.086(14)
1.5(15)
2
26.388(7)
3.3748(9)
3726(176)
0.110(14)
681(22)
0.183(15)
1.6(5)
3
28.192(5)
3.1628(5)
2715(27)
0.250(9)
1.50(14)
36.59(3)
2.4540(18)
10871(301
)857(85)
0.199(3)
4
0.20(3)
250(11)
0.29(4)
1.3(8)
5
44.53(2)
2.0330(10)
540(67)
0.18(3)
136(9)
0.25(5)
0.8(5)
6
47.057(6)
1.9296(2)
6257(228)
0.199(5)
1523(18)
0.243(12)
1.34(15)
7
55.867(6)
3561(172)
0.183(7)
862(13)
0.242(15)
1.13(15)
8
59.10(4)
1.64437(16
)1.5620(11)
284(49)
0.26(6)
104(12)
0.36(10)
1.5(13)
9
64.981(19)
1.4340(4)
605(71)
0.16(2)
160(8)
0.26(4)
1.4(8)
10
67.36(3)
1.3890(5)
307(51)
0.16(4)
76(8)
0.25(7)
0.7(6)
11
68.889(11)
0.165(11)
266(9)
0.23(3)
1.1(4)
76.146(8)
1.36188(19
)1.24913(11
1161(98)
12
1719(120)
0.180(8)
417(10)
0.24(2)
1.3(3)
)
Universitas Sumatera Utara
67
Lampiran 6. Hasil Analisa Kuantitatif Nanosilikon Hasil Pemurnian Metode
PertamaGeneral information
Analysis date
2016/09/21 13:35:26
Sample name
Si-KCl (S)
Measurement date
File name
625-XRD-2016.asc
Operator
2016/08/31 10:44:00
Comment
Qualitative analysis results
Phase name
Formul
a
Figure of
merit
Phase reg. detail
DB card number
Silicon
Si
0.493
User (COD)
9013108
Quartz low
Si O2
1.955
01-070-2540
Silicon
Oxide
Quartz, syn
Si O2
1.101
Si O2
1.165
ICDD (PDF-2/Release
2012 RDB)
ICDD (PDF-2/Release
2012 RDB)
ICDD (PDF-2/Release
2012 RDB)
01-075-3165
01-088-2487
Weight ratio
625-XRD-2016
100
90
Phase name
Content(%)
-
Silicon
40.4(4)
-
Quartz low
38(2)
-
Silicon Oxide
6.7(3)
-
Quartz, syn
15.4(4)
80
70
60
50
40
30
20
10
0
625-XRD-2016
Silicon(%)
Quartz low(%)
Silicon Oxide(%)
Quartz, syn(%)
Measurement profile
Meas. data:625-XRD-2016/Data 1
15000
Intensity (cps)
10000
5000
0
Silicon
Quartz low
Silicon Oxide
Quartz, syn
20
40
60
2-theta (deg)
Universitas Sumatera Utara
68
Lampiran 7. Difraktogram Nanosilikon Hasil Pemurnian Metode Kedua
General information
Analysis date
2016/09/30 10:08:57
Sample name
Si KCl (dJ )
Measurement date
2016/09/30 09:29:21
File name
690-xrd-2016.ras
Operator
Administrator
Comment
Measurement profile
40000
Meas. data:690-xrd-2016/Data 1
BG data:690-xrd-2016/Data 1
Calc. data:690-xrd-2016/Data 1
30000
Intensity (cps)
20000
10000
0
20
40
60
2-theta (deg)
Peak list
No.
2theta(deg)
d(ang.)
Height(cps)
FWHM(deg
)
Int. I(cps
deg)
Int. W(deg)
Asym.
Factor
1
28.386(5)
3.1416(5)
24765(454)
0.212(4)
6243(69)
0.252(7)
4.4(7)
2
36.678(15)
2.4482(10)
493(64)
0.24(2)
177(10)
0.36(7)
0.59(12)
3
42.297(6)
2.1351(3)
873(85)
0.070(9)
88(5)
0.101(16)
0.4(2)
4
44.67(5)
2.027(2)
283(49)
0.27(7)
116(9)
0.41(10)
1.0(9)
5
47.186(5)
15127(355)
0.188(4)
3609(34)
0.239(8)
1.53(15)
6
56.013(4)
1.92459(17
)1.64042(11
8513(266)
0.199(4)
2091(21)
0.246(10)
1.56(13)
7
59.18(4)
)
1.5601(9)
194(40)
0.27(5)
71(8)
0.37(12)
0.5(4)
8
65.159(13)
1.4305(3)
387(57)
0.24(2)
120(7)
0.31(6)
3.1(8)
9
69.001(8)
0.201(9)
510(11)
0.26(2)
1.18(19)
76.235(5)
1.35995(13
)1.24790(7)
1980(128)
10
3486(170)
0.168(5)
786(12)
0.225(15)
1.10(16)
Universitas Sumatera Utara
69
Lampiran 8. Hasil Analisa Kuantitatif Nanosilikon Hasil Pemurnian Metode Kedua
neral information
Analysis date
2016/10/10 11:47:04
Sample name
Si KCl (dJ )
Measurement date
File name
690-xrd-2016.asc
Operator
2016/09/30 09:39:00
Comment
Qualitative analysis results
Phase name
Formul
a
Figure of
merit
Phase reg. Detail
DB card
number
Silicon
Silicon Oxide
Quartz alpha, alphaSi
O2
Stishovite
Quartz low
Si
Si O2
Si O2
Si O2
Si O2
0.156
1.281
1.335
3.673
1.867
User (COD)
ICDD (PDF2/Release
2012 RDB)
ICDD (PDF2/Release
2012 RDB)
ICDD (PDF2/Release
2012 RDB)
ICDD
(PDF2/Release 2012 RDB)
9013104
01-075-3165
01-089-8937
01-072-2310
01-070-2540
Weight ratio
70
65
690-xrd-2016
60
55
50
45
40
Content(%)
64.7(6)
3.0(3)
1.7(3)
9(2)
22(4)
35
30
25
20
15
10
5
0
690-xrd-2016
Silicon(%)
Silicon Oxide(%)
Quartz a...Si O2(%)
Stishovite(%)
Quartz low(%)
Measurement profile
40000
Meas. data:690-xrd-2016/Data 1
30000
20000
Intensity (cps)
-
Phase name
Silicon
Silicon Oxide
Quartz alpha, alpha-Si O2
Stishovite
Quartz low
10000
0
Silicon
Silicon Oxide
Quartz alpha, alpha-Si O2
Stishovite
Quartz low
20
30
40
50
60
70
2-theta (deg)
Universitas Sumatera Utara