Untuk mengetahui. pengaruh lama pemang.s?n terhadap hasil reaksi, maka prosentase hasil, reaksi yang diperOf- leh, dihitung dengan analisa varian raircangan disain fak torial A x B,

  51 RI NGKASAN

  Pe mb u a t a n s e nya wa kuma r i n s i nt e t i k di l a bor a t or i um de nga n bah. an da s a r da r i a l de hi d a r oma t i k da n a s e t a t a n - hi dr a t p a d a t e mpe r a t ur t i r r ggi » ba nya k p u s t a ka y a n g me m - b a h a s da n me n c a n t u mk a n c a r a pe mbua t a nnya , Te t a pi da r i be r ba ga i p u s t a k a t e r s e but ba ha n da s a r ma u p u n ka t a l i s y a n g di gun a ka n da l a m r e a k s i n y a b e r b e d a - be da .

  Pa d a p e n e l i t i a n i ni , di l a kuka n p e mbua t a n kuma r i n da r i s a l i s i l a l de hi d d a n a s e t a t a nhi dr a t de nga n ka t a l i s t r i e t i l a mi na da n n a t r i u m a s e t a t p a d a t e mpe r a t ur t i nggi ,

  Unt u k ma s i n g - ma s i n g ka t a l i s di l a kuka n p a d a l a ma pe ma n a s a n s e l a ma 6, 8, 10 da n 12 j am, Da r i ha s i l r e a ks i i ni ma k a di l a kuka n p e mu r n i a n me ngg u n a k a n pe l a r ut me t a nol

  40 i»

  , k £ mu d i a n di ke r i ngka n da l a m ove n da n s e t e l a h k e r i n g di t i m -■ b a n g de nga n t i mba nga n a na l i t i s .

  Da r i ha s i l p e mu r n i a n p a d a l a ma p e ma na s a n t e r s e but di l a kuka n uj i ke mu r n i a n de nga n r e a ks i wa r na me ngguna ka n pe r e a ks i dr a ge ndor f , kr oma t ogr a f i l a p i s a n t i pi s , t i t i k l e l e h , s pe kt r a i n f r a me r a h da n s pe kt r a da r i s i na r l e mb a y u n g ul t r a ,

  Un t u k me nge t a hui . pe nga r uh l a ma pemang. s ?n t e r ha da p ha s i l r e a ks i , ma k a pr os e nt a s e ha s i l , r e a ks i y a n g di per Of - l eh, d i h i t u n g de nga n a na l i s a va r i a n r a i r cangan di s a i n f a k t or i a l A

  x

  B,

  

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  52 Ba r i p e r hi t unga n s t a t i s t i k t e r nya t a p a d a l a ma pe ma na s a n

  , da n j a m a da pe r be da a n y a n g b e r ma k n a s e da ngka n

  6 8 ,10

  12

  a nt a r a k a t a l i s na t r i um a s e t a t da n t r i e t i l a mi na t e r ha da p pr os e nt a s e h a s i l r e a ks i a da pe r be da a n y a n g be r ma kna pul a . Ha l i ni da pa t di l i ha t p a d a t a be l de nga n de r a j at ke ma kna - .

  i an 95 ( 0, 05 ) .

  DAFTAR PUSTAKA

  La i de r , K. J . , Che mi c a l Ki ne t i c s , Me. Gr ow Hi l l Book Co I nc, , Ne w Yor k , Tor ont o, London, 1950, 247­ 295.

  Ma r t i n, A. N. , Swa r br i c k, J . , Ca mma r a t a , A • , Phys i c a l Pha r ma c y, Phys i c a l Che mi c a l Pr i nc i pl e i n. The

  Pha r ma c e ut i c a l Sc i e nc e , 2nd ed. , Le a & Fe bi - ge r , Phi l a de l pi a , 1969, 354- - 387. Vi s hnoi , N. K. , Adva nc e d Pr a c t i c a l Or ga ni c Che mi s t r y,

  1s t ed. I ndi a : Vi ka s Publ i s hi ng Hos e PVT Lt d, 1979, 129- 130, 355- 356. Nol l e r , C. R. , Che mi s t r y Of Or ga ni c Comphounds , London:

  W. B. Sa unde r s Co, Ma r uz e n Compa ny Lt d, 1965, 610- 614. '

  1. U Mor r i s on, R. T. , Boyd, R. N. Or ga ni c Che mi s t r y » 4 ed.

  Bos t on : Al l yn a nd Ba c on I nc, 1983, 896. a4- Fi e s e r , L. F. , a nd Fi e s e r , M. Or ga ni c Che mi s t r y, 3 ed.

  Ne w Yor k : Re i nhol d Publ i s hi ng Cor por a t i on, 1956, 78- 79, 105. Voge l , A. I . , A Te xt Book Of Pr a c t i c a l Che mi s t r y I nc l u­ di ng Qua l i t a t i f Or ga ni c Ana l i s i a , 3r d ed. Lon­ don : Engl i s h La ngua ge Book Soc i e t y a nd Lo n g ­ ma ns , Gr e e n & Co Lt d, 1956, 703, 713*

  An o n i m. , Or ga ni c Synt e s e s Col l e c t i ve , A Ri vi s e d Edi t i ­ on Of Annua l Vol ume 20 - 40. Hor ni ng, E. C. edi

  

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  54

  t or i a l . Vol ume 3. Ne w Yor k : J ohn Wi l e y & Sons I nc, 1982, 209- 211.

  9. Ma r t i nda l e . , The Ext r a Pha r ma c opoe i a . Wa de Ai nl a y, 28 ed. London : The Pha r ma c e ut i c a l Pr e s s , 1972, 224.

  10. Wi ndhol z . , The Me r c k I nde x An Enc yc l ope di a of Ch e mi ­ c a l s a nd Dr ug , 9t h ed. Ra hwa y. N. J . Me r k & Co, I nc , 1976, 2547.

  12. Wi ba ut , V. G. , Pr a c t i c um de r Or ga ni s he Che mi e . Ams t e r ­ da m : Wol ke r s - Noor dhof f . nv, Gr oni nge n, 1972, 224. 13*Pe s s e nde n, R. J . , Pe s s e nde n, J . S. , Ki mi a Or ga ni k, pe nt e r j . Al oys i us Ha dya na PudJ a a dma ka , j i l i d 2. Edi s i 2. J a ka r t a : Pe ne r bi t Er l a ngga , 1984, 189 - 191.

  H. Ma c e k , K. , Pha r ma c e ut i c a l Appl i c a t i on of Thi n La ye r a nd Pa pe r Chr oma t ogr a phy. El s e vi e r Publ i s hi ng Co. , Ams t e r da m, London, Ne w Yo r k , 1972, 563­ 565. 1 5 . Ha r dj ono, S. , Spe kt r os kopi . Edi s i 1. Yogya ka r t a : Li be r t y, 1958, 22- 26, 41, 61, 73- 77, 85.

  1

  6

  . Hadi Sut r i s no. , Bas i c: Expe r i me nt a l De s i gn a nd Ana l y­ s i s , Sur a ba ya , Ai r l a ngga Uni ve r s i t y Pr e s s , 1976.

  

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11. Cl a us , E. P. , Pha r ma c ognos y. 4 t h ed. Phi l a de l pi a : Le a & Fe bi ge r , 1961, 149, 151, 242.

  55

  17. St a hl , E. , Ana l l s i s Oba t Se c a r a Kr oma t ogr a f i Da n Mi kr os kopi . Ba ndung : Pe n e r Mt I TB , 1985* 1- 7, 16- 17.

  18. Ba r r ow, M. , Phys i c a l Che mi s t r y. Se c ond Edi t i on, To k ­ yo : Koga kus ha Compa ny, l t d, 1966, 451- 457.

  19. Da ni e l , W. W. , Bl os t a t l s t l k : A Founda t i on For An a ­ l ys i s I n The He a l t h Sc i e nc e s , Se c ond Edi t i on Ne w Yor k s J ohn Wi l e y & Sons , 1978, 223- 224, 447.

  20. Muha ma d Mul ya , Ac hma d Sya hr a ni . , Apl i ka s i Ana l l s i s Spe kt r of ot ome t r i UV- VI S, Edi s i 1987, Sur a ba ya , 1- 27.

  21. Sut r i s no*, Fi s i ka Me ka nl ka , Ba ndung : Pe ne r bl t I TB, 1979, 18 5 - 18 8 .

  22. Al e xa nde r , I . , Wa t e r ma n, P. G. , Phyt oc he mi s t r y, Sc ot l a nd : De pa r t e me n of Pha r ma c e ut i c a l Ch e ­ mi s t r y, Uni ve r s i t a a of St r a t he l yde , 1978, 8 4 5 ­

  8 6 0 .

  Sant a

  Ba r ba r a : Uni ve r s i t a s of Ca l i f or ni a , 1969, 241, 244- 245.

  

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23. Mi l l e r , G. H. , Che mi s t r y,

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