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Journal .29. Page. 709-716.
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Syah Reza. 2012. Preparasi dan Karakterisasi Bentonit Tapanuli Terinterkalasi Surfaktan Kationik ODMTABr dan Aplikasinya Sebagai Adsorben
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and disproportionation reactions between SSZ-33, TNU-9, mordenite and ZSM-5 zeolite catalysts. Chemistry English Journal.166. Page. 348-357.
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54
LAMPIRAN
55
LAMPIRAN 1 Hasil dari Analisis XRD
Peak List
General information
Analysis date 20160229 10:06:16
Sample name zeolit kasinasi
Measurement date 20160229 09:55:16
File name 066-xrd-2016.ras
Operator Administrator
Comment
Measurement profile
Peak list
No. 2-thetadeg
dang. Heightcount
s FWHMdeg
Int. Icounts deg
Int. Wdeg Asym.
factor 1
6.606 13.3813
416 0.5813
446 1.13
45 2
9.83315 8.98814
21215 0.292
904 0.425
0.82 3
13.553 6.53015
819 0.645
695 0.8616
2.04 4
19.655 4.51412
537 0.264
143 0.2710
1.08 5
21.943 4.0486
20214 0.446
13120 0.6515
1.57 6
22.312 3.9814
24116 0.494
15921 0.6613
0.2915 7
25.69916 3.4642
19214 0.23217
477 0.255
1.23 8
26.319 3.38511
829 1.3714
1208 1.53
0.62 9
27.682 3.2213
16313 0.582
1016 0.628
0.367
2-theta deg
Intensity counts
20 40
60 80
-100 100
200 300
400
56
10 30.034
2.9734 668
0.584 413
0.6313 0.72
11 30.905
2.8924 457
0.274 12.817
0.298 0.96
12 35.7010
2.5137 346
1.569 575
1.74 0.5717
13 50.89211
1.79284 396
0.134 9.710
0.257 0.89
14 64.32
1.4474 83
1.14 163
2.110 0.23
57
Peak List
General information
Analysis date 20160229 09:52:29
Sample name zeolit tanpa kasinasi
Measurement date 20160229 09:39:16
File name 065-xrd-2016.ras
Operator Administrator
Comment
Measurement profile
Peak list
No. 2-thetadeg
dang. Heightcount
s FWHMdeg
Int. Icounts deg
Int. Wdeg Asym.
Factor 1
5.279 16.83
10510 9.36
1902103 183
5197 2
9.98415 8.85314
22915 0.42513
1034 0.455
1.73 3
11.344 7.803
426 0.274
122 0.2910
2.315 4
13.565 6.522
9310 0.816
1065 1.1417
1.13 5
19.153 4.6308
457 0.105
82 0.188
0.46 6
19.842 4.4724
678 0.274
232 0.348
4.316 7
20.9416 4.243
275 2.13
11018 4.014
0.2010 8
22.5587 3.938412
30618 0.782
30412 0.9910
4.24 9
23.833 3.7315
437 0.356
193 0.4414
53 10
25.75514 3.456319
21415 0.552
2167 1.0110
0.385 11
27.78519 3.2082
18314 0.643
1705 0.9310
0.446
2-theta deg
Intensity counts
20 40
60 80
100 200
300 400
500
58
12 30.113
2.9663 879
0.653 613
0.7011 0.6311
13 31.033
2.8793 608
0.262 16.714
0.286 1.25
14 32.053
2.7913 547
0.233 15.412
0.296 0.74
15 32.846
2.7255 245
0.336 10.014
0.4214 1.19
16 35.949
2.4976 396
1.748 714
1.94 0.7416
17 51.02
1.7898 123
1.22 164
1.47 1.19
18 67.96
1.37810 73
5.56 396
63 3.118
59
Peak List
General information
Analysis date 20160328 10:49:46
Sample name CuO Z:3 : 1 A
Measurement date 20160328 10:28:03
File name 168-xrd-2016.ras
Operator Administrator
Comment
Measurement profile
Peak list
No. 2-thetadeg
dang. Heightcount
s FWHMdeg
Int. Icounts deg
Int. Wdeg Asym.
factor 1
13.304 6.652
517 0.399
325 0.6318
2.211 2
21.534 4.1238
12511 0.844
1306 1.0414
0.3812 3
25.47318 3.4942
15112 0.26018
483 0.324
2.17 4
26.025 3.4217
527 0.7711
577 1.13
0.2311 5
27.602 3.2293
17613 0.432
916 0.527
2.78 6
30.753 2.9053
285 0.549
183 0.62
510 7
35.463 2.529418
386 0.889
483 1.33
0.63
Meas. data:168-xrd-2016Data 1 BG data:168-xrd-2016Data 1
Calc. data:168-xrd-2016Data 1
2-theta deg
Intensity counts
20 40
60 80
200 400
600 800
60
Peak List
General information
Analysis date 20160328 11:01:21
Sample name CuO Z:1 : 1 B
Measurement date 20160328 10:48:35
File name 169-xrd-2016.ras
Operator Administrator
Comment
Measurement profile
Peak list
No. 2-thetadeg
dang. Heightcount
s FWHMdeg
Int. Icounts deg
Int. Wdeg Asym.
factor 1
6.329 14.02
386 1.73
799 2.16
45 2
13.247 6.684
457 0.7810
545 1.23
0.95 3
21.633 4.1056
15212 0.923
1684 1.1012
0.7712 4
23.433 3.7935
305 0.5411
213 0.72
43 5
25.463 3.4963
13712 0.322
483 0.355
1.45 6
26.058 3.41710
497 0.579
314 0.6316
0.64 7
27.523 3.2394
13512 0.653
955 0.7010
1.84 8
35.352 2.537015
487 1.096
703 1.53
0.299
Meas. data:169-xrd-2016Data 1 BG data:169-xrd-2016Data 1
Calc. data:169-xrd-2016Data 1
2-theta deg
Intensity counts
20 40
60 80
200 400
600
61
Peak List
General information
Analysis date 20160328 11:16:41
Sample name CuO Z:1 : 3 C
Measurement date 20160328 11:00:22
File name 170-xrd-2016.ras
Operator Administrator
Comment
Measurement profile
Peak list
No. 2-thetadeg
dang. Heightcount
s FWHMdeg
Int. Icounts deg
Int. Wdeg Asym.
factor 1
6.4310 13.72
578 0.4714
436 0.72
23 2
9.695 9.124
789 0.394
325 0.4111
1.05 3
13.396 6.613
739 0.557
565 0.7716
0.95 4
19.495 4.55213
517 0.355
193 0.3712
0.85 5
21.653 4.1025
18714 0.854
2028 1.0812
0.297 6
25.603 3.4774
19614 0.243
614 0.314
1.712 7
26.142 3.4063
477 0.5512
455 1.03
0.33 8
27.7284 3.21465
114334 0.1045
1398 0.12211
2.13 9
27.79116 3.207518
14412 0.594
1006 0.6910
2.46 10
30.843 2.8972
346 0.699
254 0.73
32 11
35.532 2.524517
427 1.077
594 1.43
0.3618
Meas. data:170-xrd-2016Data 1 BG data:170-xrd-2016Data 1
Calc. data:170-xrd-2016Data 1
2-theta deg
Intensity counts
20 40
60 80
500 1000
1500 2000
62
LAMPIRAN 2 Perhitungn Ukuran Kristal Zeolit Alam dan CuO-Zeolit Alam
Persamaan Scherrer D =
Dimana: D = Ukuran kristal Å
= panjang gelombang sinar-X yang digunakan 1,5406 Å k = konstanta Scherrer 0,9
= puncak pada setengah tinggi intensitas FWHM = Full Width at a Half Maximum
= FWHM
O
rad = sudut difraksi