KESIMPULAN KESIMPULAN DAN SARAN

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UI Depok. 54 LAMPIRAN 55 LAMPIRAN 1 Hasil dari Analisis XRD Peak List General information Analysis date 20160229 10:06:16 Sample name zeolit kasinasi Measurement date 20160229 09:55:16 File name 066-xrd-2016.ras Operator Administrator Comment Measurement profile Peak list No. 2-thetadeg dang. Heightcount s FWHMdeg Int. Icounts deg Int. Wdeg Asym. factor 1 6.606 13.3813 416 0.5813 446 1.13 45 2 9.83315 8.98814 21215 0.292 904 0.425 0.82 3 13.553 6.53015 819 0.645 695 0.8616 2.04 4 19.655 4.51412 537 0.264 143 0.2710 1.08 5 21.943 4.0486 20214 0.446 13120 0.6515 1.57 6 22.312 3.9814 24116 0.494 15921 0.6613 0.2915 7 25.69916 3.4642 19214 0.23217 477 0.255 1.23 8 26.319 3.38511 829 1.3714 1208 1.53 0.62 9 27.682 3.2213 16313 0.582 1016 0.628 0.367 2-theta deg Intensity counts 20 40 60 80 -100 100 200 300 400 56 10 30.034 2.9734 668 0.584 413 0.6313 0.72 11 30.905 2.8924 457 0.274 12.817 0.298 0.96 12 35.7010 2.5137 346 1.569 575 1.74 0.5717 13 50.89211 1.79284 396 0.134 9.710 0.257 0.89 14 64.32 1.4474 83 1.14 163 2.110 0.23 57 Peak List General information Analysis date 20160229 09:52:29 Sample name zeolit tanpa kasinasi Measurement date 20160229 09:39:16 File name 065-xrd-2016.ras Operator Administrator Comment Measurement profile Peak list No. 2-thetadeg dang. Heightcount s FWHMdeg Int. Icounts deg Int. Wdeg Asym. Factor 1 5.279 16.83 10510 9.36 1902103 183 5197 2 9.98415 8.85314 22915 0.42513 1034 0.455 1.73 3 11.344 7.803 426 0.274 122 0.2910 2.315 4 13.565 6.522 9310 0.816 1065 1.1417 1.13 5 19.153 4.6308 457 0.105 82 0.188 0.46 6 19.842 4.4724 678 0.274 232 0.348 4.316 7 20.9416 4.243 275 2.13 11018 4.014 0.2010 8 22.5587 3.938412 30618 0.782 30412 0.9910 4.24 9 23.833 3.7315 437 0.356 193 0.4414 53 10 25.75514 3.456319 21415 0.552 2167 1.0110 0.385 11 27.78519 3.2082 18314 0.643 1705 0.9310 0.446 2-theta deg Intensity counts 20 40 60 80 100 200 300 400 500 58 12 30.113 2.9663 879 0.653 613 0.7011 0.6311 13 31.033 2.8793 608 0.262 16.714 0.286 1.25 14 32.053 2.7913 547 0.233 15.412 0.296 0.74 15 32.846 2.7255 245 0.336 10.014 0.4214 1.19 16 35.949 2.4976 396 1.748 714 1.94 0.7416 17 51.02 1.7898 123 1.22 164 1.47 1.19 18 67.96 1.37810 73 5.56 396 63 3.118 59 Peak List General information Analysis date 20160328 10:49:46 Sample name CuO Z:3 : 1 A Measurement date 20160328 10:28:03 File name 168-xrd-2016.ras Operator Administrator Comment Measurement profile Peak list No. 2-thetadeg dang. Heightcount s FWHMdeg Int. Icounts deg Int. Wdeg Asym. factor 1 13.304 6.652 517 0.399 325 0.6318 2.211 2 21.534 4.1238 12511 0.844 1306 1.0414 0.3812 3 25.47318 3.4942 15112 0.26018 483 0.324 2.17 4 26.025 3.4217 527 0.7711 577 1.13 0.2311 5 27.602 3.2293 17613 0.432 916 0.527 2.78 6 30.753 2.9053 285 0.549 183 0.62 510 7 35.463 2.529418 386 0.889 483 1.33 0.63 Meas. data:168-xrd-2016Data 1 BG data:168-xrd-2016Data 1 Calc. data:168-xrd-2016Data 1 2-theta deg Intensity counts 20 40 60 80 200 400 600 800 60 Peak List General information Analysis date 20160328 11:01:21 Sample name CuO Z:1 : 1 B Measurement date 20160328 10:48:35 File name 169-xrd-2016.ras Operator Administrator Comment Measurement profile Peak list No. 2-thetadeg dang. Heightcount s FWHMdeg Int. Icounts deg Int. Wdeg Asym. factor 1 6.329 14.02 386 1.73 799 2.16 45 2 13.247 6.684 457 0.7810 545 1.23 0.95 3 21.633 4.1056 15212 0.923 1684 1.1012 0.7712 4 23.433 3.7935 305 0.5411 213 0.72 43 5 25.463 3.4963 13712 0.322 483 0.355 1.45 6 26.058 3.41710 497 0.579 314 0.6316 0.64 7 27.523 3.2394 13512 0.653 955 0.7010 1.84 8 35.352 2.537015 487 1.096 703 1.53 0.299 Meas. data:169-xrd-2016Data 1 BG data:169-xrd-2016Data 1 Calc. data:169-xrd-2016Data 1 2-theta deg Intensity counts 20 40 60 80 200 400 600 61 Peak List General information Analysis date 20160328 11:16:41 Sample name CuO Z:1 : 3 C Measurement date 20160328 11:00:22 File name 170-xrd-2016.ras Operator Administrator Comment Measurement profile Peak list No. 2-thetadeg dang. Heightcount s FWHMdeg Int. Icounts deg Int. Wdeg Asym. factor 1 6.4310 13.72 578 0.4714 436 0.72 23 2 9.695 9.124 789 0.394 325 0.4111 1.05 3 13.396 6.613 739 0.557 565 0.7716 0.95 4 19.495 4.55213 517 0.355 193 0.3712 0.85 5 21.653 4.1025 18714 0.854 2028 1.0812 0.297 6 25.603 3.4774 19614 0.243 614 0.314 1.712 7 26.142 3.4063 477 0.5512 455 1.03 0.33 8 27.7284 3.21465 114334 0.1045 1398 0.12211 2.13 9 27.79116 3.207518 14412 0.594 1006 0.6910 2.46 10 30.843 2.8972 346 0.699 254 0.73 32 11 35.532 2.524517 427 1.077 594 1.43 0.3618 Meas. data:170-xrd-2016Data 1 BG data:170-xrd-2016Data 1 Calc. data:170-xrd-2016Data 1 2-theta deg Intensity counts 20 40 60 80 500 1000 1500 2000 62 LAMPIRAN 2 Perhitungn Ukuran Kristal Zeolit Alam dan CuO-Zeolit Alam Persamaan Scherrer D = Dimana: D = Ukuran kristal Å = panjang gelombang sinar-X yang digunakan 1,5406 Å k = konstanta Scherrer 0,9 = puncak pada setengah tinggi intensitas FWHM = Full Width at a Half Maximum = FWHM O rad = sudut difraksi

1. Zeolit alam sebelum kalsinasi

2 θ = 9,984 θ = 4,992 cos θ = 0,9962 FWHM = 0,425 = 0,425 x π180 = 0,0074 rad Ukuran kristal = = 188,0801 Å = 18,80801 nm βθ = 22,558 θ = 11,279 cos θ = 0,980 FWHM = 0,78 = 0,78 x π180 = 0,01γ6 rad Ukuran kristal = = 104,0294 Å = 10,40294 nm βθ = 25,755 θ = 12,8775 cos θ = 0,974 FWHM = 0,55 = 0,55 x π180 = 0,00λ5 rad Ukuran kristal = = 149,8437 Å = 14,98437 nm 63 Ukuran rata-rata = 18,80801+10,40294+14,984373 = 14,7317 nm 2. Zeolit alam setelah kalsinasi βθ = 9,833 θ = 4,9165 cos θ = 0,9963 FWHM = 0,29 = 0,βλ x π180 = 0,0051 rad Ukuran kristal = = 272,8732 Å = 27,28732 nm βθ = 22,31 θ = 11,155 cos θ = 0,9811 FWHM = 0,49 = 0,4λ x π180 = 0,0085 rad Ukuran kristal = = 166,2604 Å = 16,62604 nm βθ = 25,699 θ = 12,8495 cos θ = 0,9749 FWHM = 0,232 = 0,232 x π180 = 0,0040 rad Ukuran kristal = = 355,5503 Å = 35,55503 nm Ukuran rata-rata = 27,28732+16,62604+35,555033 = 26,4894 nm 3. CuO-Zeolit alam 1:3 βθ = 21,65 θ = 10,825 cos θ = 0,9822 FWHM = 0,85 = 0,85 x π180 = 0,0148 rad Ukuran kristal = = 95,38048 Å = 9,538048 nm βθ = 25,60 θ = 12,80 cos θ = 0,9751 FWHM = 0,24 = 0,24 x π180 = 0,004187 rad Ukuran kristal = = 337,1462 Å = 33,71462 nm βθ = 27,728 θ = 13,864 64 cos θ = 0,9708 FWHM = 0,104 = 0,104 x π180 = 0,001814 rad Ukuran kristal = = 787,3281 Å = 78,73281 nm Ukuran rata-rata = 9,538048+33,71462+78,732813 = 40,661826 nm 4. CuO-Zeolit alam 1:1 2 θ = 21,63 θ = 10,815 cos θ = 0,9822 FWHM = 0,92 = 0,λβ x π180 = 0,0160 rad Ukuran kristal = = 88,22694 Å = 8,822694 nm βθ = 25,46 θ = 12,73 cos θ = 0,9754 FWHM = 0,32 = 0,γβ x π180 = 0,00558β rad Ukuran kristal = = 254,6529 Å = 25,46529 nm βθ = 27,52 θ = 13,76 cos θ = 0,9713 FWHM = 0,65 = 0,65 x π180 = 0,011γ rad Ukuran kristal = = 126,325 Å = 12,6325 nm Ukuran rata-rata = 8,822694+25,46529+12,63253 = 15,6401 nm 5. CuO-Zeolit alam 3:1 βθ = 21,53 θ = 10,765 cos θ = 0,9824 FWHM = 0,84 = 0,84 x π180 = 0,0146 rad Ukuran kristal = = 96,66737 Å = 9,666737 nm βθ = 25,473 θ = 12,7365 cos θ = 0,9753 FWHM = 0,26 = 0,β6 x π180 = 0,0045γ rad 65 Ukuran kristal = = 313, 823 Å = 31,3823 nm βθ = 27,60 θ = 13,8 cos θ = 0,9711 FWHM = 0,43 = 0,43 x π180 = 0,007501 rad Ukuran kristal = = 190,3435 Å = 19,03435 nm Ukuran rata-rata = 9,666737 +31,3823+19,034353 = 20,0277 nm