Pembuatan Nanosilikon Dari Pasir Alam Kecamatan Tanjung Tiram Kabupaten Asahan Secara Magnesiotermik Dengan Penambahan Natrium Klorida Sebagai Penyerap Kalor
LAMPIRAN
Universitas Sumatera Utara
Lampiran 1. Data JCPDS Silikat (Morris,1976)
Universitas Sumatera Utara
Lampiran 2. Data JCPDS Silikon (Morris,1976)
Universitas Sumatera Utara
Lampiran 3. Difraktogram Silika Hasil Isolasi dari Pasir Alam
General information
Analysis date
Sample name
File name
Comment
2015/02/09 13:32:53
SiO2
SwdSiO2.ras
Measurement date
Operator
2015/02/09 10:44:33
administrator
Measurement profile
Meas. data:SwdSiO2/Data 1
BG data:SwdSiO2/Data 1
Calc. data:SwdSiO2/Data 1
2000
Intensity (counts)
1500
1000
500
0
20
30
40
50
60
70
2-theta (deg)
Universitas Sumatera Utara
Lampiran 4. Puncak Difraktogram Silikat Hasil Isolasi dari Pasir Alam
Peak
No.
2-theta(deg)
d(ang.)
Height(coun
ts)
FWHM(deg)
Int.
W(deg)
Asym.
factor
1.3(2)
Int.
I(counts
deg)
27(7)
1
5.7(3)
15.5(7)
20(4)
1.4(6)
0.60(17)
2
20.774(5)
4.2725(10)
617(25)
0.135(4)
102.9(17)
0.167(9)
0.57(9)
3
21.238(7)
4
21.305(5)
4.1800(14)
219(15)
0.087(15)
22(3)
0.098(18)
0.6(2)
4.1670(9)
101(10)
0.052(9)
6(2)
0.06(3)
0.2(4)
5
21.91(2)
4.053(4)
62(8)
0.196(15)
12.9(11)
0.21(4)
1.4(6)
6
22.671(17)
3.919(3)
95(10)
0.122(12)
12.4(11)
0.13(2)
0.8(4)
7
23.740(15)
3.745(2)
196(14)
0.14(3)
46(2)
0.23(3)
2.2(12)
8
25.71(4)
3.463(5)
48(7)
0.17(3)
8.7(14)
0.18(5)
2(2)
9
26.712(4)
3.3346(5)
1419(38)
0.186(3)
298(4)
0.210(9)
4.2(5)
10
26.996(11)
3.3002(13)
89(9)
0.20(5)
20(3)
0.22(6)
4(4)
11
27.17(2)
3.279(2)
157(13)
0.132(16)
22.8(18)
0.15(2)
0.8(5)
12
27.66(4)
3.223(4)
94(10)
0.59(3)
61(3)
0.65(10)
0.45(12)
13
28.018(5)
3.1821(5)
863(29)
0.095(4)
90(3)
0.105(7)
0.73(12)
14
29.955(18)
2.9805(17)
49(7)
0.10(2)
6.2(9)
0.13(4)
2.3(19)
15
31.412(9)
2.8456(8)
35(6)
0.09(2)
3.2(7)
0.09(3)
0.7(7)
16
36.50(4)
2.460(2)
55(7)
0.24(3)
14.3(14)
0.26(6)
1.3(7)
17
39.49(4)
2.280(2)
52(7)
0.22(3)
14.3(11)
0.27(6)
1.2(9)
18
40.286(9)
2.2369(5)
92(10)
0.078(15)
13.2(8)
0.14(2)
0.7(4)
19
42.618(7)
2.1197(3)
323(18)
0.119(9)
57.3(14)
0.178(14)
1.2(3)
20
45.807(13)
1.9793(5)
140(12)
0.170(14)
30.7(11)
0.22(3)
0.9(3)
21
48.338(13)
1.8814(5)
85(9)
0.125(15)
12.0(10)
0.14(3)
1.5(6)
22
48.593(9)
1.8721(3)
111(11)
0.103(9)
12.8(10)
0.12(2)
1.0(4)
23
50.089(2)
1.81963(8)
928(30)
0.108(2)
125.8(14)
0.135(6)
0.50(6)
24
50.833(10)
1.7947(3)
33(6)
0.16(3)
9.0(8)
0.27(7)
2.5(19)
25
52.608(17)
1.7383(5)
35(6)
0.102(14)
4.1(6)
0.11(4)
1.2(9)
26
54.83(2)
1.6729(6)
58(8)
0.13(3)
12.9(10)
0.22(5)
0.5(5)
27
58.42(2)
1.5783(5)
31(6)
0.110(16)
3.6(7)
0.12(4)
0.9(8)
28
59.962(3)
1.54148(7)
420(21)
0.128(3)
63.0(10)
0.150(10)
1.49(15)
29
62.05(2)
1.4945(5)
30(5)
0.09(3)
3.6(7)
0.12(4)
2(2)
30
64.056(3)
471(22)
0.121(2)
69.6(10)
0.148(9)
1.22(12)
31
65.694(6)
59(8)
0.135(11)
11.2(7)
0.19(4)
2.9(6)
32
67.812(8)
194(14)
0.194(9)
45.9(13)
0.24(2)
3.0(7)
33
68.265(7)
237(15)
0.179(8)
52.5(15)
0.22(2)
2.5(5)
34
69.428(11)
69(8)
0.132(15)
12.8(11)
0.19(4)
0.8(2)
35
73.37(5)
1.45247(6)
1.42017(11
)
1.38088(14
)
1.37280(13
)
1.35262(19
)
1.2893(7)
18(4)
0.29(6)
7.5(11)
0.43(16)
1.2(6)
36
74.206(5)
1.27691(8)
232(15)
0.121(5)
33.2(10)
0.143(14)
0.68(12)
37
75.694(5)
1.25547(6)
279(17)
0.133(5)
53.2(9)
0.191(15)
1.23(19)
38
77.685(19)
1.2282(2)
38(6)
0.232(19)
9.5(7)
0.25(6)
1.4(5)
Universitas Sumatera Utara
Lampiran 5. Hasil Analisa Kuantitatif Silikat Hasil Isolasi dari
PasirAlamGeneral information
Analysis date
Sample name
File name
Comment
2015/02/09 13:33:37
SiO2
SwdSiO2.ras
Measurement date
Operator
2015/02/09 10:44:33
administrator
Qualitative analysis results
Phase name
Formula
Figure of merit
Phase reg. detail
DB card
number
Quartz
Si O2
1.082
User (COD)
5000035
Albite, calcian,
ordered
( Na , Ca ) Al ( Si , Al
)3 O8
1.379
ICDD (PDF2/Release 2012 RDB)
00-0411480
Weight ratio
Phase name
Quartz
Albite, calcian, ordered
Content(%)
72.5(11)
27.5(8)
SwdSiO2
0
20
40
60
80
100
Wt(%)
Quartz
Albite, calcian, ordered
Unknown
Measurement profile
Meas. data:SwdSiO2/Data 1
Intensity (counts)
2000
1500
1000
500
0
Quartz, Si O2, 5000035
Albite, calcian, ordered, ( Na , Ca ) Al ( Si , Al )3 O8, 00-041-1480
20
30
40
50
60
70
2-theta (deg)
Universitas Sumatera Utara
Lampiran 6. Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
6 jam ( Hasil Pencuucian HCl 2N)
General information
Analysis date
Sample name
2015/03/31 12:49:27
File name
Comment
Tahap1.txt
Measurement date
2015/03/2
3 11:18:50
Operator
Measurement profile
Meas. data:Tahap1/Data 1
BG data:Tahap1/Data 1
Calc. data:Tahap1/Data 1
Intensity (counts)
1500
1000
500
0
20
40
60
80
2-theta (deg)
Peak list
No.
2-theta(deg)
d(ang.)
Height(coun
ts)
FWHM(d
eg)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
21.73(4)
22.95(4)
23.923(18)
25.64(3)
26.693(5)
27.54(6)
28.481(4)
29.891(18)
32.326(12)
35.740(18)
36.492(19)
37.12(3)
39.779(18)
39.995(15)
43.244(7)
44.918(18)
47.347(5)
52.30(3)
56.114(8)
62.00(5)
62.78(3)
65.20(5)
69.13(2)
76.346(4)
76.65(2)
87.992(11)
4.086(7)
3.871(7)
3.717(3)
3.471(4)
3.3369(6)
3.236(6)
3.1314(5)
2.9868(18)
2.7672(10)
2.5103(12)
2.4603(12)
2.420(2)
2.2642(10)
2.2525(8)
2.0904(3)
2.0164(8)
1.91842(19)
1.7477(8)
1.6377(2)
1.4956(12)
1.4790(7)
1.4297(9)
1.3578(4)
1.24636(5)
1.2422(3)
1.10897(11)
59(8)
51(7)
28(5)
22(5)
491(22)
26(5)
1029(32)
58(8)
48(7)
83(9)
117(11)
52(7)
30(5)
31(6)
95(10)
40(6)
709(27)
44(7)
339(18)
19(4)
50(7)
32(6)
51(7)
160(13)
26(5)
117(11)
0.38(5)
0.23(5)
0.26(8)
0.55(13)
0.103(6)
0.17(5)
0.193(3)
0.17(2)
0.19(4)
0.29(3)
0.22(4)
0.54(11)
0.39(5)
0.14(6)
0.28(3)
0.55(5)
0.194(5)
0.35(4)
0.201(10)
0.31(5)
0.43(3)
0.62(7)
0.28(4)
0.137(9)
0.07(5)
0.276(12)
Int.
I(counts
deg)
40.6(19)
19.9(15)
15.4(17)
25(2)
66.9(14)
4.9(14)
248(2)
10.8(12)
13.2(13)
41(3)
46(8)
51(11)
23(2)
7.9(12)
40.6(16)
30(2)
178(2)
22.8(14)
93.1(17)
6.3(7)
23.1(10)
29.8(17)
20.5(13)
31(3)
3(3)
39.0(11)
Int.
W(deg)
Asym.
factor
0.68(12)
0.39(8)
0.56(17)
1.1(4)
0.136(9)
0.19(9)
0.241(10)
0.19(4)
0.28(7)
0.49(9)
0.39(11)
1.0(3)
0.8(2)
0.25(8)
0.43(6)
0.75(17)
0.250(12)
0.52(11)
0.27(2)
0.33(11)
0.46(8)
0.9(2)
0.40(8)
0.19(3)
0.13(13)
0.33(4)
1.2(6)
3(3)
4(5)
3(3)
1.3(3)
0.4(7)
1.60(14)
4(2)
1.2(14)
1.9(6)
0.8(4)
0.8(4)
5(6)
0.2(3)
5(3)
4(3)
2.0(2)
1.7(4)
1.2(2)
2(2)
2.1(7)
1.2(5)
1.3(5)
0.46(5)
3(5)
1.05(17)
Universitas Sumatera Utara
Lampiran 7.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 6 jam ( Hasil Pencuucian HCl 2N)
General information
Analysis date
Sample name
2015/03/31 12:49:57
File name
Comment
Tahap1.txt
Measurement date
2015/03/23
11:18:50
Operator
Qualitative analysis results
Phase name
Formula
Figure of merit
Phase reg. detail
DB card
number
Silicon
Si
0.418
User (COD)
9013102
Olivine
Mg2 O4 Si
1.191
Mg O
1.194
cristobalite-beta high
Si O2
0.982
User (COD)
ICDD (PDF-2/Release
2012
ICDD RDB)
(PDF-2/Release
9001096
Periclase, syn
Graphite
C
0.898
2012 RDB)
User (COD)
00-045-0946
01-071-6246
9000046
Weight ratio
Tahap1
Content(%)
26.0(2)
37(7)
19.7(8)
3.61(17)
14.0(3)
Phase name
Silicon
Olivine
Periclase, syn
cristobalite-beta high
Graphite
160
150
140
130
120
110
100
90
80
70
60
50
40
30
20
10
0
Tahap1
Silicon(%)
Olivine(%)
Periclas..., syn(%)
cristoba... high(%)
Graphite(%)
Measurement profil
Meas. data:Tahap1/Data 1
Intensity (counts)
1500
1000
500
0
Silicon, Si, 9013102
Olivine, Mg2 O4 Si, 9001096
Periclase, syn, Mg O, 00-045-0946
cristobalite-beta high, Si O2, 01-071-6246
Graphite, C, 9000046
20
40
60
80
2-theta (deg)
Universitas Sumatera Utara
Lampiran 8.
Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
6 jam ( Hasil Pencucian HCl 2N dan CH3COOH 25%)
General information
Analysis date
Sample name
2015/03/31 12:37:29
File name
Comment
Tahap2.txt
Measurement date
2015/03/2
3 11:49:55
Operator
Measurement profile
Meas. data:Tahap2/Data 1
BG data:Tahap2/Data 1
Calc. data:Tahap2/Data 1
Intensity (counts)
1500
1000
500
0
20
40
60
80
2-theta (deg)
Peak list
No.
2theta(deg)
d(ang.)
Height(count
s)
FWHM(de
g)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
21.8103
23.0001
23.7515
26.6946
27.5713
28.5106
29.8256
31.3032
32.3929
35.7434
36.651
37.1648
40.1577
43.2887
44.7915
47.2963
52.3059
56.1117
62.7633
65.3307
69.213
76.4142
88.0597
4.07168
3.86368
3.74312
3.33674
3.2326
3.1282
2.9932
2.8552
2.76159
2.51003
2.44993
2.41724
2.24371
2.08841
2.02176
1.92037
1.74762
1.63777
1.47925
1.42719
1.35631
1.24541
1.10829
54(7)
29(5)
47(7)
23(5)
21(5)
997(32)
37(6)
26(5)
33(6)
62(8)
38(6)
57(8)
42(6)
95(10)
60(8)
723(27)
27(5)
382(20)
47(7)
40(6)
60(8)
206(14)
220(15)
0.36(4)
0.12(5)
0.20(3)
0.14(4)
0.36(8)
0.226(4)
0.35(8)
0.31(11)
0.17(9)
0.32(3)
0.40(6)
0.4(2)
0.09(4)
0.32(2)
0.29(6)
0.211(5)
0.33(5)
0.208(10)
0.33(6)
0.40(4)
0.34(3)
0.157(9)
0.189(10)
Int.
I(counts
deg)
30.846905
6.677735
10.316934
3.414456
7.948247
274.47077
6
18.570685
17.146738
11.921302
27.152713
21.357939
40.544637
6.818392
34.842052
36.570100
184.69146
2
12.265210
104.28947
7
19.340380
20.822153
23.894665
48.184193
60.169707
Int.
W(deg)
Asym.
factor
0.57(8)
3.6(6)
0.23(4)
2(4)
0.22(3)
0.86(17)
0.15(3)
5(10)
0.38(8)
0.7(9)
0.275(9)
3.61(16)
0.50(8)
0.8(7)
0.65(13)
2.1(8)
0.37(6)
1.2(13)
0.43(5)
3(2)
0.57(9)
2(3)
0.72(10)
2.4(6)
0.16(3)
5(17)
0.37(4)
4.4(16)
0.61(8)
1.3(3)
0.256(10) 0.89(3)
0.45(9)
2.6(6)
0.273(14) 1.3(2)
0.41(6)
1.6(3)
0.52(8)
3.2(18)
0.40(5)
3(2)
0.234(16) 3.9(5)
0.274(18) 3.1(6)
Universitas Sumatera Utara
Lampiran 9.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 6 jam ( Hasil Pencucian HCl 2N dan CH3COOH
25%)
General information
Analysis date
Sample name
2015/03/31 12:38:04
File name
Comment
Tahap2.txt
Measurement date
2015/03/2
3 11:49:55
Operator
Qualitative analysis results
Phase name
Formula
Figure of merit
Silicon
gamma-Mg2 ( Si O4 )
Periclase, syn
Stishovite
Si
Mg2 ( Si O4 )
Mg O
Si O2
0.284
1.108
0.754
1.310
Phase reg.
detail
User (COD)
ICDD (PDF2/Release
ICDD (PDF2/Release
ICDD
(PDF2/Release
DB card number
2104748
01-077-8453
01-071-9574
01-077-8643
Weight ratio
Tahap2
Content(%)
59.625079
19.485073
11.583128
9.306720
Phase name
Silicon
gamma-Mg2 ( Si O4 )
Periclase, syn
Stishovite
Unknown
100
90
80
70
60
50
40
30
20
10
0
Tahap2
Silicon(%)
gamma-Mg... O4 )(%)
Periclas..., syn(%)
Stishovite(%)
Unknown(%)
Measurement profile
Meas. data:Tahap2/Data 1
Intensity (counts)
1500
1000
500
0
Silicon, Si, 2104748
gamma-Mg2 ( Si O4 ), Mg2 ( Si O4 ), 01-077-8453
Periclase, syn, Mg O, 01-071-9574
Stishovite, Si O2, 01-077-8643
20
40
60
80
2-theta (deg)
Universitas Sumatera Utara
Lampiran 10. Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
6 jam ( Hasil Pencucian CH3COOH 25% dan HF 4,8%)
General information
Analysis date
Sample name
2015/03/31 12:57:30
File name
Comment
Tahap3.txt
Measurement date
2015/03/2
3 11:35:03
Operator
Measurement profile
1200
Meas. data:Tahap3/Data 1
BG data:Tahap3/Data 1
Calc. data:Tahap3/Data 1
1000
Intensity (counts)
800
600
400
200
0
20
40
60
80
2-theta (deg)
Peak list
No.
2-theta(deg)
d(ang.)
Height(count
s)
FWHM(de
g)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
15.233(15)
28.441(6)
29.37(3)
30.70(2)
37.16(4)
38.92(6)
43.21(3)
44.02(7)
44.67(6)
47.315(4)
51.23(3)
56.119(6)
60.99(2)
62.77(7)
65.22(4)
66.20(6)
69.124(12)
71.93(8)
75.30(11)
76.366(9)
79.36(6)
81.02(4)
83.73(3)
87.994(8)
5.812(6)
3.1356(6)
3.038(3)
2.910(2)
2.418(3)
2.312(3)
2.0922(14)
2.056(3)
2.027(2)
1.91965(15)
1.7818(9)
1.63759(16)
1.5178(5)
1.4791(15)
1.4294(8)
1.4105(11)
1.3578(2)
1.3117(13)
1.2611(16)
1.24608(12)
1.2064(7)
1.1858(5)
1.1542(3)
1.10895(8)
95(10)
740(27)
74(9)
150(12)
54(7)
48(7)
106(10)
31(6)
40(6)
879(30)
103(10)
455(21)
30(6)
34(6)
49(7)
23(5)
144(12)
7(3)
20(4)
211(15)
9(3)
11(3)
16(4)
245(16)
0.16(2)
0.201(5)
0.28(3)
0.28(2)
0.67(4)
0.31(6)
0.27(3)
0.36(9)
0.51(7)
0.172(7)
0.45(2)
0.205(7)
0.50(9)
0.39(5)
0.41(6)
0.35(11)
0.165(14)
0.7(3)
0.40(14)
0.193(9)
0.4(2)
0.35(11)
0.21(8)
0.215(8)
Int.
I(counts
deg)
28.3(16)
195(2)
31(2)
65(2)
48(3)
25(2)
39(2)
14(4)
25(7)
232(3)
60(3)
119(2)
22(5)
14(4)
33(5)
13(2)
38.2(17)
7(3)
10(3)
52(2)
4.2(15)
4.6(10)
5.6(12)
67.6(16)
Int.
W(deg)
Asym.
factor
0.30(5)
0.264(1
3)
0.41(7)
1.0(4)
2.3(3)
1.0(6)
0.9(4)
3.3(13)
1.1(10)
1.6(8)
2(3)
0.6(4)
1.68(18)
0.9(2)
1.9(3)
1.8(18)
1.5(12)
1.8(10)
1.3(11)
1.4(5)
1(2)
1.4(19)
1.7(4)
3(5)
5(12)
1.3(18)
0.84(15)
0.44(5)
0.90(19)
0.51(12)
0.37(6)
0.5(2)
0.6(3)
0.264(1
2)
0.58(9)
0.262(1
7)
0.7(3)
0.41(18)
0.66(19)
0.6(2)
0.27(3)
1.0(8)
0.5(3)
0.25(3)
0.5(3)
0.4(2)
0.35(16)
0.28(2)
Universitas Sumatera Utara
Lampiran 11.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 6 jam ( Hasil Pencucian CH3COOH 25% dan HF
4,8%)
General information
Analysis date
Sample name
2015/03/31 12:57:57
File name
Comment
Tahap3.txt
Measurement date
2015/03/23
11:35:03
Operator
Qualitative analysis results
Phase name
Silicon
Stishovite, syn
Silicon Oxide
Ringwoodite
Periclase
Formula
Si
Si O2
Si O2
Mg2 O4 Si
Mg O
Figure of merit
0.538
1.379
1.606
1.521
1.098
Phase reg. detail
User (COD)
ICDD (PDF2/Release
2012
ICDD
(PDF2/Release
User (COD)2012
DB card number
2104748
01-076-2979
01-075-3170
9000269
9006801
User (COD)
Weight ratio
Tahap3
Content(%)
49.4(5)
20.8(6)
5.9(4)
16(2)
7.9(5)
Phase name
Silicon
Stishovite, syn
Silicon Oxide
Ringwoodite
Periclase
110
100
90
80
70
60
50
40
30
20
10
0
Tahap3
Silicon(%)
Stishovi..., syn(%)
Silicon Oxide(%)
Ringwoodite(%)
Periclase(%)
Measurement profile
Meas. data:Tahap3/Data 1
Intensity (counts)
1000
500
0
Silicon, Si, 2104748
Stishovite, syn, Si O2, 01-076-2979
Silicon Oxide, Si O2, 01-075-3170
Ringwoodite, Mg2 O4 Si, 9000269
Periclase, Mg O, 9006801
20
40
60
80
2-theta (deg)
Universitas Sumatera Utara
Lampiran 12. Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
7 jam
General information
Analysis date
Sample name
File name
2015/03/31 13:00:01
NANO_RUNNINGII
NANO_SILIKA
RUNNINGII.ras
Measurement date
Operator
2015/03/19 10:06:56
administrator
Measurement profile
Meas. data:NANO_SILIKA RUNNINGII/Data
1
BG data:NANO_SILIKA RUNNINGII/Data 1
Calc. data:NANO_SILIKA RUNNINGII/Data
1
Intensity (counts)
3000
2000
1000
0
20
40
60
80
2-theta (deg)
Peak list
No.
2theta(deg)
d(ang.)
Height(count
s)
FWHM(deg
)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
15.336(7)
18.945(17)
20.898(7)
26.681(10)
28.331(4)
28.495(4)
29.550(13)
30.883(13)
37.259(7)
39.15(2)
43.236(14)
44.215(11)
44.712(19)
47.318(6)
51.504(11)
56.142(4)
58.11(3)
59.41(3)
60.50(3)
61.28(2)
62.686(18)
65.20(3)
66.495(19)
69.139(7)
72.42(5)
75.33(4)
76.450(7)
79.41(3)
81.30(13)
83.97(7)
88.038(6)
5.773(3)
4.681(4)
4.2474(14)
3.3384(12)
3.1476(5)
3.1298(4)
3.0205(13)
2.8931(12)
2.4113(4)
2.2989(12)
2.0908(6)
2.0468(5)
2.0252(8)
1.9195(2)
1.7729(3)
1.63696(12)
1.5862(8)
1.5545(8)
1.5291(7)
1.5115(5)
1.4809(4)
1.4296(6)
1.4050(4)
1.35758(12)
1.3040(8)
1.2607(6)
1.24492(10)
1.2058(4)
1.1824(15)
1.1516(8)
1.10851(6)
477(22)
33(6)
344(19)
102(10)
687(26)
1983(45)
311(18)
419(20)
167(13)
149(12)
372(19)
148(12)
176(13)
1045(32)
315(18)
673(26)
41(6)
46(7)
53(7)
114(11)
129(11)
84(9)
58(8)
254(16)
31(6)
42(6)
378(19)
36(6)
24(5)
29(5)
358(19)
0.215(7)
0.19(5)
0.108(5)
0.31(4)
0.119(13)
0.154(8)
0.203(11)
0.209(18)
0.58(3)
0.21(2)
0.244(13)
0.14(3)
0.26(4)
0.192(9)
0.234(17)
0.163(6)
0.14(4)
0.31(5)
0.23(5)
0.25(3)
0.371(18)
0.43(4)
0.24(4)
0.161(7)
0.35(6)
0.44(6)
0.210(8)
0.24(6)
0.49(9)
0.32(8)
0.199(5)
Int.
I(counts
deg)
143(3)
7(2)
41.4(17)
46(3)
111(20)
424(21)
95.1(19)
146(3)
129(4)
46.3(19)
128(3)
38(6)
84(7)
329(5)
117(2)
150(2)
7.5(15)
20(2)
16.2(15)
38(2)
56(2)
49(2)
20(2)
55.7(16)
12(2)
27(3)
114(2)
15.8(18)
12(2)
10(2)
88(2)
Int.
W(deg)
Asym.
factor
0.30(2)
0.20(11)
0.120(11)
0.45(8)
0.16(4)
0.214(15)
0.31(2)
0.35(2)
0.78(8)
0.31(4)
0.34(2)
0.26(6)
0.48(8)
0.315(15)
0.37(3)
0.222(12)
0.18(6)
0.43(12)
0.31(7)
0.33(5)
0.43(5)
0.58(9)
0.35(8)
0.22(2)
0.38(13)
0.64(17)
0.30(2)
0.44(12)
0.5(2)
0.35(13)
0.245(19)
1.7(3)
0.2(4)
0.64(17)
5(5)
0.51(19)
1.8(2)
1.3(4)
0.9(3)
3.5(10)
1.5(7)
1.0(3)
0.7(2)
0.6(2)
1.00(13)
0.82(18)
1.04(13)
0.4(5)
2.3(9)
1.8(10)
1.2(5)
0.34(10)
0.7(3)
0.34(11)
1.0(2)
3(2)
1.7(6)
1.5(3)
2(2)
0.9(9)
1.0(8)
1.23(18)
Universitas Sumatera Utara
Lampiran 13.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 7 jam
General information
Analysis date
Sample name
2015/03/31 13:05:10
NANO_RUNNINGII
File name
NANO_SILIKA
RUNNINGII.ras
Measurement
date
Operator
2015/03/19 10:06:56
administrator
Comment
Qualitative analysis results
Phase name
Silicon
Periclase
perovskite (Mg, Si)
HP,
syn,
magnesium
silicon
dioxide
Quartz
Formula
Si
Mg O
Mg Si O3
Si O2
O2 Si
Figure of merit
0.745
0.984
1.474
1.467
1.635
Phase reg. detail
User (COD)
User (COD)
ICDD (PDF-2/Release
2012
ICDD RDB)
(PDF-2/Release
2012
RDB)
User (COD)
DB card number
9013102
9013225
01-080-0568
01-070-5689
9010146
Weight ratio
Phase name
Silicon
Periclase
perovskite (Mg, Si) HP,
syn,
magnesium
silicon
dioxide catenaQuartz
Content(%)
29(6)
7(4)
13(5)
43(4)
8.0(18)
NANO_SILIKA RUNNINGII
0
50
100
Wt(%)
Silicon
Periclase
rovskite (Mg, Si) HP, syn, magnesium catena-silicate
silicon dioxide
Quartz
Measurement profile
Universitas Sumatera Utara
Universitas Sumatera Utara
Lampiran 1. Data JCPDS Silikat (Morris,1976)
Universitas Sumatera Utara
Lampiran 2. Data JCPDS Silikon (Morris,1976)
Universitas Sumatera Utara
Lampiran 3. Difraktogram Silika Hasil Isolasi dari Pasir Alam
General information
Analysis date
Sample name
File name
Comment
2015/02/09 13:32:53
SiO2
SwdSiO2.ras
Measurement date
Operator
2015/02/09 10:44:33
administrator
Measurement profile
Meas. data:SwdSiO2/Data 1
BG data:SwdSiO2/Data 1
Calc. data:SwdSiO2/Data 1
2000
Intensity (counts)
1500
1000
500
0
20
30
40
50
60
70
2-theta (deg)
Universitas Sumatera Utara
Lampiran 4. Puncak Difraktogram Silikat Hasil Isolasi dari Pasir Alam
Peak
No.
2-theta(deg)
d(ang.)
Height(coun
ts)
FWHM(deg)
Int.
W(deg)
Asym.
factor
1.3(2)
Int.
I(counts
deg)
27(7)
1
5.7(3)
15.5(7)
20(4)
1.4(6)
0.60(17)
2
20.774(5)
4.2725(10)
617(25)
0.135(4)
102.9(17)
0.167(9)
0.57(9)
3
21.238(7)
4
21.305(5)
4.1800(14)
219(15)
0.087(15)
22(3)
0.098(18)
0.6(2)
4.1670(9)
101(10)
0.052(9)
6(2)
0.06(3)
0.2(4)
5
21.91(2)
4.053(4)
62(8)
0.196(15)
12.9(11)
0.21(4)
1.4(6)
6
22.671(17)
3.919(3)
95(10)
0.122(12)
12.4(11)
0.13(2)
0.8(4)
7
23.740(15)
3.745(2)
196(14)
0.14(3)
46(2)
0.23(3)
2.2(12)
8
25.71(4)
3.463(5)
48(7)
0.17(3)
8.7(14)
0.18(5)
2(2)
9
26.712(4)
3.3346(5)
1419(38)
0.186(3)
298(4)
0.210(9)
4.2(5)
10
26.996(11)
3.3002(13)
89(9)
0.20(5)
20(3)
0.22(6)
4(4)
11
27.17(2)
3.279(2)
157(13)
0.132(16)
22.8(18)
0.15(2)
0.8(5)
12
27.66(4)
3.223(4)
94(10)
0.59(3)
61(3)
0.65(10)
0.45(12)
13
28.018(5)
3.1821(5)
863(29)
0.095(4)
90(3)
0.105(7)
0.73(12)
14
29.955(18)
2.9805(17)
49(7)
0.10(2)
6.2(9)
0.13(4)
2.3(19)
15
31.412(9)
2.8456(8)
35(6)
0.09(2)
3.2(7)
0.09(3)
0.7(7)
16
36.50(4)
2.460(2)
55(7)
0.24(3)
14.3(14)
0.26(6)
1.3(7)
17
39.49(4)
2.280(2)
52(7)
0.22(3)
14.3(11)
0.27(6)
1.2(9)
18
40.286(9)
2.2369(5)
92(10)
0.078(15)
13.2(8)
0.14(2)
0.7(4)
19
42.618(7)
2.1197(3)
323(18)
0.119(9)
57.3(14)
0.178(14)
1.2(3)
20
45.807(13)
1.9793(5)
140(12)
0.170(14)
30.7(11)
0.22(3)
0.9(3)
21
48.338(13)
1.8814(5)
85(9)
0.125(15)
12.0(10)
0.14(3)
1.5(6)
22
48.593(9)
1.8721(3)
111(11)
0.103(9)
12.8(10)
0.12(2)
1.0(4)
23
50.089(2)
1.81963(8)
928(30)
0.108(2)
125.8(14)
0.135(6)
0.50(6)
24
50.833(10)
1.7947(3)
33(6)
0.16(3)
9.0(8)
0.27(7)
2.5(19)
25
52.608(17)
1.7383(5)
35(6)
0.102(14)
4.1(6)
0.11(4)
1.2(9)
26
54.83(2)
1.6729(6)
58(8)
0.13(3)
12.9(10)
0.22(5)
0.5(5)
27
58.42(2)
1.5783(5)
31(6)
0.110(16)
3.6(7)
0.12(4)
0.9(8)
28
59.962(3)
1.54148(7)
420(21)
0.128(3)
63.0(10)
0.150(10)
1.49(15)
29
62.05(2)
1.4945(5)
30(5)
0.09(3)
3.6(7)
0.12(4)
2(2)
30
64.056(3)
471(22)
0.121(2)
69.6(10)
0.148(9)
1.22(12)
31
65.694(6)
59(8)
0.135(11)
11.2(7)
0.19(4)
2.9(6)
32
67.812(8)
194(14)
0.194(9)
45.9(13)
0.24(2)
3.0(7)
33
68.265(7)
237(15)
0.179(8)
52.5(15)
0.22(2)
2.5(5)
34
69.428(11)
69(8)
0.132(15)
12.8(11)
0.19(4)
0.8(2)
35
73.37(5)
1.45247(6)
1.42017(11
)
1.38088(14
)
1.37280(13
)
1.35262(19
)
1.2893(7)
18(4)
0.29(6)
7.5(11)
0.43(16)
1.2(6)
36
74.206(5)
1.27691(8)
232(15)
0.121(5)
33.2(10)
0.143(14)
0.68(12)
37
75.694(5)
1.25547(6)
279(17)
0.133(5)
53.2(9)
0.191(15)
1.23(19)
38
77.685(19)
1.2282(2)
38(6)
0.232(19)
9.5(7)
0.25(6)
1.4(5)
Universitas Sumatera Utara
Lampiran 5. Hasil Analisa Kuantitatif Silikat Hasil Isolasi dari
PasirAlamGeneral information
Analysis date
Sample name
File name
Comment
2015/02/09 13:33:37
SiO2
SwdSiO2.ras
Measurement date
Operator
2015/02/09 10:44:33
administrator
Qualitative analysis results
Phase name
Formula
Figure of merit
Phase reg. detail
DB card
number
Quartz
Si O2
1.082
User (COD)
5000035
Albite, calcian,
ordered
( Na , Ca ) Al ( Si , Al
)3 O8
1.379
ICDD (PDF2/Release 2012 RDB)
00-0411480
Weight ratio
Phase name
Quartz
Albite, calcian, ordered
Content(%)
72.5(11)
27.5(8)
SwdSiO2
0
20
40
60
80
100
Wt(%)
Quartz
Albite, calcian, ordered
Unknown
Measurement profile
Meas. data:SwdSiO2/Data 1
Intensity (counts)
2000
1500
1000
500
0
Quartz, Si O2, 5000035
Albite, calcian, ordered, ( Na , Ca ) Al ( Si , Al )3 O8, 00-041-1480
20
30
40
50
60
70
2-theta (deg)
Universitas Sumatera Utara
Lampiran 6. Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
6 jam ( Hasil Pencuucian HCl 2N)
General information
Analysis date
Sample name
2015/03/31 12:49:27
File name
Comment
Tahap1.txt
Measurement date
2015/03/2
3 11:18:50
Operator
Measurement profile
Meas. data:Tahap1/Data 1
BG data:Tahap1/Data 1
Calc. data:Tahap1/Data 1
Intensity (counts)
1500
1000
500
0
20
40
60
80
2-theta (deg)
Peak list
No.
2-theta(deg)
d(ang.)
Height(coun
ts)
FWHM(d
eg)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
21.73(4)
22.95(4)
23.923(18)
25.64(3)
26.693(5)
27.54(6)
28.481(4)
29.891(18)
32.326(12)
35.740(18)
36.492(19)
37.12(3)
39.779(18)
39.995(15)
43.244(7)
44.918(18)
47.347(5)
52.30(3)
56.114(8)
62.00(5)
62.78(3)
65.20(5)
69.13(2)
76.346(4)
76.65(2)
87.992(11)
4.086(7)
3.871(7)
3.717(3)
3.471(4)
3.3369(6)
3.236(6)
3.1314(5)
2.9868(18)
2.7672(10)
2.5103(12)
2.4603(12)
2.420(2)
2.2642(10)
2.2525(8)
2.0904(3)
2.0164(8)
1.91842(19)
1.7477(8)
1.6377(2)
1.4956(12)
1.4790(7)
1.4297(9)
1.3578(4)
1.24636(5)
1.2422(3)
1.10897(11)
59(8)
51(7)
28(5)
22(5)
491(22)
26(5)
1029(32)
58(8)
48(7)
83(9)
117(11)
52(7)
30(5)
31(6)
95(10)
40(6)
709(27)
44(7)
339(18)
19(4)
50(7)
32(6)
51(7)
160(13)
26(5)
117(11)
0.38(5)
0.23(5)
0.26(8)
0.55(13)
0.103(6)
0.17(5)
0.193(3)
0.17(2)
0.19(4)
0.29(3)
0.22(4)
0.54(11)
0.39(5)
0.14(6)
0.28(3)
0.55(5)
0.194(5)
0.35(4)
0.201(10)
0.31(5)
0.43(3)
0.62(7)
0.28(4)
0.137(9)
0.07(5)
0.276(12)
Int.
I(counts
deg)
40.6(19)
19.9(15)
15.4(17)
25(2)
66.9(14)
4.9(14)
248(2)
10.8(12)
13.2(13)
41(3)
46(8)
51(11)
23(2)
7.9(12)
40.6(16)
30(2)
178(2)
22.8(14)
93.1(17)
6.3(7)
23.1(10)
29.8(17)
20.5(13)
31(3)
3(3)
39.0(11)
Int.
W(deg)
Asym.
factor
0.68(12)
0.39(8)
0.56(17)
1.1(4)
0.136(9)
0.19(9)
0.241(10)
0.19(4)
0.28(7)
0.49(9)
0.39(11)
1.0(3)
0.8(2)
0.25(8)
0.43(6)
0.75(17)
0.250(12)
0.52(11)
0.27(2)
0.33(11)
0.46(8)
0.9(2)
0.40(8)
0.19(3)
0.13(13)
0.33(4)
1.2(6)
3(3)
4(5)
3(3)
1.3(3)
0.4(7)
1.60(14)
4(2)
1.2(14)
1.9(6)
0.8(4)
0.8(4)
5(6)
0.2(3)
5(3)
4(3)
2.0(2)
1.7(4)
1.2(2)
2(2)
2.1(7)
1.2(5)
1.3(5)
0.46(5)
3(5)
1.05(17)
Universitas Sumatera Utara
Lampiran 7.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 6 jam ( Hasil Pencuucian HCl 2N)
General information
Analysis date
Sample name
2015/03/31 12:49:57
File name
Comment
Tahap1.txt
Measurement date
2015/03/23
11:18:50
Operator
Qualitative analysis results
Phase name
Formula
Figure of merit
Phase reg. detail
DB card
number
Silicon
Si
0.418
User (COD)
9013102
Olivine
Mg2 O4 Si
1.191
Mg O
1.194
cristobalite-beta high
Si O2
0.982
User (COD)
ICDD (PDF-2/Release
2012
ICDD RDB)
(PDF-2/Release
9001096
Periclase, syn
Graphite
C
0.898
2012 RDB)
User (COD)
00-045-0946
01-071-6246
9000046
Weight ratio
Tahap1
Content(%)
26.0(2)
37(7)
19.7(8)
3.61(17)
14.0(3)
Phase name
Silicon
Olivine
Periclase, syn
cristobalite-beta high
Graphite
160
150
140
130
120
110
100
90
80
70
60
50
40
30
20
10
0
Tahap1
Silicon(%)
Olivine(%)
Periclas..., syn(%)
cristoba... high(%)
Graphite(%)
Measurement profil
Meas. data:Tahap1/Data 1
Intensity (counts)
1500
1000
500
0
Silicon, Si, 9013102
Olivine, Mg2 O4 Si, 9001096
Periclase, syn, Mg O, 00-045-0946
cristobalite-beta high, Si O2, 01-071-6246
Graphite, C, 9000046
20
40
60
80
2-theta (deg)
Universitas Sumatera Utara
Lampiran 8.
Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
6 jam ( Hasil Pencucian HCl 2N dan CH3COOH 25%)
General information
Analysis date
Sample name
2015/03/31 12:37:29
File name
Comment
Tahap2.txt
Measurement date
2015/03/2
3 11:49:55
Operator
Measurement profile
Meas. data:Tahap2/Data 1
BG data:Tahap2/Data 1
Calc. data:Tahap2/Data 1
Intensity (counts)
1500
1000
500
0
20
40
60
80
2-theta (deg)
Peak list
No.
2theta(deg)
d(ang.)
Height(count
s)
FWHM(de
g)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
21.8103
23.0001
23.7515
26.6946
27.5713
28.5106
29.8256
31.3032
32.3929
35.7434
36.651
37.1648
40.1577
43.2887
44.7915
47.2963
52.3059
56.1117
62.7633
65.3307
69.213
76.4142
88.0597
4.07168
3.86368
3.74312
3.33674
3.2326
3.1282
2.9932
2.8552
2.76159
2.51003
2.44993
2.41724
2.24371
2.08841
2.02176
1.92037
1.74762
1.63777
1.47925
1.42719
1.35631
1.24541
1.10829
54(7)
29(5)
47(7)
23(5)
21(5)
997(32)
37(6)
26(5)
33(6)
62(8)
38(6)
57(8)
42(6)
95(10)
60(8)
723(27)
27(5)
382(20)
47(7)
40(6)
60(8)
206(14)
220(15)
0.36(4)
0.12(5)
0.20(3)
0.14(4)
0.36(8)
0.226(4)
0.35(8)
0.31(11)
0.17(9)
0.32(3)
0.40(6)
0.4(2)
0.09(4)
0.32(2)
0.29(6)
0.211(5)
0.33(5)
0.208(10)
0.33(6)
0.40(4)
0.34(3)
0.157(9)
0.189(10)
Int.
I(counts
deg)
30.846905
6.677735
10.316934
3.414456
7.948247
274.47077
6
18.570685
17.146738
11.921302
27.152713
21.357939
40.544637
6.818392
34.842052
36.570100
184.69146
2
12.265210
104.28947
7
19.340380
20.822153
23.894665
48.184193
60.169707
Int.
W(deg)
Asym.
factor
0.57(8)
3.6(6)
0.23(4)
2(4)
0.22(3)
0.86(17)
0.15(3)
5(10)
0.38(8)
0.7(9)
0.275(9)
3.61(16)
0.50(8)
0.8(7)
0.65(13)
2.1(8)
0.37(6)
1.2(13)
0.43(5)
3(2)
0.57(9)
2(3)
0.72(10)
2.4(6)
0.16(3)
5(17)
0.37(4)
4.4(16)
0.61(8)
1.3(3)
0.256(10) 0.89(3)
0.45(9)
2.6(6)
0.273(14) 1.3(2)
0.41(6)
1.6(3)
0.52(8)
3.2(18)
0.40(5)
3(2)
0.234(16) 3.9(5)
0.274(18) 3.1(6)
Universitas Sumatera Utara
Lampiran 9.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 6 jam ( Hasil Pencucian HCl 2N dan CH3COOH
25%)
General information
Analysis date
Sample name
2015/03/31 12:38:04
File name
Comment
Tahap2.txt
Measurement date
2015/03/2
3 11:49:55
Operator
Qualitative analysis results
Phase name
Formula
Figure of merit
Silicon
gamma-Mg2 ( Si O4 )
Periclase, syn
Stishovite
Si
Mg2 ( Si O4 )
Mg O
Si O2
0.284
1.108
0.754
1.310
Phase reg.
detail
User (COD)
ICDD (PDF2/Release
ICDD (PDF2/Release
ICDD
(PDF2/Release
DB card number
2104748
01-077-8453
01-071-9574
01-077-8643
Weight ratio
Tahap2
Content(%)
59.625079
19.485073
11.583128
9.306720
Phase name
Silicon
gamma-Mg2 ( Si O4 )
Periclase, syn
Stishovite
Unknown
100
90
80
70
60
50
40
30
20
10
0
Tahap2
Silicon(%)
gamma-Mg... O4 )(%)
Periclas..., syn(%)
Stishovite(%)
Unknown(%)
Measurement profile
Meas. data:Tahap2/Data 1
Intensity (counts)
1500
1000
500
0
Silicon, Si, 2104748
gamma-Mg2 ( Si O4 ), Mg2 ( Si O4 ), 01-077-8453
Periclase, syn, Mg O, 01-071-9574
Stishovite, Si O2, 01-077-8643
20
40
60
80
2-theta (deg)
Universitas Sumatera Utara
Lampiran 10. Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
6 jam ( Hasil Pencucian CH3COOH 25% dan HF 4,8%)
General information
Analysis date
Sample name
2015/03/31 12:57:30
File name
Comment
Tahap3.txt
Measurement date
2015/03/2
3 11:35:03
Operator
Measurement profile
1200
Meas. data:Tahap3/Data 1
BG data:Tahap3/Data 1
Calc. data:Tahap3/Data 1
1000
Intensity (counts)
800
600
400
200
0
20
40
60
80
2-theta (deg)
Peak list
No.
2-theta(deg)
d(ang.)
Height(count
s)
FWHM(de
g)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
15.233(15)
28.441(6)
29.37(3)
30.70(2)
37.16(4)
38.92(6)
43.21(3)
44.02(7)
44.67(6)
47.315(4)
51.23(3)
56.119(6)
60.99(2)
62.77(7)
65.22(4)
66.20(6)
69.124(12)
71.93(8)
75.30(11)
76.366(9)
79.36(6)
81.02(4)
83.73(3)
87.994(8)
5.812(6)
3.1356(6)
3.038(3)
2.910(2)
2.418(3)
2.312(3)
2.0922(14)
2.056(3)
2.027(2)
1.91965(15)
1.7818(9)
1.63759(16)
1.5178(5)
1.4791(15)
1.4294(8)
1.4105(11)
1.3578(2)
1.3117(13)
1.2611(16)
1.24608(12)
1.2064(7)
1.1858(5)
1.1542(3)
1.10895(8)
95(10)
740(27)
74(9)
150(12)
54(7)
48(7)
106(10)
31(6)
40(6)
879(30)
103(10)
455(21)
30(6)
34(6)
49(7)
23(5)
144(12)
7(3)
20(4)
211(15)
9(3)
11(3)
16(4)
245(16)
0.16(2)
0.201(5)
0.28(3)
0.28(2)
0.67(4)
0.31(6)
0.27(3)
0.36(9)
0.51(7)
0.172(7)
0.45(2)
0.205(7)
0.50(9)
0.39(5)
0.41(6)
0.35(11)
0.165(14)
0.7(3)
0.40(14)
0.193(9)
0.4(2)
0.35(11)
0.21(8)
0.215(8)
Int.
I(counts
deg)
28.3(16)
195(2)
31(2)
65(2)
48(3)
25(2)
39(2)
14(4)
25(7)
232(3)
60(3)
119(2)
22(5)
14(4)
33(5)
13(2)
38.2(17)
7(3)
10(3)
52(2)
4.2(15)
4.6(10)
5.6(12)
67.6(16)
Int.
W(deg)
Asym.
factor
0.30(5)
0.264(1
3)
0.41(7)
1.0(4)
2.3(3)
1.0(6)
0.9(4)
3.3(13)
1.1(10)
1.6(8)
2(3)
0.6(4)
1.68(18)
0.9(2)
1.9(3)
1.8(18)
1.5(12)
1.8(10)
1.3(11)
1.4(5)
1(2)
1.4(19)
1.7(4)
3(5)
5(12)
1.3(18)
0.84(15)
0.44(5)
0.90(19)
0.51(12)
0.37(6)
0.5(2)
0.6(3)
0.264(1
2)
0.58(9)
0.262(1
7)
0.7(3)
0.41(18)
0.66(19)
0.6(2)
0.27(3)
1.0(8)
0.5(3)
0.25(3)
0.5(3)
0.4(2)
0.35(16)
0.28(2)
Universitas Sumatera Utara
Lampiran 11.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 6 jam ( Hasil Pencucian CH3COOH 25% dan HF
4,8%)
General information
Analysis date
Sample name
2015/03/31 12:57:57
File name
Comment
Tahap3.txt
Measurement date
2015/03/23
11:35:03
Operator
Qualitative analysis results
Phase name
Silicon
Stishovite, syn
Silicon Oxide
Ringwoodite
Periclase
Formula
Si
Si O2
Si O2
Mg2 O4 Si
Mg O
Figure of merit
0.538
1.379
1.606
1.521
1.098
Phase reg. detail
User (COD)
ICDD (PDF2/Release
2012
ICDD
(PDF2/Release
User (COD)2012
DB card number
2104748
01-076-2979
01-075-3170
9000269
9006801
User (COD)
Weight ratio
Tahap3
Content(%)
49.4(5)
20.8(6)
5.9(4)
16(2)
7.9(5)
Phase name
Silicon
Stishovite, syn
Silicon Oxide
Ringwoodite
Periclase
110
100
90
80
70
60
50
40
30
20
10
0
Tahap3
Silicon(%)
Stishovi..., syn(%)
Silicon Oxide(%)
Ringwoodite(%)
Periclase(%)
Measurement profile
Meas. data:Tahap3/Data 1
Intensity (counts)
1000
500
0
Silicon, Si, 2104748
Stishovite, syn, Si O2, 01-076-2979
Silicon Oxide, Si O2, 01-075-3170
Ringwoodite, Mg2 O4 Si, 9000269
Periclase, Mg O, 9006801
20
40
60
80
2-theta (deg)
Universitas Sumatera Utara
Lampiran 12. Difraktogram Nanosilikon Hasil Reaksi Pada Suhu 800°C selama
7 jam
General information
Analysis date
Sample name
File name
2015/03/31 13:00:01
NANO_RUNNINGII
NANO_SILIKA
RUNNINGII.ras
Measurement date
Operator
2015/03/19 10:06:56
administrator
Measurement profile
Meas. data:NANO_SILIKA RUNNINGII/Data
1
BG data:NANO_SILIKA RUNNINGII/Data 1
Calc. data:NANO_SILIKA RUNNINGII/Data
1
Intensity (counts)
3000
2000
1000
0
20
40
60
80
2-theta (deg)
Peak list
No.
2theta(deg)
d(ang.)
Height(count
s)
FWHM(deg
)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
15.336(7)
18.945(17)
20.898(7)
26.681(10)
28.331(4)
28.495(4)
29.550(13)
30.883(13)
37.259(7)
39.15(2)
43.236(14)
44.215(11)
44.712(19)
47.318(6)
51.504(11)
56.142(4)
58.11(3)
59.41(3)
60.50(3)
61.28(2)
62.686(18)
65.20(3)
66.495(19)
69.139(7)
72.42(5)
75.33(4)
76.450(7)
79.41(3)
81.30(13)
83.97(7)
88.038(6)
5.773(3)
4.681(4)
4.2474(14)
3.3384(12)
3.1476(5)
3.1298(4)
3.0205(13)
2.8931(12)
2.4113(4)
2.2989(12)
2.0908(6)
2.0468(5)
2.0252(8)
1.9195(2)
1.7729(3)
1.63696(12)
1.5862(8)
1.5545(8)
1.5291(7)
1.5115(5)
1.4809(4)
1.4296(6)
1.4050(4)
1.35758(12)
1.3040(8)
1.2607(6)
1.24492(10)
1.2058(4)
1.1824(15)
1.1516(8)
1.10851(6)
477(22)
33(6)
344(19)
102(10)
687(26)
1983(45)
311(18)
419(20)
167(13)
149(12)
372(19)
148(12)
176(13)
1045(32)
315(18)
673(26)
41(6)
46(7)
53(7)
114(11)
129(11)
84(9)
58(8)
254(16)
31(6)
42(6)
378(19)
36(6)
24(5)
29(5)
358(19)
0.215(7)
0.19(5)
0.108(5)
0.31(4)
0.119(13)
0.154(8)
0.203(11)
0.209(18)
0.58(3)
0.21(2)
0.244(13)
0.14(3)
0.26(4)
0.192(9)
0.234(17)
0.163(6)
0.14(4)
0.31(5)
0.23(5)
0.25(3)
0.371(18)
0.43(4)
0.24(4)
0.161(7)
0.35(6)
0.44(6)
0.210(8)
0.24(6)
0.49(9)
0.32(8)
0.199(5)
Int.
I(counts
deg)
143(3)
7(2)
41.4(17)
46(3)
111(20)
424(21)
95.1(19)
146(3)
129(4)
46.3(19)
128(3)
38(6)
84(7)
329(5)
117(2)
150(2)
7.5(15)
20(2)
16.2(15)
38(2)
56(2)
49(2)
20(2)
55.7(16)
12(2)
27(3)
114(2)
15.8(18)
12(2)
10(2)
88(2)
Int.
W(deg)
Asym.
factor
0.30(2)
0.20(11)
0.120(11)
0.45(8)
0.16(4)
0.214(15)
0.31(2)
0.35(2)
0.78(8)
0.31(4)
0.34(2)
0.26(6)
0.48(8)
0.315(15)
0.37(3)
0.222(12)
0.18(6)
0.43(12)
0.31(7)
0.33(5)
0.43(5)
0.58(9)
0.35(8)
0.22(2)
0.38(13)
0.64(17)
0.30(2)
0.44(12)
0.5(2)
0.35(13)
0.245(19)
1.7(3)
0.2(4)
0.64(17)
5(5)
0.51(19)
1.8(2)
1.3(4)
0.9(3)
3.5(10)
1.5(7)
1.0(3)
0.7(2)
0.6(2)
1.00(13)
0.82(18)
1.04(13)
0.4(5)
2.3(9)
1.8(10)
1.2(5)
0.34(10)
0.7(3)
0.34(11)
1.0(2)
3(2)
1.7(6)
1.5(3)
2(2)
0.9(9)
1.0(8)
1.23(18)
Universitas Sumatera Utara
Lampiran 13.
Hasil Analisa Kuantitatif Nanosilikon Hasil Reaksi Pada Suhu
800°C selama 7 jam
General information
Analysis date
Sample name
2015/03/31 13:05:10
NANO_RUNNINGII
File name
NANO_SILIKA
RUNNINGII.ras
Measurement
date
Operator
2015/03/19 10:06:56
administrator
Comment
Qualitative analysis results
Phase name
Silicon
Periclase
perovskite (Mg, Si)
HP,
syn,
magnesium
silicon
dioxide
Quartz
Formula
Si
Mg O
Mg Si O3
Si O2
O2 Si
Figure of merit
0.745
0.984
1.474
1.467
1.635
Phase reg. detail
User (COD)
User (COD)
ICDD (PDF-2/Release
2012
ICDD RDB)
(PDF-2/Release
2012
RDB)
User (COD)
DB card number
9013102
9013225
01-080-0568
01-070-5689
9010146
Weight ratio
Phase name
Silicon
Periclase
perovskite (Mg, Si) HP,
syn,
magnesium
silicon
dioxide catenaQuartz
Content(%)
29(6)
7(4)
13(5)
43(4)
8.0(18)
NANO_SILIKA RUNNINGII
0
50
100
Wt(%)
Silicon
Periclase
rovskite (Mg, Si) HP, syn, magnesium catena-silicate
silicon dioxide
Quartz
Measurement profile
Universitas Sumatera Utara