Analisis Komposisi Asam Lemak Dari Berbagai Merek Sabun Mandi Dengan Menggunakan GC-MS
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Lampiran 7. Gambar spekt
rum massa darisabundet
t
ol
Library Search
>
Line#:1 R.Time:24.667(Scan#:2961) MassPeaks:99
RawMode:Single 24.667(2961) BasePeak:74.05(879113)
BG Mode:None Group 1 - Event 1
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Sampel
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Hit#:1 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
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Hit#:2 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
129
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:3 Entry:113510 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:4 Entry:113510 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
115
143
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171
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:5 Entry:113512 Library:WILEY7.LIB
SI:94 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
20
30
40
50
60
101
70
80
90
100
129
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143
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Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:30.533(Scan#:3665) MassPeaks:61
RawMode:Single 30.533(3665) BasePeak:74.05(253599)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
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Hit#:1 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
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Hit#:2 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
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Hit#:3 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
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Hit#:4 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
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Hit#:5 Entry:148370 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
20
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101
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Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:35.892(Scan#:4308) MassPeaks:130
RawMode:Single 35.892(4308) BasePeak:74.05(2199629)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
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51
115
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Hit#:1 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
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101
39
115
129
157
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Hit#:2 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
57
101
39
115
129
157
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Hit#:3 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
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Hit#:4 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
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171
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Hit#:5 Entry:180434 Library:WILEY7.LIB
SI:94 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
143
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101
27
20
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50
Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:39.875(Scan#:4786) MassPeaks:67
RawMode:Single 39.875(4786) BasePeak:67.05(41863)
BG Mode:None Group 1 - Event 1
100
67
81
95
55
Sampel
109
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135
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164
207
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Hit#:1 Entry:205831 Library:WILEY7.LIB
SI:94 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
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41
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Hit#:2 Entry:205831 Library:WILEY7.LIB
SI:94 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
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55
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Hit#:3 Entry:205820 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
123
27
136
150
294
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Hit#:4 Entry:205820 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
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Hit#:5 Entry:205817 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
20
294
123
27
40
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263
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51
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Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.133(Scan#:4817) MassPeaks:170
RawMode:Single 40.133(4817) BasePeak:55.05(500029)
BG Mode:None Group 1 - Event 1
100
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69
74
97
Sampel
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Hit#:1 Entry:207862 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
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Hit#:2 Entry:207862 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
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Hit#:3 Entry:207854 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
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222
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Hit#:4 Entry:207854 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
152
222
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Hit#:5 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
30
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110
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150
166
222
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170
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296
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Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.717(Scan#:4887) MassPeaks:105
RawMode:Single 40.717(4887) BasePeak:74.05(550658)
BG Mode:None Group 1 - Event 1
100
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87
Sampel
55
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Hit#:1 Entry:209839 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
143
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101
27
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Hit#:2 Entry:209839 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
143
57
101
27
115
129
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Hit#:3 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
115
298
129
185
157
199
255
213
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267
10
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Hit#:4 Entry:209842 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
18
143
57
41
101
115
129
185
157
199
255
213
241
298
267
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110
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290
Hit#:5 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
10
30
50
70
90
115
110
298
129
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185
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53
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Universitas Sumatera Utara
Lampiran 8. Gambar spekt
rum massa darisabunlux
Library Search
>
Line#:1 R.Time:11.325(Scan#:1360) MassPeaks:26
RawMode:Single 11.325(1360) BasePeak:74.05(124650)
BG Mode:None Group 1 - Event 1
100
74
Sampel
87
5557
127
115
101
53
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Hit#:1 Entry:47794 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
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Hit#:2 Entry:47794 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
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Hit#:3 Entry:47791 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
41
27
Me (CH 2 ) 6 C(O) OMe
87
43
57
127
115
101
158
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Hit#:4 Entry:47791 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
41
27
Me (CH 2 ) 6 C(O) OMe
87
43
57
127
115
101
158
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20
30
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100
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120
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140
150
Hit#:5 Entry:47799 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
43
10
20
57
41
27
30
40
50
60
70
80
90
54
100
127
115
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
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Line#:1 R.Time:18.217(Scan#:2187) MassPeaks:29
RawMode:Single 18.217(2187) BasePeak:74.05(76702)
BG Mode:None Group 1 - Event 1
100
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87
Sampel
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Hit#:1 Entry:79106 Library:WILEY7.LIB
SI:96 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
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Hit#:2 Entry:79106 Library:WILEY7.LIB
SI:96 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
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Hit#:3 Entry:79114 Library:WILEY7.LIB
SI:95 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
41
Me (CH 2 ) 8 C(O) OMe
59
27
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186
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Hit#:4 Entry:79114 Library:WILEY7.LIB
SI:95 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
41
Me (CH 2 ) 8 C(O) OMe
59
27
143
101
155
129
115
186
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Hit#:5 Entry:79112 Library:WILEY7.LIB
SI:95 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
43
28
59
27
20
Me (CH 2 ) 8 C(O) OMe
30
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101
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100
129
115
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55
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:24.675(Scan#:2962) MassPeaks:70
RawMode:Single 24.675(2962) BasePeak:74.05(491450)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
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53
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Hit#:1 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
129
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183
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Hit#:2 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
129
115
143
157
171
214
183
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Hit#:3 Entry:113510 Library:WILEY7.LIB
SI:95 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
115
143
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171
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:4 Entry:113510 Library:WILEY7.LIB
SI:95 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
115
143
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171
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:5 Entry:113512 Library:WILEY7.LIB
SI:94 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
20
30
40
50
60
101
70
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130
56
143
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
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Line#:1 R.Time:30.542(Scan#:3666) MassPeaks:40
RawMode:Single 30.542(3666) BasePeak:74.05(82709)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
53
115
129
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242
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Hit#:1 Entry:148367 Library:WILEY7.LIB
SI:96 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
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Hit#:2 Entry:148367 Library:WILEY7.LIB
SI:96 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
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Hit#:3 Entry:148370 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
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129
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Hit#:4 Entry:148370 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
101
115
129
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Hit#:5 Entry:148374 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
57
101
40
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
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Line#:1 R.Time:35.875(Scan#:4306) MassPeaks:88
RawMode:Single 35.875(4306) BasePeak:74.05(534881)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
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53
115
129
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Hit#:1 Entry:180434 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
143
57
101
27
115
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Hit#:2 Entry:180434 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
143
57
101
27
115
129
157
171
185
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Hit#:3 Entry:180475 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:5129-60-2 MolWeight:270 RetIndex:0
CompName:Pentadecanoic acid, 14-methyl-, methyl ester (CAS) METHYL 14-METHYL-PENTADECANOATE $$ 14-METHYL-PENTADECANSAEUR
100
74
87
Me 2 CH (CH 2 ) 12 C(O) OMe
41
57
143
101
31
115
227
129
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Hit#:4 Entry:180475 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:5129-60-2 MolWeight:270 RetIndex:0
CompName:Pentadecanoic acid, 14-methyl-, methyl ester (CAS) METHYL 14-METHYL-PENTADECANOATE $$ 14-METHYL-PENTADECANSAEUR
100
74
87
Me 2 CH (CH 2 ) 12 C(O) OMe
41
57
143
101
31
115
227
129
171
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239
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Hit#:5 Entry:257015 Library:WILEY7.LIB
SI:95 Formula:C21 H38 O4 CAS:140-03-4 MolWeight:354 RetIndex:0
CompName:9-Octadecenoic acid, 12-(acetyloxy)-, methyl ester, [R-(Z)]- (CAS) Flexricin P-4 $$ Methyl 12-acetoxyoleate $$ Methyl acetyl ricinoleate $$ M
100
74
87
OAc
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH(CH 2 ) 5 Me
55
41
143
57
14
10
101
27
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58
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
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Line#:1 R.Time:39.983(Scan#:4799) MassPeaks:40
RawMode:Single 39.983(4799) BasePeak:67.05(16992)
BG Mode:None Group 1 - Event 1
100
67
81
55
95
Sampel
109
121
53
135
207
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Hit#:1 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
81
55
95
109
27
123
136
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294
164
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Hit#:2 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
81
55
95
109
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123
136
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294
164
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Hit#:3 Entry:232178 Library:WILEY7.LIB
SI:93 Formula:C21 H38 O2 CAS:2463-02-7 MolWeight:322 RetIndex:0
CompName:11,14-Eicosadienoic acid, methyl ester (CAS) METHYL-11,14-EICOSADIENOATE $$
100
67
41
220
240
260
280
55
81
95
Me O C(O) (CH 2 ) 9 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
39
123
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Hit#:4 Entry:232178 Library:WILEY7.LIB
SI:93 Formula:C21 H38 O2 CAS:2463-02-7 MolWeight:322 RetIndex:0
CompName:11,14-Eicosadienoic acid, methyl ester (CAS) METHYL-11,14-EICOSADIENOATE $$
100
67
41
220
240
260
280
55
81
95
Me O C(O) (CH 2 ) 9 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
39
123
135
150
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Hit#:5 Entry:205809 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:2566-97-4 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid, methyl ester, (E,E)- (CAS) Methyl linolelaidate $$ METHYL T9, T12 OCTADECADIENOATE $$ METHYL TRA
100
41
67
55
81
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
95
109
39
20
40
123
60
80
100
120
135
140
149
163
160
180
59
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220
240
260
280
Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
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Line#:1 R.Time:40.125(Scan#:4816) MassPeaks:114
RawMode:Single 40.125(4816) BasePeak:55.05(119344)
BG Mode:None Group 1 - Event 1
100
55
69
83
97
98
Sampel
123
53
137
152
166
180
207
193
222
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264
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Hit#:1 Entry:207855 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
41
69 74
87
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
98
123
27
137
180
264
222
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Hit#:2 Entry:207855 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
41
69 74
87
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
98
123
27
137
180
264
222
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Hit#:3 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
39
152
166
222
180
296
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40
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80
100
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160
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280
Hit#:4 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
39
152
166
222
180
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40
60
80
100
120
140
160
180
Hit#:5 Entry:207515 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2345-29-1 MolWeight:296 RetIndex:0
CompName:8-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-8-ENOATE $$
100
55
296
200
220
240
260
280
41
69 74
84
Me O C(O) (CH 2 )6 CH CH (CH 2 ) 8 Me
98
20
264
123
27
40
60
80
100
120
180
137
140
222
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180
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.725(Scan#:4888) MassPeaks:46
RawMode:Single 40.725(4888) BasePeak:74.05(56956)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
54
115
129
157
171
185
199
213
241
255
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290
Hit#:1 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
115
298
129
185
157
199
255
213
241
267
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290
Hit#:2 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
115
298
129
185
157
199
255
213
241
267
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Hit#:3 Entry:209842 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
18
143
57
41
101
115
129
185
157
199
255
213
241
298
267
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Hit#:4 Entry:209842 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
18
143
57
41
101
115
129
185
157
199
255
213
241
298
267
10
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130
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290
Hit#:5 Entry:209839 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
143
57
101
27
10
30
50
70
90
115
110
129
130
157
150
171
170
61
185
190
255
199
213
210
230
298
267
241
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Universitas Sumatera Utara
Lampiran 9. Gambar spekt
rum massa darisabunci
t
ra
Library Search
>
Line#:1 R.Time:11.325(Scan#:1360) MassPeaks:43
RawMode:Single 11.325(1360) BasePeak:74.00(480446)
BG Mode:None Group 1 - Event 1
100
74
Sampel
87
55 57
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115
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143
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Hit#:1 Entry:47794 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
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Hit#:2 Entry:47794 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
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Hit#:3 Entry:47792 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
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Hit#:4 Entry:47792 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
20
30
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60
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100
110
120
130
140
150
Hit#:5 Entry:47799 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
43
10
20
57
41
27
30
40
50
60
70
80
90
62
100
127
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Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:18.217(Scan#:2187) MassPeaks:46
RawMode:Single 18.217(2187) BasePeak:74.00(261743)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
53
59
143
101
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129
115
186
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Hit#:1 Entry:79106 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
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186
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Hit#:2 Entry:79106 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
101
129
115
143
155
186
20
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Hit#:3 Entry:79111 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
101
129
112
143
155
186
20
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Hit#:4 Entry:79111 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
101
129
112
143
155
186
20
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Hit#:5 Entry:79114 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
41
59
27
20
30
40
Me (CH 2 ) 8 C(O) OMe
50
60
143
101
70
80
90
100
110
63
155
129
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Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:24.692(Scan#:2964) MassPeaks:94
RawMode:Single 24.692(2964) BasePeak:74.05(1653988)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
69
101
51
115
129
143
157
171
183
199
214
253
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:1 Entry:113515 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:2 Entry:113515 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:3 Entry:113510 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:4 Entry:113510 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:5 Entry:113512 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
20
30
40
50
60
101
70
80
90
115
129
143
157
171
183
214
100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
64
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:30.558(Scan#:3668) MassPeaks:76
RawMode:Single 30.558(3668) BasePeak:74.00(497812)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
69
101
53
115
129
157
185
171
199
211
242
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Hit#:1 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
171
185
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242
211
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60 70
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90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:2 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
171
185
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211
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40 50
60 70
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90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:3 Entry:148370 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
101
115
129
143
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242
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Hit#:4 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
157
171
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242
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90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:5 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
20
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50
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100
115
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140
65
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Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:35.917(Scan#:4311) MassPeaks:133
RawMode:Single 35.917(4311) BasePeak:74.05(2327218)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
51
115
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Hit#:1 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
57
101
39
115
129
157
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20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:2 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
57
101
39
115
129
157
171
185
199
213
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239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:3 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
157
171
185
199
213
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239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:4 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
157
171
185
199
213
227
239
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Hit#:5 Entry:180451 Library:WILEY7.LIB
SI:94 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
57
101
27
20
30
40
50
60
70
80
115
129
143
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171
185
199
213
227
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270
90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
66
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:39.992(Scan#:4800) MassPeaks:91
RawMode:Single 39.992(4800) BasePeak:67.05(93673)
BG Mode:None Group 1 - Event 1
100
67
81
95
55
Sampel
109
123
135
51
150
164
178
207
191
262
220
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Hit#:1 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
294
280
81
55
95
109
27
123
136
150
294
164
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100
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Hit#:2 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
81
55
95
109
27
123
136
150
294
164
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100
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280
Hit#:3 Entry:205817 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
294
123
27
136
150
263
164
20
40
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100
120
140
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260
280
Hit#:4 Entry:205817 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
294
123
27
136
150
263
164
20
40
60
80
100
120
140
160
180
200
220
240
260
280
Hit#:5 Entry:205809 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:2566-97-4 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid, methyl ester, (E,E)- (CAS) Methyl linolelaidate $$ METHYL T9, T12 OCTADECADIENOATE $$ METHYL TRA
100
41
67
55
81
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
95
109
39
20
40
123
60
80
100
120
135
140
149
163
160
180
67
200
220
240
260
280
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.150(Scan#:4819) MassPeaks:151
RawMode:Single 40.150(4819) BasePeak:55.05(324616)
BG Mode:None Group 1 - Event 1
100
55
69
74
97
98
Sampel
123
137
51
152
166
180
193
207
222
235
246
264
266
296
30
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70
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110
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290
Hit#:1 Entry:207854 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
152
222
30
50
70
90
110
130
150
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190
210
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250
270
290
Hit#:2 Entry:207854 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
152
222
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:3 Entry:207862 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
166
180
222
264
30
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70
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110
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190
210
230
250
270
290
Hit#:4 Entry:207862 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
166
180
222
264
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:5 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
30
50
70
90
110
130
152
150
166
222
180
170
68
296
190
210
230
250
270
290
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.733(Scan#:4889) MassPeaks:84
RawMode:Single 40.733(4889) BasePeak:74.05(180631)
BG Mode:None Group 1 - Event 1
100
74
87
55
Sampel
143
69
101
53
115
129
157
171
185
199
213
241
227
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Universitas Sumatera Utara
Lampiran 7. Gambar spekt
rum massa darisabundet
t
ol
Library Search
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Line#:1 R.Time:24.667(Scan#:2961) MassPeaks:99
RawMode:Single 24.667(2961) BasePeak:74.05(879113)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
101
50
129
115
143
157
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183
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Hit#:1 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
129
115
143
157
171
214
183
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:2 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
129
115
143
157
171
214
183
20
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:3 Entry:113510 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
115
143
157
171
183
214
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50
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90
100 110 120 130 140 150 160 170 180 190 200 210
Hit#:4 Entry:113510 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
115
143
157
171
183
214
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70
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90
100 110 120 130 140 150 160 170 180 190 200 210
Hit#:5 Entry:113512 Library:WILEY7.LIB
SI:94 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
20
30
40
50
60
101
70
80
90
100
129
115
110
120
130
48
143
157
140
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170
183
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214
190
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210
Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:30.533(Scan#:3665) MassPeaks:61
RawMode:Single 30.533(3665) BasePeak:74.05(253599)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
53
115
129
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211
242
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Hit#:1 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
157
171
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242
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Hit#:2 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
157
171
185
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211
242
20 30
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60 70
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Hit#:3 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
171
185
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242
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20 30
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90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:4 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
171
185
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242
211
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60 70
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90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:5 Entry:148370 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
20
30
101
40
50
60
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90
100
115
110
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130
143
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49
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Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:35.892(Scan#:4308) MassPeaks:130
RawMode:Single 35.892(4308) BasePeak:74.05(2199629)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
51
115
129
157
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185
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213
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270
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Hit#:1 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
57
101
39
115
129
157
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185
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Hit#:2 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
57
101
39
115
129
157
171
185
199
213
227
239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:3 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
157
171
185
199
213
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239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:4 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
157
171
185
199
213
227
239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:5 Entry:180434 Library:WILEY7.LIB
SI:94 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
143
57
101
27
20
30
40
50
60
70
80
115
129
157
171
185
199
227
213
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90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
50
Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:39.875(Scan#:4786) MassPeaks:67
RawMode:Single 39.875(4786) BasePeak:67.05(41863)
BG Mode:None Group 1 - Event 1
100
67
81
95
55
Sampel
109
121
53
135
150
164
207
178
262
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Hit#:1 Entry:205831 Library:WILEY7.LIB
SI:94 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
294
280
81
55
95
109
27
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294
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Hit#:2 Entry:205831 Library:WILEY7.LIB
SI:94 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
81
55
95
109
27
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136
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294
164
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Hit#:3 Entry:205820 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
123
27
136
150
294
263
164
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Hit#:4 Entry:205820 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
123
27
136
150
294
263
164
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Hit#:5 Entry:205817 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
20
294
123
27
40
60
80
100
120
136
140
150
263
164
160
180
51
200
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240
260
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Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.133(Scan#:4817) MassPeaks:170
RawMode:Single 40.133(4817) BasePeak:55.05(500029)
BG Mode:None Group 1 - Event 1
100
55
69
74
97
Sampel
98
123
137
152
51
166
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222
193
207
235
246
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Hit#:1 Entry:207862 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
166
180
222
264
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Hit#:2 Entry:207862 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
166
180
222
264
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170
190
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Hit#:3 Entry:207854 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
152
222
30
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110
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170
190
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270
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Hit#:4 Entry:207854 Library:WILEY7.LIB
SI:96 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
152
222
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:5 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
30
50
70
90
110
130
152
150
166
222
180
170
52
296
190
210
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250
270
290
Universitas Sumatera Utara
Lampiran 7. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.717(Scan#:4887) MassPeaks:105
RawMode:Single 40.717(4887) BasePeak:74.05(550658)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
53
115
129
157
171
185
199
213
241
227
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267
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Hit#:1 Entry:209839 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
143
57
101
27
115
129
157
171
185
255
199
213
298
267
241
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Hit#:2 Entry:209839 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
143
57
101
27
115
129
157
171
185
255
199
213
298
267
241
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290
Hit#:3 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
115
298
129
185
157
199
255
213
241
267
10
30
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110
130
150
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190
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230
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270
290
Hit#:4 Entry:209842 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
18
143
57
41
101
115
129
185
157
199
255
213
241
298
267
10
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:5 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
10
30
50
70
90
115
110
298
129
130
185
157
150
170
53
190
199
255
213
210
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230
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267
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290
Universitas Sumatera Utara
Lampiran 8. Gambar spekt
rum massa darisabunlux
Library Search
>
Line#:1 R.Time:11.325(Scan#:1360) MassPeaks:26
RawMode:Single 11.325(1360) BasePeak:74.05(124650)
BG Mode:None Group 1 - Event 1
100
74
Sampel
87
5557
127
115
101
53
10
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40
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60
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100
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120
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Hit#:1 Entry:47794 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
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20
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40
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60
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100
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120
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Hit#:2 Entry:47794 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
20
30
40
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60
70
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90
100
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120
130
140
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Hit#:3 Entry:47791 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
41
27
Me (CH 2 ) 6 C(O) OMe
87
43
57
127
115
101
158
10
20
30
40
50
60
70
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90
100
110
120
130
140
150
Hit#:4 Entry:47791 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
41
27
Me (CH 2 ) 6 C(O) OMe
87
43
57
127
115
101
158
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
Hit#:5 Entry:47799 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
43
10
20
57
41
27
30
40
50
60
70
80
90
54
100
127
115
101
110
158
143
120
130
140
150
Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:18.217(Scan#:2187) MassPeaks:29
RawMode:Single 18.217(2187) BasePeak:74.05(76702)
BG Mode:None Group 1 - Event 1
100
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87
Sampel
55
59
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53
129
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Hit#:1 Entry:79106 Library:WILEY7.LIB
SI:96 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
101
129
115
143
155
186
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Hit#:2 Entry:79106 Library:WILEY7.LIB
SI:96 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
101
129
115
143
155
186
20
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Hit#:3 Entry:79114 Library:WILEY7.LIB
SI:95 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
41
Me (CH 2 ) 8 C(O) OMe
59
27
143
101
155
129
115
186
20
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Hit#:4 Entry:79114 Library:WILEY7.LIB
SI:95 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
41
Me (CH 2 ) 8 C(O) OMe
59
27
143
101
155
129
115
186
20
30
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Hit#:5 Entry:79112 Library:WILEY7.LIB
SI:95 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
43
28
59
27
20
Me (CH 2 ) 8 C(O) OMe
30
40
50
60
101
70
80
90
100
129
115
110
55
120
130
143
140
155
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186
160
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:24.675(Scan#:2962) MassPeaks:70
RawMode:Single 24.675(2962) BasePeak:74.05(491450)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
101
53
129
115
143
157
171
183
214
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:1 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
129
115
143
157
171
214
183
20
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:2 Entry:113515 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
129
115
143
157
171
214
183
20
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100 110 120 130 140 150 160 170 180 190 200 210
Hit#:3 Entry:113510 Library:WILEY7.LIB
SI:95 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
115
143
157
171
183
214
20
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50
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70
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90
100 110 120 130 140 150 160 170 180 190 200 210
Hit#:4 Entry:113510 Library:WILEY7.LIB
SI:95 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
129
115
143
157
171
183
214
20
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90
100 110 120 130 140 150 160 170 180 190 200 210
Hit#:5 Entry:113512 Library:WILEY7.LIB
SI:94 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
20
30
40
50
60
101
70
80
90
100
129
115
110
120
130
56
143
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183
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214
190
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210
Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:30.542(Scan#:3666) MassPeaks:40
RawMode:Single 30.542(3666) BasePeak:74.05(82709)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
53
115
129
157
185
171
199
211
242
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Hit#:1 Entry:148367 Library:WILEY7.LIB
SI:96 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
157
171
185
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242
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Hit#:2 Entry:148367 Library:WILEY7.LIB
SI:96 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
157
171
185
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211
242
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90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:3 Entry:148370 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
101
115
129
143
157
185
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242
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Hit#:4 Entry:148370 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
101
115
129
143
157
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242
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Hit#:5 Entry:148374 Library:WILEY7.LIB
SI:94 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
57
101
40
20
30
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50
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Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:35.875(Scan#:4306) MassPeaks:88
RawMode:Single 35.875(4306) BasePeak:74.05(534881)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
53
115
129
157
171
185
199
213
227
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Hit#:1 Entry:180434 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
143
57
101
27
115
129
157
171
185
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227
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Hit#:2 Entry:180434 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
143
57
101
27
115
129
157
171
185
199
227
213
270
239
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110
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Hit#:3 Entry:180475 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:5129-60-2 MolWeight:270 RetIndex:0
CompName:Pentadecanoic acid, 14-methyl-, methyl ester (CAS) METHYL 14-METHYL-PENTADECANOATE $$ 14-METHYL-PENTADECANSAEUR
100
74
87
Me 2 CH (CH 2 ) 12 C(O) OMe
41
57
143
101
31
115
227
129
171
185
199
213
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239
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Hit#:4 Entry:180475 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:5129-60-2 MolWeight:270 RetIndex:0
CompName:Pentadecanoic acid, 14-methyl-, methyl ester (CAS) METHYL 14-METHYL-PENTADECANOATE $$ 14-METHYL-PENTADECANSAEUR
100
74
87
Me 2 CH (CH 2 ) 12 C(O) OMe
41
57
143
101
31
115
227
129
171
185
199
213
270
239
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Hit#:5 Entry:257015 Library:WILEY7.LIB
SI:95 Formula:C21 H38 O4 CAS:140-03-4 MolWeight:354 RetIndex:0
CompName:9-Octadecenoic acid, 12-(acetyloxy)-, methyl ester, [R-(Z)]- (CAS) Flexricin P-4 $$ Methyl 12-acetoxyoleate $$ Methyl acetyl ricinoleate $$ M
100
74
87
OAc
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH(CH 2 ) 5 Me
55
41
143
57
14
10
101
27
30
50
70
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115
110
129
130
157
150
58
171
170
185
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213
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270
Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:39.983(Scan#:4799) MassPeaks:40
RawMode:Single 39.983(4799) BasePeak:67.05(16992)
BG Mode:None Group 1 - Event 1
100
67
81
55
95
Sampel
109
121
53
135
207
149
20
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Hit#:1 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
81
55
95
109
27
123
136
150
294
164
20
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Hit#:2 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
81
55
95
109
27
123
136
150
294
164
20
40
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140
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Hit#:3 Entry:232178 Library:WILEY7.LIB
SI:93 Formula:C21 H38 O2 CAS:2463-02-7 MolWeight:322 RetIndex:0
CompName:11,14-Eicosadienoic acid, methyl ester (CAS) METHYL-11,14-EICOSADIENOATE $$
100
67
41
220
240
260
280
55
81
95
Me O C(O) (CH 2 ) 9 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
39
123
135
150
20
40
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Hit#:4 Entry:232178 Library:WILEY7.LIB
SI:93 Formula:C21 H38 O2 CAS:2463-02-7 MolWeight:322 RetIndex:0
CompName:11,14-Eicosadienoic acid, methyl ester (CAS) METHYL-11,14-EICOSADIENOATE $$
100
67
41
220
240
260
280
55
81
95
Me O C(O) (CH 2 ) 9 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
39
123
135
150
20
40
60
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100
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140
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Hit#:5 Entry:205809 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:2566-97-4 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid, methyl ester, (E,E)- (CAS) Methyl linolelaidate $$ METHYL T9, T12 OCTADECADIENOATE $$ METHYL TRA
100
41
67
55
81
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
95
109
39
20
40
123
60
80
100
120
135
140
149
163
160
180
59
200
220
240
260
280
Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.125(Scan#:4816) MassPeaks:114
RawMode:Single 40.125(4816) BasePeak:55.05(119344)
BG Mode:None Group 1 - Event 1
100
55
69
83
97
98
Sampel
123
53
137
152
166
180
207
193
222
235
264
246
20
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280
Hit#:1 Entry:207855 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
41
69 74
87
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
98
123
27
137
180
264
222
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Hit#:2 Entry:207855 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
41
69 74
87
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
98
123
27
137
180
264
222
20
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60
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100
120
140
160
180
200
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240
260
280
Hit#:3 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
39
152
166
222
180
296
20
40
60
80
100
120
140
160
180
200
220
240
260
280
Hit#:4 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
39
152
166
222
180
20
40
60
80
100
120
140
160
180
Hit#:5 Entry:207515 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2345-29-1 MolWeight:296 RetIndex:0
CompName:8-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-8-ENOATE $$
100
55
296
200
220
240
260
280
41
69 74
84
Me O C(O) (CH 2 )6 CH CH (CH 2 ) 8 Me
98
20
264
123
27
40
60
80
100
120
180
137
140
222
160
180
60
200
220
240
260
280
Universitas Sumatera Utara
Lampiran 8. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.725(Scan#:4888) MassPeaks:46
RawMode:Single 40.725(4888) BasePeak:74.05(56956)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
54
115
129
157
171
185
199
213
241
255
269
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290
Hit#:1 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
115
298
129
185
157
199
255
213
241
267
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130
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170
190
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250
270
290
Hit#:2 Entry:209838 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
18
143
57
101
115
298
129
185
157
199
255
213
241
267
10
30
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70
90
110
130
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170
190
210
230
250
270
290
Hit#:3 Entry:209842 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
18
143
57
41
101
115
129
185
157
199
255
213
241
298
267
10
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50
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90
110
130
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170
190
210
230
250
270
290
Hit#:4 Entry:209842 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
18
143
57
41
101
115
129
185
157
199
255
213
241
298
267
10
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:5 Entry:209839 Library:WILEY7.LIB
SI:95 Formula:C19 H38 O2 CAS:112-61-8 MolWeight:298 RetIndex:0
CompName:Octadecanoic acid, methyl ester (CAS) Methyl stearate $$ Methyl octadecanoate $$ Methyl n-octadecanoate $$ Stearic acid methyl ester $$ Kem
100
74
87
Me (CH 2 ) 16 C(O) OMe
43
41
143
57
101
27
10
30
50
70
90
115
110
129
130
157
150
171
170
61
185
190
255
199
213
210
230
298
267
241
250
270
290
Universitas Sumatera Utara
Lampiran 9. Gambar spekt
rum massa darisabunci
t
ra
Library Search
>
Line#:1 R.Time:11.325(Scan#:1360) MassPeaks:43
RawMode:Single 11.325(1360) BasePeak:74.00(480446)
BG Mode:None Group 1 - Event 1
100
74
Sampel
87
55 57
127
115
101
51
143
10
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Hit#:1 Entry:47794 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
20
30
40
50
60
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90
100
110
120
130
140
150
Hit#:2 Entry:47794 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
Hit#:3 Entry:47792 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
Hit#:4 Entry:47792 Library:WILEY7.LIB
SI:98 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
4143
57
27
127
115
101
158
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
Hit#:5 Entry:47799 Library:WILEY7.LIB
SI:97 Formula:C9 H18 O2 CAS:111-11-5 MolWeight:158 RetIndex:0
CompName:Octanoic acid, methyl ester (CAS) Methyl octanoate $$ OCTANOIC ACID METHYL ESTER $$ Methyl caprylate $$ Methyl n-octanoate $$ C
100
74
Me (CH 2 ) 6 C(O) OMe
87
43
10
20
57
41
27
30
40
50
60
70
80
90
62
100
127
115
101
110
158
143
120
130
140
150
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:18.217(Scan#:2187) MassPeaks:46
RawMode:Single 18.217(2187) BasePeak:74.00(261743)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
53
59
143
101
155
129
115
186
20
30
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100
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Hit#:1 Entry:79106 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
101
129
115
143
155
186
20
30
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Hit#:2 Entry:79106 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
27
101
129
115
143
155
186
20
30
40
50
60
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90
100
110
120
130
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170
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Hit#:3 Entry:79111 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
101
129
112
143
155
186
20
30
40
50
60
70
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90
100
110
120
130
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170
180
Hit#:4 Entry:79111 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
Me (CH 2 ) 8 C(O) OMe
87
41
59
101
129
112
143
155
186
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
170
180
Hit#:5 Entry:79114 Library:WILEY7.LIB
SI:97 Formula:C11 H22 O2 CAS:110-42-9 MolWeight:186 RetIndex:0
CompName:Decanoic acid, methyl ester (CAS) Methyl caprate $$ Methyl decanoate $$ Capric acid methyl ester $$ Uniphat A30 $$ Metholene 2095 $$ Met
100
74
87
41
59
27
20
30
40
Me (CH 2 ) 8 C(O) OMe
50
60
143
101
70
80
90
100
110
63
155
129
115
120
130
140
150
186
160
170
180
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:24.692(Scan#:2964) MassPeaks:94
RawMode:Single 24.692(2964) BasePeak:74.05(1653988)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
69
101
51
115
129
143
157
171
183
199
214
253
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:1 Entry:113515 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:2 Entry:113515 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
41
57
39
Me (CH 2 ) 10 C(O) OMe
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:3 Entry:113510 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:4 Entry:113510 Library:WILEY7.LIB
SI:97 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
101
115
129
143
157
171
183
214
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
Hit#:5 Entry:113512 Library:WILEY7.LIB
SI:96 Formula:C13 H26 O2 CAS:111-82-0 MolWeight:214 RetIndex:0
CompName:Dodecanoic acid, methyl ester (CAS) Methyl laurate $$ Methyl dodecanoate $$ Methyl n-dodecanoate $$ Lauric acid methyl ester $$ Metholene
100
74
87
Me (CH 2 ) 10 C(O) OMe
41
57
27
20
30
40
50
60
101
70
80
90
115
129
143
157
171
183
214
100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250
64
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:30.558(Scan#:3668) MassPeaks:76
RawMode:Single 30.558(3668) BasePeak:74.00(497812)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
69
101
53
115
129
157
185
171
199
211
242
20 30
40 50
60 70
80
90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:1 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
171
185
199
242
211
20 30
40 50
60 70
80
90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:2 Entry:148369 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
41
Me (CH 2 ) 12 C(O) OMe
143
57
101
39
115
129
157
171
185
199
242
211
20 30
40 50
60 70
80
90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:3 Entry:148370 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
57
27
101
115
129
143
157
185
199
211
242
20 30
40 50
60 70
80
90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:4 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
115
129
157
171
185
199
211
242
20 30
40 50
60 70
80
90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240
Hit#:5 Entry:148367 Library:WILEY7.LIB
SI:95 Formula:C15 H30 O2 CAS:124-10-7 MolWeight:242 RetIndex:0
CompName:Tetradecanoic acid, methyl ester (CAS) Methyl myristate $$ Methyl tetradecanoate $$ Methyl n-tetradecanoate $$ Myristic acid methyl ester $$
100
74
87
Me (CH 2 ) 12 C(O) OMe
41
143
69
101
39
20
30
40
50
60
70
80
90
100
115
110
120
129
130
157
140
65
150
160
171
170
185
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190
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200
211
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242
220
230
240
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
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Line#:1 R.Time:35.917(Scan#:4311) MassPeaks:133
RawMode:Single 35.917(4311) BasePeak:74.05(2327218)
BG Mode:None Group 1 - Event 1
100
74
87
Sampel
55
143
101
51
115
129
157
171
185
199
213
227
239
255
270
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:1 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
57
101
39
115
129
157
171
185
199
213
227
239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:2 Entry:180435 Library:WILEY7.LIB
SI:96 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
270
143
57
101
39
115
129
157
171
185
199
213
227
239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:3 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
157
171
185
199
213
227
239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:4 Entry:180438 Library:WILEY7.LIB
SI:95 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
41
57
101
115
129
270
143
157
171
185
199
213
227
239
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
Hit#:5 Entry:180451 Library:WILEY7.LIB
SI:94 Formula:C17 H34 O2 CAS:112-39-0 MolWeight:270 RetIndex:0
CompName:Hexadecanoic acid, methyl ester (CAS) Methyl palmitate $$ Methyl hexadecanoate $$ Methyl n-hexadecanoate $$ Uniphat A60 $$ Metholene 2
100
74
87
Me (CH 2 ) 14 C(O) OMe
43
41
57
101
27
20
30
40
50
60
70
80
115
129
143
157
171
185
199
213
227
239
270
90 100 110 120 130 140 150 160 170 180 190 200 210 220 230 240 250 260 270
66
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:39.992(Scan#:4800) MassPeaks:91
RawMode:Single 39.992(4800) BasePeak:67.05(93673)
BG Mode:None Group 1 - Event 1
100
67
81
95
55
Sampel
109
123
135
51
150
164
178
207
191
262
220
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100
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180
200
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240
260
Hit#:1 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
294
280
81
55
95
109
27
123
136
150
294
164
20
40
60
80
100
120
140
160
180
200
220
240
260
Hit#:2 Entry:205831 Library:WILEY7.LIB
SI:95 Formula:C19 H34 O2 CAS:2462-85-3 MolWeight:294 RetIndex:0
CompName:OCTADECA-9,12-DIENOIC ACID METHYL ESTER $$ 9,12-OCTADECADIENOIC ACID, METHYL ESTER $$
100
67
41
280
81
55
95
109
27
123
136
150
294
164
20
40
60
80
100
120
140
160
180
200
220
240
260
280
Hit#:3 Entry:205817 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
294
123
27
136
150
263
164
20
40
60
80
100
120
140
160
180
200
220
240
260
280
Hit#:4 Entry:205817 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:112-63-0 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid (Z,Z)-, methyl ester (CAS) Methyl linoleate $$ METHYL CIS-9,CIS-12-OCTADECADIENOATE $$ Methyl octad
100
67
81
41
55
95
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
109
294
123
27
136
150
263
164
20
40
60
80
100
120
140
160
180
200
220
240
260
280
Hit#:5 Entry:205809 Library:WILEY7.LIB
SI:93 Formula:C19 H34 O2 CAS:2566-97-4 MolWeight:294 RetIndex:0
CompName:9,12-Octadecadienoic acid, methyl ester, (E,E)- (CAS) Methyl linolelaidate $$ METHYL T9, T12 OCTADECADIENOATE $$ METHYL TRA
100
41
67
55
81
Me O C(O) (CH 2 ) 7 CH CHCH 2 CH CH(CH 2 ) 4 Me
95
109
39
20
40
123
60
80
100
120
135
140
149
163
160
180
67
200
220
240
260
280
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.150(Scan#:4819) MassPeaks:151
RawMode:Single 40.150(4819) BasePeak:55.05(324616)
BG Mode:None Group 1 - Event 1
100
55
69
74
97
98
Sampel
123
137
51
152
166
180
193
207
222
235
246
264
266
296
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:1 Entry:207854 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
152
222
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:2 Entry:207854 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
97
98
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
41
123
137
180
152
222
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:3 Entry:207862 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
166
180
222
264
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:4 Entry:207862 Library:WILEY7.LIB
SI:95 Formula:C19 H36 O2 CAS:112-62-9 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid (Z)-, methyl ester (CAS) Methyl oleate $$ Methyl cis-9-octadecenoate $$ Oleic acid methyl ester $$ Oleic acid, methyl este
100
55
69
74
96
41
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
123
137
166
180
222
264
30
50
70
90
110
130
150
170
190
210
230
250
270
290
Hit#:5 Entry:207860 Library:WILEY7.LIB
SI:94 Formula:C19 H36 O2 CAS:2462-84-2 MolWeight:296 RetIndex:0
CompName:9-Octadecenoic acid, methyl ester (CAS) METHYL OCTADEC-9-ENOATE $$ Methyl 9-octadecenoate $$ METHYL OLEATE $$
100
55
69
41
83
97
Me O C(O) (CH 2 )7 CH CH (CH 2 ) 7 Me
264
123
137
30
50
70
90
110
130
152
150
166
222
180
170
68
296
190
210
230
250
270
290
Universitas Sumatera Utara
Lampiran 9. (lanj
ut
an)
Library Search
>
Line#:1 R.Time:40.733(Scan#:4889) MassPeaks:84
RawMode:Single 40.733(4889) BasePeak:74.05(180631)
BG Mode:None Group 1 - Event 1
100
74
87
55
Sampel
143
69
101
53
115
129
157
171
185
199
213
241
227