Pengaruh Pengeringan Terhadap Mutu Nasi Uduk Instan

D R Y IN G E F F E C T S O N IN S T A N T N A SI U D U K Q U A L IT Y
A n to n iu s K u rn ia an d B u d iatm an S atiaw ih ard ja

D ep artm en t o f F o o d S cien ce an d T ec h n o lo g y , F ac u lty o f A g ricu ltu ral T ech n o lo g y , B o g o r A g ricu ltu ral
U n iv ersity , IP B D arm ag a C am p u s, P O B O X 2 2 0 , B o g o r, W e st Ja v a, In d o n esia

P h o n e : + 6 2 8 1 3 1 6 3 3 2 5 2 7 , E - m a i l : a n t o n iu s k u r n ia @ y a h o o .c o m

A B STR A C T

R ice is th e sta p le fo o d fo r m o st o f In d o n esia n . T h e p r o d u ctio n o f rice in c rea se s e ve ry ye a r s. In 2 0 1 0 ,
t h e p r o d u c t i o n o f r i c e w a s a b o u t 6 5 ,9 8 b i l l i o n t o n ,w h i l e c o n s u m t i o n o f r i c e i s 1 3 9 ,5 k g / c a p i t a l / y e a r . B a s e d o n
th ese d a ta , th e d evelo p m e n t o f rice p r o d u ct is a p o ten tia l m a rket. N o w a d a y s m a n y p eo p le d o n o t h a v e m u ch tim e
to p r ep a re th eir fo o d . In sta n t fo o d is co m m o n ly ch o o se d b y th e m o d er n p eo p le . Q u ic k c o o kin g rice m eth o d s
h a ve b ee n co m m o n ly u se d sin c e 1 9 7 0 , b u t th eir p ro d u ct s a re n o t p o p u la r in In d o n e sia . T h e p u rp o s e o f th is
res ea rch is to p ro d u c e a q u ic k co o kin g ric e w ith sp ecia l ta ste n a tive to W e st S u m a te ra e, ca lled “ n a si u d u k ” .
T h e p re p a ra tio n in v o lve s s o a kin g , c o o kin g (g ela tin izin g ) a n d d ryin g u sin g flu id ize d b ed d ry er.T h is re se a rc h w a s
fo cu s ed o n to fin d o u t th e o p tim u m

d ryin g c o n d itio n s o r tr ea tm en t to p ro d u ce th e g o o d q u a lity o f q u ic k c o o kin g


r i c e . T h i s r e s e a r c h u s e d t h r e e d i f f e r e n t d r y i n g t r e a t m e n t s , n a m e l y A ,B , a n d C
co m b in a tio n

of

tim e

and

tem p e ra tu r e

h isto r y . It

w as

fo u n d

th a t

the


trea tm e n t w h ich w e re b a se d o n

o p tim u m

of

d ryin g

m eth o d

w as

th e

A

tra tm en t. In th e A tre a tm en t, th e ric e w a s fr ee zed fo r 2 4 h o u rs a t -2 0 ° C . A fter th a t, ric e w a s d ried fo r 3 0 m in u te s
a t ro o m tem p e ra tu r e a n d th en in cr ea sed th e tem p era tu re stra rt fro m


4 0°C , 60°C , and 80°C

fo r 1 0 m in u te s in

ea ch tem p e ra tu re. T h is m eth o d re su lted in a g o o d a c cep ta n ce f ro m p a n elists.

K eyw o rd s : q u ic k co o kin g ric e, d ryin g , flu id ized b ed d r ye r

ii

A N T O N IU S K U R N IA . F 2 4 0 7 0 0 9 5 .P en g a r u h P en g erin g a n T erh a d a p M u tu N a si U d u k In sta n . D i b aw ah
b im b in g an

D r .I r . B u d i a t m a n S a t i a w i h a r d j a , M .S c . 2 0 1 2 .

R IN G K A SA N

N asi ad ala h m ak an p o k o k b ag i se b ag ia n b e sar m as y arak at In d o n esi a. P ro d u k si b eras b erk em b an g teru s
setiap tah u n . P ad a 2 0 1 0 ,
tah u n .


B erd asarkan

bany ak

oran g

tid ak

d ata

p r o d u k s i b e r a s m e n c a p a i 6 5 , 9 8 j u t a t o n . K o n s u m s i b e r a s a d a l a h 1 3 9 ,5 k g / k a p i t a /
terseb u t,

m em ilik i

pen gem b ang an

w ak tu


cukup

bera s

u n tu k

da pat

m en y ia p k a n

m erupa ka n

pasar

m ak ana n

m ereka.

yan g


m e n j a n j i k a n .S a a t

Pro duk

in sta n

in i

um um ny a

sem a k in b an y ak d ig em ari u n tu k d ik o n s u m si. P ro s es p e n g o la h an n asi in stan m u lai d ik em b an g k an p ad a tah u n
1 9 7 0 , n am u n p ro d u k terseb u t tid ak d ip asark an d i In d o n esia.
T u ju an

d alam

p en elitian

k ali


in i

ad ala h

u n tu k

m e n g h asilk an

produ k

n asi

in sta n ,

d eng an

bum b u

trad isio n al y an g b eras al d ari S u m atra B arat, y an g d ise b u t n a si u d u k . P ersiap an p ro d u k n a si u d u k m elip u ti tah ap
p eren d am an , p em as ak a n , p em b e k u an , d an p en g erin g a n m e n g g u n a k an flu id ized b ed d r yer .

F o k u s p a d a p en elitian in i u n tu k m e n cari k o n d isi p en g erin g an y an g o p tim u m
yang

b aik . P en elitian k ali in i m en g g u n a k an

tig a p erlak u a n p en g erin g an

yang

u n tu k m e n g h asilk an p ro su k

b erb e d a, y aitu A , B , d an

m eru p ak an k o m b in a si d ari w ak tu d an su h u y a n g tep at. M e to d e p en g erin g an y an g o p tim u m
ad alah

m eto d e p en g erin g an A . K o n d isi p e n g erin g an A

m en it p ertam a m en g g u n ak an
p ad a su h u 4 0 ° C

60°C

ad ala h n asi d ik erin g k an

pada

d alam

C

i

p e n elitian in i

su h u ru an g s elam a

30

flu id ized b e d d ry er d en g an sp ee d b lo w er p ad a lev el 9 , selan ju tn y a d ik erin g k an


selam a 1 0 m en it d e n g a n s p ee d b lo w er d itu ru n k an p ad a lev el 7 , lalu s u h u d in aik k an m en jad i

s elam a 1 0 m en it m en g g u n ak a n b lo w er p ad a s p ee d 7 , d alam

1 0 m en it terak h ir su h u d in aik k a n m en jad i

8 0 ° C d en g an sp eed b lo w er lev el 7 . M eto d e p e n g erin g a n A m e n g h asilk an p en erim aan y an g p alin g b aik d ian tara
p erlak u a n lain n y a.

iii

I.

1 .1

PE N D A H U L U A N

L a ta r B e la k a n g
B eras ( O ry za sa tiva ) m eru p ak a n jen is serealia y an g d ijad ik a n m ak an a n p o k o k b a g i p en d u d u k


In d o n e sia.

B erd asark an

A n gka

R am alan

(A R A M )

III-2010

yan g

d ik elu ark an

o le h

B PS

d ik etah u i

b a h w a p r o d u k s i p a d i d i I n d o n e s i a s e b e s a r 6 5 ,9 8 j u t a t o n g a b a h k e r i n g g i l i n g ( G K G ) , n a i k 1 ,5 8 j u t a t o n
( 2 ,4 6 p e r s e n ) d i b a n d i n g p r o d u k s i t a h u n 2 0 0 9

s e b e s a r 6 4 ,4 0 j u t a t o n

y an g tin g g i d iim b an g i d en g a n tin g k at k o n su m si n a si d alam

G K G . K ap a sitas p ro d u k si b era s

n eg eri y an g tin g g i. T in g k at k o n s u m si n asi

d i I n d o n e s i a a d a l a h 1 3 9 ,5 k g / k a p i t a / t a h u n p a d a 2 0 0 9 . T i n g g i n y a k o n s u m s i n a s i d i I n d o n e s i a m e m b u a t
beras

m erupak an

k o m o d ita s

yang

san g at

b erp elu an g

u n tu k

d iek sp lo tiasi

leb ih

la n ju t

d alam

p en g elo laan n y a.
P en g o lah a n

bera s

sa at

in i

um um nya

d io la h

m en jad i

n asi

atau p u n

b eras.

P en g o lah an

bera s

trad isio n al u m u m n y a m em b u tu h k an w ak tu s ek itar 3 0 m e n it. W ak tu terseb u t m eru p a k an w ak tu u n tu k
m en an ak b era s h in g g a m atan g , jik a d itam b ah k an d en g an w ak tu p ersiap an n y a m ak a d ib u tu h k an w ak tu
sek itar

1

jam . T ah ap

p em a sak an

n asi

yan g

p a n jan g

m em b uat

p em a sak an n a si y a n g leb ih p rak tis d en g an m en g g u n a k an
m u d ah d an p ra k tis d alam

s eb a g ian

b esar

orang

rice co o k er. P e n g g u n a an

m em ilih

cara

rice c o o k er leb ih

p em as ak an n a si, m es k ip u n d em ik ian m a sih p erlu cara p em asa k an y an g leb ih

p rak tis d a n sia p d is an tap .
K ece nderun ga n

yang

b erkem b ang

d alam

m a sy a k arat

m od ern

sa at

in i

ad alah

m en g o n su m si

m ak an an in sta n y a n g d a p at d en g a n m u d a h d isiap k an d an d is an tap . T u n tu tan efesien si w ak tu , m em b u at
k o n s u m en u n tu k m em ilih m ak an a n in sta n s eb a g ai p o l a k o n su m si s eh ari -h ari.
P ro d u k m a k an an in stan y an g saat in i b ered ar d i p as aran san g at jaran g y an g m en g g u n ak an b era s
seb ag ai

bahan

dasarnya .

M aka nan

in stan

yang

s elam a

in i

d iju al

m em ilik i

k esan

m en g e n y a n g k an k o n su m en , ta n p a m em b erik an k ep u as an b ag i k o n su m e n . Istilah “ b elu m
b elu m

han ya

u n tu k

m a k an , k alau

m ak an n asi” m em b u at m ak an an in sta n terseb u t h an y a m en ah an lap ar k o n s u m en , d a n k o n su m en

tetap m eras a “ b elu m m a k an ”.
P en g em b a n g a n tek n o lo g i n a si siap s aji su d ah lam a d ik em b a n g k an , n am u n u n tu k p ela k sa n a an n y a
d alam

p as ar In d o n e sia m asih su lit u n tu k m ereb u t h ati k o n su m en . P ro d u k n a si in stan y an g p ern ah a d a

um um ny a
karena

d isajik an

k arak teristik

d alam
n asi

b e n tu k

goreng

n a si

in sta n

g o ren g . N asi
tid ak

sam a

goren g

s ep erti

in stan

n asi

terse b u t

goreng

y ang

su lit

m enem bu s

um um ny a

p a sar,

d ik o n s u m si

m asy arak at.
H asil

o lah an

lain

dari

beras

ad ala h

n asi

u d u k , selam a

in i

n asi

uduk

telah

d ik en al

lu as

o leh

m asy arak at k h u su sn y a d i p u lau Jaw a. M en g k o n su m si n asi u d u k b u k a n lah h al y a n g asin g b ag i se b a g ian
m asy arak at. N a si u d u k in sta n m u n g k in d ap at d iterim a o leh k o n s u m en , seh in g g a d ap at d ik em b a n g k an
leb ih lan ju t d alam

1 .2

sk ala y an g le b ih b esar.

T u ju a n P e n e litia n
P en elitian in i m em p u n y ai tu ju a n u n tu k m en g etah u i p en g aru h p en g erin g a n p ro d u k n a si u d u k

in stan sia p s aji d en g an m en g g u n ak an p en g erin g flu id ized b e d d rye r.

1

II.

2 .1

T IN J A U A N P U S T A K A

S e k ila s T e n ta n g N a s i I n sta n
N asi in stan

ad ala h

d en g an c ara p ersiap an y an g

n asi ce p at m a sak

y an g d a p at d isia p k a n d alam

sed erh an a. N a si in stan m em ilik i

w ak tu 3

sam p ai 5 m e n it

c i ri k h a s d e n g a n b u t i r b e r a sn y a y a n g

d ib u at p o ro u s. S tru k tu r y an g leb ih p o ro u s a k an m em p erc ep at air p an as y an g m asu k k e d al am n y a s aat
d ireh id rasi. S etelah d im a sa k , p ro d u k h aru s se su ai d en g an n asi b ias a d alam

h al rasa, aro m a, d a n tek stu r

(R ew th o n g ,et al, 2 0 1 0 ) . J en is b eras y an g d ig u n ak a n u m u m n y a a d alah b eras d en g an b u lir p an jan g , atau
beras

lo n g

g ra in .

B era s

den gan

b u lir

p an jan g

um um ny a

m em ilik i

b en tu k

d ik erin g k a n k em b ali, k are n a d ap at m en y eru p ai b en tu k b u tir b eras s eb elu m

y ang

leb ih

b aik

saat

d ik erin g k an

T ab el 1 . N ilai N u trisi B eras

Z at G izi

K adar

K arb o h id rat

79%

L em ak

0 .6 6 %

P ro tein

7 .1 3 %

A ir

12%

S u m b er : N u trisi D ata U S D A ,2 0 1 2

N asi in stan d ib u at d e n g a n cara p erlak u an p em as ak a n aw al d an g elatin isasi d en g an m e n g g u n a k an air,
uap

ata u

ga bun gan

k ed uan ya.

G elatin is asi

p ati

d ise b ab k an

o le h

pem ben gka ka n

g ran u la

ak ib at

p em an as an y an g m en y eb a b k a n terjad in y a p en ek a n an g ran u la satu d an la in n y a. P em b en g k ak an g ra n u la
b ersifat reve rsib le, n am u n k etik a m elew ati su h u 6 8 -7 8 ⁰ C

p em b en g k ak an g ran u la b ersifat irre ver sib le

y a n g d i s e b u t g e l a t i n s a s i . S u h u t e r s e b u t d i s e b u t s u h u g e l a t i n i s a s i ( F e n n e m a ,1 9 8 5 ) .
K isaran su h u y an g m e n y eb a b k a n 9 0 % b u tir p ati d alam

air p an a s m em b e n g k ak d an tid ak d a p at

k em b ali p a d a b en tu k as aln y a d ise b u t B irefrin g en t E n d P o in t T em p era tu re atau d is eb u t B E P T . K is aran
beras y ang

ad a d ip a saran m em p u n y ai B E P T

ren d ah (5 5 -6 9 ⁰ C ), m ed iu m

(7 0 -7 4 ⁰ C ), d an tin g g i (7 5 -

7 7 ⁰ C ) ( J u l i a n o ,1 9 7 2 ) . G e l a t i n s a s i p a t i a k a n m e n y e b a b k a n p e r m u k a a n b u t i r b e r a s m e n j a d i r e t a k . B i l a
d im asa k ,

p eng em ba ga nny a

tid ak

se b e sar

p eng em ba gan

p ati

asal.

T ertah a n n y a

p en gem b ang an

in i

d iseb ab k an p em b atas o leh k o m p o n en n o n p ati. G el atin sasi g ran u la p ati m eru p ak an sala h s atu la n g k ah
k u n ci d alam

p em b u ata n n asi cep at s aji. G elatin sa si p ati b ersifat irr eve rsib el, d an m eru p a k an h al y a n g

p en tin g d alam

p ro ses reh id ra si b eras in sta n k erin g y an g terg elatin isasi sem p u rn a u n tu k d isiap k an d an

d ik o n s u m si (W irak artak u s u m ah y a n g d ia cu o leh F ird h au s 2 0 0 3 ) .
N asi in stan d ap at d ib e d ak an m e n jad i b eb erap a tip e b erd a sark a n tin g k at k ad ar air, su h u , w ak tu
p e m a s a k a n a w a l , d a n k o n d i s i p e n g e r i n g a n ( L u h , e t a l ,1 9 8 0 ) . B e r d a s a r k a n p e r l a k u a n i n i d a p a t d i h a s i l k a n
b eb era p a je n is n asi in sta n , y aitu :
1.

U n d e r co o k ed rice y an g m em b u tu h k an w ak tu 1 0 -1 5 m e n it w ak tu p en y ajian

2.

T a ke rice m em b u tu h k an w ak tu 5 m en it u n tu k p ersia p a n

3.

M in u te rice m em b u tu h k a n 1 -2 m en it u n tu k p ersia p an

4.

R ea d y to e a t b r ea kfa st ce re a l d ap at lan g su n g d is a n tap

S elam a
d ip aten k an (L u h

em p at

p u lu h

tah u n

terak h ir

bany ak

m eto d e

p em b u atan

b eras

in sta n

e t a l ,1 9 8 0 ) . M e t o d e y a n g b e r k e m b a n g d a p a t d i k e l o m p o k k a n d a l a m

yan g

telah

1 0 je n is m eto d e

p em b u atan . M eto d e t erseb u t terb ag i d alam :
1.

B eras m u la-m u la d iren d am

d alam

air sam p ai k ad ar air m en jad i 3 0 % . K em u d ian d im as ak

deng an

kadar

air

air

pan as

sam p ai

50 -60

%

den ga n

atau

tan p a

m en ggu nak an

u ap.

K em u d ian p ere b u san atau p e n g u k u san d iteru sk an sam p ai k ad ar airn y a m e n jad i 6 0 -7 0 %
d an k em u d ian d ik erin g k a n d e n g a n h ati-h ati sam p ai k a d ar air 8 -1 4 %
stru k tu rn y a

b erp o ri.

M o d ifik asi

yan g

d ilak u k a n

terh a d ap

c ara

in i

d en g a n m en jag a ag ar
an tara

lain

d eng an

2

p e r l a k u a n p a n a s k e r i n g p e n d a h u l u a n u n t u k m e m b u a t b e r p o r i - p o r i b u t i r - b u ti r b e r a s s e b e l u m
d im asa k d a n d ik erin g k an .
2.

B eras

d iren d am ,

d ireb u s,

d ik u k u s

deng an

tek a n a n

u n tu k

m em bu at

b u tir -b u tir

beras

terg elatin isasi, d k erin g k a n d en g an su h u y a n g re n d a h u n tu k m en g h asilk an b u tir -b u tir b eras
y an g a g ak b erat d an m en g k ilat, k em u d ian d ib eri p erlak u a n d e n g a n p en g em b an g an p a d a
tek an a n d an su h u tin g g i u n tu k m em p ero leh stru k tu r b erp o ri -p o ri y an g d iin g in k an .
3.

B eras d ip re g elatisa si, d ig ilin g atau d itek a n u n tu k m em p ero leh b u tiran y an g ag ak g ep en g
dan

k em u d ian d ik erin g k a n u n tu k m em p ero leh

b u tiran b eras

den gan

k a d ar air 1 2 %

d an

m en g k ilat.
B e r a s d i b e r i p e r l a k u a n d e n g a n u d a r a p a n a s y a n g m e n g a l i r c e p a t p a d a s u h u 6 5 ,6 – 3 1 5 ,6 ˚ C

4.

u n tu k

m em bu at

proses

d ek strin asi

p ati

d alam

b eras,

m em bu at

berp ori -pori

atau

m en g em b an g k a n b u tiran b eras .
5.

B eras d iaro n , k em u d ia n d ib ek u k an , d ith a w in g d an d ik erin g k an .

6.

M eto d e G u n P u ffin g

y ang m erupa kan

k o m b in asi d ari p erlak u a n -p erlak u an p en d ah u lu an

terh ad ap b eras d en g a n p en g g u n aa n s u h u d an te k a n an tin g g i, d iik u ti d en g an p e n g elu aran
sec ara c ep at k e d alam ru an g a n y a n g te k an an n y a le b ih ren d ah .
7.

N asi m a sak d en g a n p e n g erin g an b ek u .

8.

P erlak u a n ata u p em b erian b ah an k im ia.

9.

K o m b in asi 2 ata u leb ih d ari m eto d e d iatas

1 0 .M e t o d e l a i n .

M en u ru t H u b eis (1 9 8 4 ), b eras in stan y a n g d in ilai p alin g b aik m elalu i ta h ap an se b ag ai b erik u t :
perend am an

b eras

dengan

laru tan

N a2H P O

0 ,2

4

%

selam a

18-19

jam

(pH

5 ,2 ) ;

p en etralan

deng an

N a O H 1 N ( p H 7 ,0 - 7 ,3 ) ; p e m a s a k a n s e l a m a 7 m e n i t ; p e n g u k u s a n 1 0 m e n i t ; p e n c u c i a n d a n p e n g e r i n g a n .
B eras

in stan

yang

d ih a silk an

m elalu i

p ro ses

terse b u t

d ap at

d iu b ah

m en ja d i

n a si

m elalu i

p ro se s

r e h i d r a s i . K a d a r a i r b e r a s i n s t a n s e b a g a i p r o d u k a k h i r d a p a t b e r k i s a r 9 - 1 2 ,5 % y a i t u s u a t u k e a d a a n a m a n
sim p an d im a n a n ilai k ad ar air terseb u t d alam

k ead aa n setim b a n g d e n g an k o n d isi lin g k u n g a n n o rm al.

P ati y an g telah m en g alam i g elatin isasi d ap at d ik erin g k an , tetap i m o le k u l-m o lek u l ters eb u t tid ak d ap at
k em b ali lag i k e sifat-sifat asaln y a se b elu m
m en y era p air d alam
air

k em b ali

g elatin isa si. B a h an y an g telah k erin g terseb u t m a sih m am p u

ju m lah y an g b esar. S ifat in ilah y an g d ig u n a k an ag ar b era s in sta n d ap at m en y erap

den gan

m u da h,

y aitu

d eng an

m e ngg una kan

p ati

yan g

telah

m e n g alam i

g elatin isasi

(W in arn o , 1 9 8 4 ).

2 .2 .

T a h a p P em b u a ta n N a si In sta n
T aha p

p em b u atan

p eren d am an d alam
d alam

air

d in g in

n asi

p eren d am an d alam
4

0 .2 %

dap at

d ilak u k an

dengan

be berap a

cara,

d ia n taran y a

ad alah

laru tan k im ia, p em b ek u an , d an p e n g erin g a n . P ad a d a sarn y a p ati y a n g d im as u k k an
aka n

m en yerap

d iserap terb atas d an h a n y a 2 6 %

N a2 H P O

in sta n

air

dan

aka n

terjad i

peng em ba ng an

p ati. T eta p i

ju m lah

air

yang

d ari b erat aw al. U n tu k m en in g k atk an d a y a s erap air p erlu d ilak u k an

laru tan k im ia. M en u ru t H u b eis (1 9 8 4 ), p ere n d am an d ap at d ilak u k an d alam

selam a 1 8 jam . G aram

n atriu m

laru tan

fo sfat ak an m en g a k ib atk a n stru k tu r fisik b eras p as ca

tan ak le b ih p o ro u s, h al in i m en y eb a b k a n p en y erap an

air ak an

leb ih

cep at pa da

w a k tu

peren dam an

m au p u n reh id rasi. P en am b ah an fo sfat s eb a g ai se n y a w a y an g m e n g io n p ad a p ro d u k y a n g b erasal d ari
p ati ak an m en y eb ab k an g ran u l a p ati tah an terh ad a p retro g rad asi selam a p en d in g in an d an p e n in g k atan
su h u s etelah p en d in g in an .
T ah a p p em b u at an b erik u tn y a ad ala h p em b e k u a n . P ro ses p em b ek u an d a n p e n y im p a n an b e k u
ak an m e n in g k atk an p en g em b a n g a n m o le k u l p ati. P em b e k u a n a k a n m ele p a sk a n air y an g terd a p at d alam
sistem

g el.

P ro se s

in i

d ilak u k a n

u n tu k

m en g h a silk an

sifat

p o ro sitas

y ang

tin g g i

s eh in g g a

w ak tu

reh id rasi m en jad i sem ak in sin g k at.
N asi in stan d a p at m en y erap air p an as d en g an ce p at se h in g a d ap at d ik o n s u m si d alam

b ebera pa

m en it. N asi in stan d ap at terb en tu k b ila p o ri -p o ri b eras terb u k a leb ar s eh in g g a m em u d a h k a n reh id rasi
dan

d ip ero le h

lam b at s eb elu m

w ak tu

reh id rasi

y an g

sin g k at, cara

n asi d ik erin g k a n . P em b ek u an

yang

dap at

d ilak u k a n

ad alah

den ga n

pem b eku an

lam b at y a n g m en g h a silk an k ristal es y an g b esar ak an

3

m em b u at ro n g g a p o ri y an g b e sar u n tu k d ih id rasi d en g an c ep at, seh in g g a u k u ra n b era s m e n jad i leb ih
besar.
P em be kua n p ada

su h u

0

-20

C

selam a

20

jam

m en g h a silk an

stru k tu r

k ristal es y an g

b e sar,

p ro se s in i m em e cah k an stru k tu r k o lo id p ati d a n m e n g h asilk a n stru k tu r k ern el y a n g p o ro u s (R ew th o n g
et al, 2 0 1 0 ) . P ro d u k y an g d ih a silk an d ap at d e n g a n c ep at m e n y era p a ir p a d a p em a sa k an k em b ali.
T aha pan

s elan ju tn y a

dari

p em b u ata n

n asi

in stan

ad alah

p e n g erin g an .

P e n g erin g an

ad alah

m eto d e u n tu k m en g aw etk an b a h an p an g an . T u ju an p en g erin g an a d alah m e n g u ra n g i k ad ar air b ah an
sam p ai

m endap at

b io lo g is

dan

kadar

k im ia

air

terten tu

se b elu m

b aha n

yang

dap at

d io lah

m engh am bat

ata u

laju

d im an fa atk an .

k eru sa k an

b aha n

P en guran gan

ak ib at

kad ar

air,

ak tiv itas
m em buat

k o m p o n en zat g izi p ad a k o n s en trasi y an g le b ih tin g g i.
P en g erin g an

adalah

su atu

p eristiw a

p erp in d ah an

m as sa

dan

energi

yan g

terjad i

d alam

p em isa h an air ata u k elem b a b an d ari su atu b ah a n sam p ai b atas k a n d u n g a n air y an g d iten tu k an d en g an
m engg una kan

udara

seb ag ai

flu id a

su m b er

pa nas

dan

p en erim a

uap

c airan

(T rey b al,

1 981).

P en g erin g an m a k an an m em ilik i d u a tu ju an u tam a. T u ju a n p e rtam a ad alah s eb a g ai saran a p en g aw etan
m akan an.
b ertah an

M ik ro o rg a n ism e
h id u p

p ada

y ang

m e n g a k ib atk a n

lin g k u n g a n

d eng an

k eru sak an

kad ar

air

yang

m a kan an
re nda h.

tid ak

S elain

d apat
itu ,

berk em ba ng

b any ak

en zim

d an
yang

m en g a k ib atk a n p eru b ah an k im ia p ad a m ak a n an tid a k d ap at b erfu n g si tan p a k eh ad iran air (G ean k o p lis,
1 9 9 5 ). T u ju an
yang

telah

ked ua

ad ala h u n tu k m em in im alk a n b ia y a d i strib u si b ah an m a k an an

d ik erin g k a n

ak an

m em ilik i

berat

yang

leb ih

rend ah

dan

ukura n

karen a m ak an an

yan g

leb ih

k ecil .

P en g erin g an m e ru p a k a n o p erasi y an g ru m it y an g m elip u ti p erp in d ah a n p an a s d an m as sa se cara tran sien
serta b eb era p a laju p ro se s, sep erti tran sfo rm asi fisik ata u

k im ia, y an g d ap at m en y eb ab k an p eru b ah an

m u tu h a sil m au p u n m ek an ism e p erp in d ah an p an as d an m as sa. P eru b ah a n fis ik y a n g m u n g k in terjad i
m elip u ti : p en g k eru tan , p en g g u m p u lan , k ristalisasi, tran sisi g elas. p a d a b eb erap a k a su s, d ap at terjad i
reak si

k im ia

atau

b io k im ia

yan g

d iin g in k a n

ata u

tid ak

d iin g in k an ,

yang

m en yeb abk an

perub ah an

w arn a, tek stu r, aro m a atau sifat lai n p ad atan y an g d ih asilk a n . P e n g erin g a n terjad i m elalu i p en g u ap an
cairan d en g an p em b erian p a n a s k e b a h an u m p an b as ah
P ad a u m u m n y a zat p ad at selalu m en g an d u n g se d ik it frak si air seb a g ai air terik at. Z at p ad at
y an g ak a n d ik erin g k an b ias an y a terd ap at d alam

b en tu k serp ih (flak e), b ijian (g ran u le), k ristal (cry stal),

serb u k (p o w d er), lem p e n g (sla b ), atau lem b aran
berbed a

satu

sam a lain . Z at c air y an g

a kan

sin am b u n g (co n tin o u s sh eet) d en g a n sifat -sifat y an g

d iu ap k an m u n g k in terd ap at p ad a

sep erti p ad a k ristal; d ap at p u la s elu ru h zat c air terd ap at d i d alam

perm u kaa n z at p adat

zat p ad at sep erti p ad a p em is ah an

p elaru t d ari lem b ara n p o lim er; atau d ap at p u la seb ag ian z at cair s eb a g ian d i lu ar d an seb ag ian d i d alam .
U m p an p en g erin g m u n g k in b eru p a zat cair d i m an a zat p ad at m ela y an g s eb ag ai p artik el, atau d ap at
p u la b erb en tu k laru tan . H a sil p en g erin g an a d a y an g tah a n terh ad ap
b erad a d alam
su h u

ren dah

lin g k u n g a n y an g sa n g at p a n a s, ad a p u la
ata u

p ad at d i d alam

sed an g . P erb ed aan

p en g erin g

p en a n g a n an m ek a n ik k a sar d an

y an g m em erlu k an p en a n g a n an

teru tam a

terletak

d alam

hal

cara

h ati-h ati p ad a

m em in d ah k an

zat

zo n a p en g erin g d a n d alam p ro s es p erp in d ah a n k alo rn y a.

P ro se s p e n g erin g an m e n g h asilk a n stru k tu r p o ro u s y an g ak an m em u d ah k an air u n tu k d ap at
m eresa p k e

d alam

b eras

sa at reh i d rasi. S u h u

o p tim u m

p e n g erin g a n n asi in sta n

m en u ru t R ew th o n g ,

2 0 1 0 a d alah 8 0 ° C . S em e n tara m en u ru t Ja d in g et al, 2 0 1 1 , su h u u n tu k m en g erin g k an g ran u la b erk isar
an tara 6 0 – 7 0 ° C .

2 .3 .

F lu id iz e d B e d D r y e r
T ek n o lo g i F lu id ized b ed d r yer m eru p a k an sala h satu altern atif p ilih an tek n o lo g i p en g erin g a n ,

karena

te k n o lo g i

k o n v en sio n al
produk

de ng an

kom pak,

in i

lain n y a,

m em ilik i

p erp in d ah an

se h in g g a

k ap a sitas

kan dun gan

dengan

in v e stasi

air

yan g

aw al

serag am

relatif

pan as

dan

p en g erin g an

m as sa

da pat

le b ih
leb ih

b aik

b e sar

(S ireg ar, 2 0 0 6 ). T ek n o lo g i

rendah

dan

um um n ya

tek n o lo g i

dari
d an

flu id ized
in i

jen is

d ap at
bed

d ip ak ai

p e n g erin g an
m en g h a silk an
drye r
u n tu k

cuk up
prod uk

b erb en tu k g ra n u lar (M u ju m d ar A S d a n D ev a h a stin S , 2 0 0 3 ). P e n g erin g an m en g g u n ak a n flu id ized b ed
d ry er m em ilik i b eb erap a k eu n tu n g a n , d ia n taran y a :
a.

L aju p en g erin g an tin g g i, k aren a p er s en tu h an an tara p artik el d an u d ara y a n g terjad i sa n g at b aik

b.

L u as p erm u k aa n b a h a n y a n g b erse n tu h a n d en g an aliran u d ara le b ih b esar

c.

E fisien si p a n as tin g g i k are n a k o efisien laju p in d ah p an as d an p in d a h m a ss a m em b es ar

d an m en y eb a b k a n tin g g in y a laju p in d ah p a n a s d a n m a ss a.

4

d.

B iay a in v esta si d a n p em elih araan relatif leb ih ren d ah
P rin sip k erja p ad a alat flu id ized b ed d r ye r d en g an m en iu p k an u d ara p a n a s d ari b ag ian b aw ah

bed.

U dara

pa nas

terse b u t

a kan

m en arik

air

yan g

ada

pada

bah an

u n tu k

k elu ar, s eh in g g a

terjad i

b u b b lin g d a n m e n g a n g k at p ro d u k y an g ad a d iat as b ed . T in g k at b u b b lin g y an g terjad i terg a n tu n g p a d a
besaran

ud ara

yan g

d itu p k a n

( S i r e g a r ,2 0 0 6 ) .

P rin sip

flu id ized

k erja

bed

drye r

dap at

d ilih at

pada

G am bar 1

P lat p erfo rasi

U dara

U dara

U dara

U dara

U dara

U dara

1

2

3

4

5

6

P artik el d alam

p artik el m u lai

P artik el

flu id isasi

flu id isasi

tran sp o rt

k ead aa n d iam

terflu id isasi

terflu id isasi

terb aik

d alam

p n eu m atik

k o n d isi

pada ba han

b erleb ih an

k erin g

G am b ar 1 . P rin sip k erja flu id ized b ed d ry er

F lu id ized b ed d r yer terb ag i ata s b eb erap a b ag ia n , y aitu :
a. B lo w er
B lo w er b erfu n g si u n tu k m e n g h asilk a n aliran u d ata y a n g ak an d ig u n ak a n p ad a p ro s es flu id isasi.
K ip as ju g a b erfu n g si se b ag ai p e n g h em b u s u d ara p an a s k e d alam

ru ang

p en g erin g d an u n tu k

m en g a n g k at b a h an ag ar p ro se s flu id isa si terjad i.
b . E lem en P em an as
E lem en p em a n a s b erfu n g si u n tu k m em a n as k an u d ara h in g g a k elem b a b an relatif u d ara p en g erin g
tu ru n , d an

k alo r

y ang

d ih asilk a n

d ib aw a

o le h

aliran

ud ara

y ang

m elew ati

elem e n

pem ana s

seh in g g a p ro se s p en g u a p an air d ari d alam b ah an d ap at b erlan g su n g .
c. H oppe r
H opper

b erfu n g si se b ag ai tem p at m em asu k k an b ah a n y an g ak an d ik erin g k a n k eru an g p e n g erin g

d . T h er m o c o u p le
T h er m o c o p u le b erfu n g si se b ag ai p e n g u k u r tem p eratu r u d ara m asu k d an u d ara k elu ar.

P en g erin g an m en g g u n ak an F lu id ized b e d d ry er d a p at d ig u n a k an u n tu k m e n g erin g k an g ran u la.
P en g erin g an

m e ngg una kan

F lu id iz ed

b ed

d rye r

m am p u

m em p ertah an k an

k o m p o sisi

k im ia

dan

m e m p e r b a i k i s i f a t f i s i k o k i m i a p a t i s a g u k e r i n g ( J a d i n g e t a l ,2 0 1 1 ) . K e m a m p u a n u n t u k m e n g e r i n g k a n
g ran u la

in i

d iseb ab k an

kem am pu an

alat

u n tu k

m enc apai

p ro ses

flu id isa si

yang

o p tim al

seh in g g a

m am p u m e n c ap ai w ak tu p en g erin g an y a n g sin g k at.

5

a. G ran u la p ati b as ah

b . G ran u la p ati h asil

c. G ran u la

p ati

p en g erin g an

p en g erin g an

m en g g u n a k an F lu id ize d

k o n v en sio n al

h a sil

b ed d ry er
S u m b e r : J a d i n g e t a l ,2 0 1 1
G am b ar 2 . B en tu k g ran u la p ati

6

III.

3 .1

B A H A N D A N M E T O D E

B a h a n d a n A la t
B ah a n u tam a y an g d ig u n a k an d i d alam

p en elitian in i ad alah b eras s erta b u m b u n a si u d u k y a n g

m elip u ti sereh , d a u n jeru k , s an tan , d an g aram . B era s y a n g d ig u n a k an d alam
p era v arietas IR
ad alah

4 2 d an b eras p u l en v arietas IR

64

p e n elitian in i ad alah b era s

d en g an p erb an d in g a n 2 :1 . A lat y an g d ig u n ak an

f l u i d i z e d b e d d r y e r ,p a n c i , d a n d a n g , k o m p o r , t i m b a n g a n a n a l i t i k , g e l a s p e n g a d u k , t e r m o m e t e r ,

w a terb a th , g elas u k u r, c aw an

alu m u n iu m , g ela s p iala, d a n alat g ela s lain u n tu k

a n alisis p ro k sim at.

K o m p o si si b ah an m em b u at n a si u d u k d ap at d ilih at p ad a T ab el 2 .

T ab el 2 . K o m p o sisi b ah an n asi u d u k
B aha n

K o m p o s is i

B eras

500 g

A ir

600 m l

S an tan

20 m l

P en y ed a p (ro y co sa p i)

2 g

G aram

8 g

S ereh

10 g

D au n S alam

5 g

G a m b a r 3 .B a h a n m e m b u a t n a s i u d u k

S p esifik asi :
M odel N o. A P S . 6
S e r i a l N o .: A P S - B 1 4 2 6
E C t y p e - a p p r o v a l N o .: T 6 1 2 6
T e s t C e r t i f i c a t e N p .: T C 6 1 0 1
M F D B y : U W E C o ., L td .

G am b ar 4 . T im b an g an

S p esifik asi :
T y p e : F lu id B ed D ry er
M odel N o. M K II
S e r i a l N o .: F N D / 2 4 0 / 9 1 / 5 7 4 2
M ad e b y : A rm field
G am b ar 5 . F lu d ize d B ed D rye r

7

3 .2

M e t o d e P e n e l it i a n
M eto d e p en elitian y an g d ig u n a k an d alam p en elitian in i terd iri d ari p en elitian p en d ah u lu an d an

p en elitian u tam a . B erd a sark a n p en elitan terd ah u lu o l eh F ird h a u s ( 2 0 0 3 ), telah d iteliti ten tan g m eto d e
p en g erin g an n asi in stan b eru p a p en g aru h p ere n d am an d alam
perend am an

d alam

laru tan

k im ia,

m en g h asilk a n n asi in sta n y an g
N a2H P O

4

b aik .

m eto d e

pem asaka n

P a d a ta h ap

laru tan N atriu m
ju g a

p erlu

F o sfat. S elain p en g aru h

d ip erb aik i

d alam

p e n d a h u lu a n d ilak u k a n p eren d am an

k aitan n y a

d alam

laru tan

seb e sar 0 ,2 % s elam a 1 2 0 m en it. P a d a p em a sa k an d ig u n ak an reto rt u n tu k m em a sak n a si u d u k

(G am b ar 6 ). P ad a tah a p p e n d a h u lu a n ju g a

d ilak u k an p em a sak an m e n g g u n a k an m eto d e

aron k uku s .

P em as ak an n asi u d u k m en g g u n ak an reto rt d en g an m en g g u n ak an s u h u 1 2 1 ˚C , d e n g a n 3 ren ta n g w ak tu
yang

b erb e d a y aitu 5 , 1 0 , d an 1 5 m en it. S etelah b eras m ata n g k em u d ia n d ico b a u n tu k d i b ek u k a n .

P em b e k u a n b eras d ila k u k an s elam a
d ib u at p a d a tah ap

p en d ah u lu an

2 4 jam

pad a suhu

ad ala h 6 0 ° C

dan

-20˚C

p a d a freez er. S u h u p en g erin g an

8 0 ° C . P en g am atan

yang

y an g d ilak u k an terh ad a p tah ap

p en d ah u lu an ad ala h p en g am atan se cara v isu al h a sil p en g erin g an .

B eras

P en c u cian

P eren d am an selam a 1 2 0 m e n it + N a 2H P O

4

0 ,2 %

P em as ak an d alam

P em as ak an d alam

P em as ak an d alam

reto rt selam a 5 m en it +

reto rt selam a 1 0 m en it

reto rt selam a 1 5 m en it

penam bah an bum b u

+ pe nam b aha n b um bu

+ pe nam b aha n b um bu

P en g aro n a n s elam a 1 0
m en it + b u m b u

P en g u k u sa n s elam a
3 0 m e n it

P em b e k u a n s elam a 2 4 jam

P en g erin g an

P en g erin g an

su h u 6 0 ° C

su h u 8 0 ° C

N asi U d u k

In sta n

G am b ar 6 . S k em a P em b u atan N asi U d u k In sta n tah ap p en elitian p en d ah u lu an

S etelah m em p ero leh d ata p en g am atan h asil p e n elitian p e n d a h u lu a n (lih at p ad a B ab H asil d an
P em b a h a san ), d ilak u k a n p e n elitian u tam a s ep erti terlih at p ad a G am b ar 7 . P ro s ed u r in i b erfo k u s p a d a
p erlak u a n p en g erin g an y an g d id u g a ak an p alin g b erp en g aru h terh ad a p p ro d u k

8

B eras

P en c u cian

P eren d am an selam a 1 2 0 m e n it + N a 2H P O

4

0 ,2 %

P en g aro n a n s elam a 1 0 m e n it + p e n am b ah an b u m b u

P en g u k u sa n s elam a 3 0 m e n it

P em b e k u a n ( free zin g ) s elam a 2 4 jam

P erlak u a n p en g erin g an A

P erlak u a n p en g erin g an

N asi U d u k

G am bar

A

yang

P erlak u a n p en g erin g an C

In sta n

7 . S k em a P em b u atan N asi U d u k In stan tah ap p en elitian u tam a

P erlak u a n p en g erin g an
p en g erin g an

B

d im ak su d

y a n g d ig u n ak an p ad a p en elitian u tam a
ad ala h

n a si

yang

tela h

y aitu A , B

d ib ek u k an , d ik erin g k a n

d an C . P erlak u an

pad a

F lu id ized

B ed

D rye r p ad a su h u k am ar d an k e cep atan b lo w er d is et p ad a lev el 9 selam a 3 0 m en it p ertam a. S elan ju tn y a
su h u d in aik k an m en ja d i 4 0 ˚C

selam a

1 0 m en it d a n k ece p atan

b lo w er d itu ru n k an

p a d a le v el 7 . S u h u

b lo w er selan ju tn y a d in aik k an m e n jad i 6 0 ˚C selam a 1 0 m en it d an k ec ep ata n b lo w e r tetap
P ad a 1 0 m en it terk ah ir su h u d in aik k a n m e n jad i 8 0 ˚C d en g an k e cep atan b lo w e r
P erlak u a n p e n g erin g a n B

p ad a lev el 7 .

tetap p a d a lev el 7 .

p a d a p en elitian in i d ilak u k a n d en g a n p erlak u an

p en g erin g an

n asi

y an g telah d ib e k u k an p ad a F lu id iz ed B ed D r ye r d en g an su h u k am ar d a n lev el k e ce p atan b lo w er p a d a
lev el 9 selam a 3 0 m e n it. S etela h itu F lu id iz ed B ed D ry er d in aik k an m en ja d i 6 0 ˚C
d itu ru n k an m en jad i lev el 7
p en g erin g an
k ec ep ata n

n asi

b lo w er

selam a

3 0 m en it. P erlak u an

yan g

telah

d ib ek u k an

pad a

lev el

9

selam a

p ada
30

F lu id iz ed

p en g erin g a n C
B ed

m en it. K em u d ian

d alam

D rye r

den gan

su h u

F lu id iz ed

d a n lev el b lo w e r

p en elitian in i ad alah

suhu

k am ar

dan

B ed

D ry er

d in aik k an

lev el

m en jad i 8 0 ˚C serta k ece p ata n b lo w e r d itu ru n k an p a d a lev el 7 selam a 3 0 m en it.
P ro se s reh id rasi n a si u d u k in stan d ilak u k an d en g an m e n aru h b eras d alam
gram

d a n air d en g an su h u 9 0 ° C

g ela s se b an y ak 2 0

se b a n y a k 1 5 0 m l d an d iam k an selam a 5 m e n it (G am b ar 9 ). A n alisis

y an g d ilak u k a n ad al ah rasio reh id rasi, p o ro sitas, o rg a n o lep tik serta p ro k sim at u n tu k h a sil terb aik . U ji
o rg an o le p tik terh ad ap n asi in sta n k erin g y an g tela h d ireh id rasi d e n g a n m en g g u n ak an u ji h ed o n ik sk ala

9

tu ju h . A n alisis o rg a n o lep tik in i m en g g u n ak a n u ji ratin g h ed o n ik m en g g u n ak an 3 0 p an elis y an g tid ak
terlatih . T ah ap p ertam a an alisis m en g g u n ak a n A N O V A u n tu k m en g eta h u i p en g aru h tah ap a n p erlak u an
p en g erin g an

pada

taraf

sig n ifik an si

5

% .

S etela h

d ik eta h u i

terd a p at

p erbed aan

sig n ifik an

d ian tara

k etig a p erlak u an , k em u d ian d ilak u k an u ji lan ju t y an g b eru p a u ji D u n can u n tu k m en g et ah u i sam p el d ari
p erlak u a n m a n a y a n g b erb e d a d ari tiap p erlak u a n . S etelah d id a p atk a n n asi in stan d e n g a n n ilai u ji ratin g
h ed o n ik y an g tertin g g i, m ak a d ilan ju tk an d e n g a n a n alisis p ro k sim at terh ad ap n asi in stan ters eb u t.

2 0 g N asi u d u k in stan

1 5 0 m l air d e n g a n s u h u
90 °C

T aru h d alam g elas tertu tu p d an tu n g g u s am p ai 5 m en it

N asi u d u k in stan siap d i san ta p

G am b ar 8 . S k em a reh id ra si n a si u d u k in sta n

3 .3

A n a lisis P r o d u k

3 .3 .1 .

R a sio R e h id ra si
C o n to h

seb any ak

10

gram

d im asu k k a n

ke

d alam

g ela s

p iala,

d itam b ah

dengan

15 0

m l

o

aq u a d e s. C o n to h k em u d ia n d im as u k k an k e w a te rb a th b ersu h u 8 0 C selam a 1 0 m en it. H asil p em as ak an
d ib iark an sam p ai m e n ca p ai su h u k am ar, k em u d ian d itim b an g b erat n asi y an g tela h d ireh id ra si s etelah
d i t i ri sk a n . R a si o r e h i d r a si ( R r ) d i h i t u n g d e n g a n r u m u s :

B erat n asi in stan setelah reh id rasi (g )
R r

=
B erat co n to h n a si in sta n (g )

3 .3 .2 .

R o n g g a K o so n g ( V o id S p a c e)
V o id sp a ce

in stan

ad ala h b e sarn y a ru an g

d im asu k k a n k e d alam

kosong

antar beras

d alam

w a d ah . B u tiran -b u tiran b eras

g ela s u k u r 2 5 m l sam p ai p e n u h , k em u d ia n d itam b ah k an to lu en s am p ai

b u tiran terseb u t tere n d am lalu d iu k u r v o lu m e to lu en y an g d ib u tu h k a n .



3 .3 .3 .

=



100%



U ji O rg a n o lep tik

N

= vo id sp a ce

V c

= v o lu m e cairan

V

= v o lu m e to tal

( A d a w iy a h D R d a n W a y sim a . 2 0 0 9 )

U ji o rg an o lep tik y an g d ilak u k an ad ala h u ji p en erim aan terh ad ap w arn a, aro m a, tek stu r, ra sa
d an citra k es elu ru h a n d im an a s etiap p a n elis d ih aru s k a n m en g em u k ak a n tan g g ap an p rib ad in y a terh ad ap

10

produk

yang

d isajik a n . U ji

p en erim aan

yan g

d ilak u k a n

ad alah

u ji h e d o n ik

yang

m en g g u n a k an 3 0 p an elis tid ak terlatih . S k ala h e d o n ic y an g d ig u n ak an ad alah 1
7=

S a n g at S u k a ; 6 = S u k a; 5 = A g a k S u k a; 4 = N etral; 3 = A g ak

T id ak



d ilak u k an

d eng an

7, di m an a ang ka

S u k a; 2 = T id ak S u k a; 1 = S a n g at

T id ak S u k a

3 .3 .4 .

K a d a r A ir

(SN I 01-39 45-199 5)

P en g u k u ra n d ilak u k an d e n g a n m en g g u n ak a n m eto d e o v en . C aw an k o so n g d ik erin g k a n d alam
o v en s elam a 1 5 m e n it d an d id in g in k a n d alam
y an g tela h d ik erin g k an d im as u k k an d alam
o

oven pad a suhu 105 C
ke

d e sik ato r, k em u d ia n d itim b an g . S e b an y ak 5 g ram

co n to h

ca w an y an g telah d itim b an g s elan ju tn y a d ik erin g k an d alam

selam a 6 jam , c aw an y a n g telah b erisi co n to h terse b u t sel an ju tn y a d ip in d ah k an

d esik ato r, d id in g in k an ,

dan

d itim b an g . P en g erin g an

d ilak u k an

sam p ai

d ip ero leh

berat

k o n sta n ,

k em u d ia n d ih itu n g b erd asark an k eh ilan g an b erat y aitu selisih b erat aw al d ik u ran g i b erat ak h ir.







�� ( %



��

%



) =



=



− (



∗ 100%
)

∗ 100%



a = B erat caw an k o s o n g k erin g ( g )
x = B erat sam p el aw al (g )
y = B erat caw an + sam p el k erin g
x = B erat sam p el b a sa h

K adar A bu ( SN I 01 – 3 945 – 1 995 )

3 .3 .5 .

C o n to h b era s d itim b an g s eb a n y a k 2 -3 g ram

k e d alam

caw an p o r selen y an g telah d ik etah u i

b o b o tn y a. A ra n g k an d i ata s n y ala p em b a k ar, lalu a b u k an d alam
o

550 C

tan u r listrik p ad a

su h u m a k sim u m

sam p ai p en g ab u an seles ai (sek ali - sek ali p in tu tan u r d ib u k a se d ik it ag ar o k sig e n b is a m a su k ).

D in g in k an d alam

d e sik ato r lalu d itim b an g h in g g a b o b o t tetap .

K adar a bu (% ) = x – a x 10 0%
w

a

= B erat caw an k o s o n g k erin g (g )

w = B erat s am p le aw al (g )
x = B erat abu + b erat caw an

3 .3 .6 .

K a d a r P ro tein d en g a n M eto d e K je ld a h l
S eba nya k

selen iu m

0 .2 5

0 .2 5 g r a m

gram

dan 3 m l H

sam p le,
2

SO

4

d im a su k k an

d alam

lab u

K jeld ah l

m l

dan

tam b ah k an

p ek at. K em u d ia n lak u k an d estru k si (p em an asa n d alam

m e n d i d i h ) s e l a m a 1 j a m , s a m p a i l a r u t a n j e r n i h .s e t e l a h d i n g i n t a m b a h k a n
N a O H 4 0 % ,l a l u d i d e s t i l a s i . H a s i l d e s t i l a s i d i t a m p u n g d a l a m
m l H 3B O 3 2%

100

d an 2 tetes in d icato r B ro m

kea da an

5 0 m l aq u ad est d a n 2 0 m l

lab u E rlen m ey er y an g b erisi cam p u ran 1 0

C re so l G re en -M eth yl R ed

b erw arn a m era h m u d a. S etelah

v o l u m e h a s i l t a m p u n g a n ( d e s t i l a t ) m e n j a d i 1 0 m l d a n b e r w a r n a h i j a u k e b i r u a n ,d e s t i l a s i d i h e n t i k a n d a n
d estilasi d ititrasi d en g an H C L 0 ,1 N

sam p ai b erw arn a m era h m u d a. P erlak u an y an g s am a d ilak u k an

ju g a terh ad ap b lan k o . D e n g an m eto d e in i d ip ero leh k ad ar N itro g en to tal y an g d ih itu n g d e n g a n ru m u s:
% N = (m l H C l – m l b lan k o ) x n o rm alitas x 1 4 x 1 0 0
m g sam p el
% P r o t e i n = % N x 6 ,2 5

3 .3 .7 .

K a d a r L em a k d e n g a n M eto d e S o x h let
S eba nya k

2

gram

sam pel

d ise b ar

di

atas

kapas

y an g

b eralas

k ertas

s arin g

d an

d ig u lu n g

m em b en tu k th im b le, lalu d im as u k k an k e d alam la b u so x h let. K em u d ian ek strak si selam a 6 jam , d en g an

11

p e l a r u t l e m a k b e r u p a h e k s a n s e b a n y a k 1 5 0 m l .L e m a k y a n g t e r e k s t r a k , k e m u d i a n d i k e r i n g k a n d a l a m
o v en p a d a su h u 1 0 0

0

C s elam a 1 jam .

% lem ak = B erat lem ak x 1 0 0
B erat co n to h
B erat lem ak = (b erat lab u + lem a k ) – b erat lab u

3 .3 .8 .

W a k tu R eh id r a si
S am p el y an g d ian g g a p terb aik d iam b il se b an y a k 2 0 g d itim b an g d an d ic am p u r d en g an 6 0 m l

air p ad a s u h u 9 0 ° C
teren d am

d i d alam

g ela s p iala 2 5 0 m l. W ak tu reh id ra si d iu k u r m u lai seja k s elu ru h s am p el

air p an a s s am p ai air terserap s em u a.

12

IV .

4 .1

H A S IL D A N P E M B A H A S A N

P e n e l i ti a n P e n d a h u l u a n
H asil d ari p en elitian p en d a h u lu a n

m en u n ju k k an b a h w a p erlak u an p em as ak an m en g g u n ak an

reto rt selam a 5 m en it m en g h a silk an n asi y an g k eras d an k u ran g m as ak . P em a sak an selam a 1 5 m e n it
m en g h asilk a n n asi y an g h an cu r a k ib at terlalu m a sa k . A d ap u n p em a sa k an d e n g an reto rt s elam a 1 0 leb ih
k u ran g s eta ra d alam p en am p a k an v is u al d en g an aro n k u k u s , k aren a itu h asil p em as ak an reto rt s elam a 5
d an 1 5 m e n it tid ak d ik erin g k an

d a n p erb an d in g an h a siln y a d ap at d ilih at p ad a T a b el 3 .

T ab el 3 . K arak teristik n asi h asil p em asa k a n d a n p en g erin g an
P erlak u a n

P en g am atan v isu al p ro d u k

1

L en g k et, tid ak b isa m en jad i b u tiran tu n g g al, b erw arn a a g ak k e co k lata n

2

L en g k et, tid ak b isa m en jad i b u tiran tu n g g al, b erw arn a k eco k latan

3

T id ak len g k et, b isa m en jad i b u tiran tu n g g al, b erw arn a a g ak k e co k lata n

4

T id ak len g k et, b isa m en jad i b u tiran tu n g g al, b erw arn a k eco k latan

K eteran g a n :
p erlak u a n 1 : b eras d im as ak m e n g g u n ak a n reto rt selam a 1 0 m en it d an d ik erin g k an p ad a s u h u 6 0 ° C
p erlak u a n 2 : b eras d im as ak m e n g g u n ak a n reto rt selam a 1 0 m en it d an d ik erin g k an p ad a s u h u 8 0 ° C
p erlak u a n 3 : b eras d im as ak m e n g g u n ak a n m eto d e aro n k u k u s d a n d ik erin g k an p a d a su h u 6 0 ° C
p erlak u a n 4 : b eras d im as ak m e n g g u n ak a n m eto d e aro n k u k u s d a n d ik erin g k an p a d a su h u 8 0 ° C

P em as ak an m en g g u n ak an reto rt m e n g h asilk a n b eras y a n g len g k et, seh in g g a s aat d ik erin g k an
m en g g u n a k an flu id ized b ed d r yer m e n g h asilk an b u tiran b era s y an g tid a k d ap at terp isah k aren a len g k et.
N asi

yang

le n g k et

terseb u t

d iseb ab k an

o leh

b eras

yan g

terg elatin isa si.

B era s

y ang

d im as ak

m en g g u n a k an reto rt m en g alam i g elatin isa si p ati y an g b erleb ih a n , k are n a tek an a n p a d a saat p em as ak an
terlalu

b esar

G elatin isasi

d an
pad a

m eny eb abk an
bera s

yan g

stru k tu r

d im as ak

sel

b eras

m en jad i

m en ggu nak a n

reto rt

rusak

dan

m en g ak ib atk an

m enyeb abk an

terjad in y a

len g k et .

p em asak an

b erleb ih an (o ve r c o o k ed ) .
B erd as ark an d ata ters eb u t, m ak a d ip ilih m eto d e p em as ak a n m e n g g u n a k an aro n k u k u s. P a d a
p em a sak an m en g g u n ak an m eto d e

aron

ku kus

d id ap ati b eras

y an g tid a k len g k et

dan

d a p at m en jad i

b u tiran tu n g g al sa at d ik erin g k an .

4 .2

P e n e l i ti a n U t a m a

4 .2 .1

R a sio R e h id ra si
G am b ar rasio reh id ra si (G am b ar

9 ) m en u n ju k k an seb erap a b e sar d a y a serap sam p el terh ad ap

air. D ata terseb u t m en u n ju k k an tin g k at p e n y era p an air n asi u d u k in stan setela h d ik erin g k an . D ik e tah u i
b ah w a s am p el d en g an p erlak u an p en g erin g an A m em ilik i rasio reh id ra si y an g p alin g tin g g i, y aitu 5 ,8 .
S am p el in i m em ilik i rasio
pada

sam p el

in i.

reh id rasi p alin g tin g g i d iseb ab k an p en g erin g an b ertah ap y an g d ilak u k an

P en g erin g an

b ertah ap

y ang

d ilak u k an

m en guran gi

resik o

ca se

h a r d en in g .

C a se

h a rd en in g m eru p ak a n fen o m en a terjad in y a p en g eras an p ad a b a g ian k u lit ak ib at p em an a sa n b erleb ih an
y an g m en y eb ab k an k eru s ak a n p a d a sel s eh in g g a m en g k eru t d a n air d alam

b ah an p an g an tid a k d ap at

k elu ar s ec ara s em p u rn a. M eto d e p en g erin g a n b ertah ap , m em u n g k in k an air p a d a b ah an
teratu r

m en in g g alk an

sam p el.

P e n g erin g an

b ertah ap

in i

m en g h asilk a n

b eras

k elu ar se cara

in stan

y ang

leb ih

m en g em b an g d ari p en am p ak an lu ar, b ila d ib a n d in g k an d e n g a n s am p el lain n y a.
S am pel

d eng an

p erlak u an

p en g erin g a n

B

m em ilik i

rasio

reh id rasi

4.

D ata

terseb u t

m en u n ju k k a n b a h w a sam p el in i m asih m em ilik i k em am p u an reh id ra si, m es k ip u n n ilain y a tid ak se b aik
sam p el p ertam a. P en y eb a b
Suhu 60

o

p erb e d aa n ra sio reh id ra si in i a d alah

suhu

p e n g erin g an

yang

d ig u n ak a n .

C y a n g d ig u n ak a n , seb en arn y a m asih m as u k p ad a re n tan g su h u p en g erin g a n n asi u d u k in sta n ,

n am u n p e n g e rin g an sec ara lan g su n g ak a n m e n g a k ib atk a n air y a n g ad a p ad a b ah an p an g an tid a k d ap at

13

k elu ar s ec ara s em p u rn a. A ir y an g tertin g g al p ad a b a h an p a n g an ak a n m e n u ru n k an rasio re h id rasi b ah an
p an g an ters eb u t.
S am pel

k etig a, ad alah

sam p el d e n g an p erlak u a n p en g erin g an

C . S am p el terseb u t m em ilik i

rasio reh id rasi y an g p alin g ren d ah . N ilai terseb u t d iseb ab k an air y an g b erad a d alam
terseb u t tid a k k elu ar

sec ara

sem p u rn a

d ise b ab k an

o leh

c a s e h a rd en in g

p ada

n asi u d u k in stan

b aha n p an gan

tes eb u t

ak ib at c ara p e n g erin g an y an g tid ak te p at.

8

5. 8

6
4
4

3
2

0
A
B
C

G am b ar 9 . R asio reh id rasi b eras h a sil p erlak u a n

R o n g g a K o so n g ( V o id S p a ce)

4 .2 .2

N ilai vo id sp a c e y a n g d id a p at p a d a p en elitian in i m en g g am b ark an ro n g g a a n tar b eras d alam
w ad ah . M ak in b e sar n ilai ro n g g a an tar b eras , m en u n ju k k an u k u ran b era s y an g m ak in b e sar. S em ak in
b es ar b u tiran b eras m en u n ju k k an n ilai p o ro sitas b era s y an g s em ak in b e sar. S am p el d e n g a n p erlak u a n A
m em ilik i

n il a i

rongga

an tar

beras

d ala m

m e m i l i k i n il a i r o n g g a a n t a r b e r a s d a l a m

w ada h

p alin g

tin g g i

seb es ar

6 1 .8 % . S a m p e l

w a d a h s e b e s a r 4 9 .8 % . P e r l a k u a n C

p erlak u an

B

m em ilik i n ilai p erlak u an

an tar b era s p alin g ren d ah y aitu 4 3 .2 % .
M elalu i d ata terseb u t d ik eta h u i b ah w a b eras d e n g an p erlak u an A m em ilik i ro n g g a y an g p alin g
b es ar d ian tara d u a s am p el lain n y a . R o n g g a a n tar b era s y an g b esar, m en u n ju k k an u k u ra n b eras y a n g
b es ar. U k u ra n b eras y a n g b e sar, m en u n ju k k an p o ro sita s b eras y a n g b e sar . P erlak u a n C
rongga

an tar

b era s d alam

w ada h

y an g k ecil. N ilai terse b u t m e n u n ju k k a n

ukuran

m em ilik i n ilai

b eras

yang

k ecil.

S e m a k i n k e c i l u k u r a n b e r a s , m e n u n j u k k a n k o n d i s i p o r o s i t a s y a n g k e c i l p u l a ..
B esarn y a n ilai ro n g g a y an g d id ap at, b erh u b u n g a n d en g an rasio reh id rasi. R o n g g a b eras y a n g
b es ar, ak an m en g h asilk an n ilai rasio reh id rasi y an g tin g g i. N ilai rasio reh id rasi y an g tin g g i, d iseb ab k an
b eras m em ilik i ro n g g a y an g b esar. S a at d ilak u k an p ro ses reh id ra si, b eras d e n g a n u k u ran ro n g g a y a n g
leb ih b e sar ak an le b ih b a n y a k m e n y era p air. P ad a p e rlak u a n A , m em ilik i p o ro sita s y a n g p alin g tin g g i.
S aat