b. Perhitungan indeks bias pada suhu standar Apriyantono, 1989
R = R’ – K T’-T R = 1,489
– 0,00385 27
o
C – 20
o
C R = 1,486
Keterangan : R : Indeks bias pada suhu standar
R’ : Indeks bias pada suhu pembacaan T : Suhu standar 20
o
C T’ : Suhu pembacaan
K : 0.000385
B.2 Pengujian berat jenis
C. Hasil Evaluasi Sediaan Krim
C.1 Tabulasi hasil pengujian viskositas krim
Replikasi Berat jenis
1 0,896
2 0,899
3 0,893
Rata-rata ± SD 0,896 ± 0,003
RSD 0,30
Replikasi Viskositas dPas
F F
1
F
2
F
3
1 180
160 150
140 2
180 160
150 140
3 180
160 155
145 4
175 170
155 145
5 185
160 155
140 Rata-rata ± SD
180 ± 3,16
162 ± 4,00
153 ± 2,45
142 ± 2,45
RSD 1,76
2,47 1,60
1,72
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C.2 Tabulasi hasil pengujian daya sebar krim
Berat Beban
g
Diameter Sebar cm F
F
1
F
2
F
3
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
4,10 4,00 4,25 4,20 4,20 4,35 4,15 4,60 4,50 4,25 4,35 4,45 4,40 4,30 4,30 4,50 4,70 4,80 4,50 4,55 5
4,25 4,10 4,35 4,25 4,25 4,45 4,25 4,70 4,60 4,35 4,45 4,55 4,55 4,40 4,45 4,65 4,80 4,90 4,65 4,75 10
4,30 4,20 4,45 4,45 4,35 4,55 4,35 4,85 4,75 4,50 4,70 4,75 4,70 4,75 4,60 4,90 5,10 5,25 4,90 4,95 15
4,45 4,30 4,50 4,50 4,40 4,70 4,40 4,95 4,90 4,60 4,75 4,80 4,85 4,80 4,70 5,05 5,35 5,35 5,05 5,15 20
4,50 4,40 4,60 4,55 4,45 4,75 4,55 5,05 4,95 4,70 4,80 4,90 4,90 4,85 5,10 5,15 5,35 5,45 5,15 5,20 25
4,55 4,55 4,70 4,65 4,50 4,80 4,65 5,10 5,05 4,75 4,90 4,95 5,00 4,95 5,20 5,25 5,40 5,50 5,25 5,25 30
4,60 4,60 4,80 4,70 4,55 4,85 4,70 5,15 5,10 4,85 4,95 5,10 5,10 5,00 5,25 5,30 5,55 5,60 5,30 5,35 35
4,70 4,65 4,85 4,75 4,60 4,95 4,75 5,25 5,15 4,90 5,00 5,15 5,15 5,05 5,30 5,35 5,65 5,65 5,35 5,40 40
4,75 4,70 4,90 4,80 4,70 5,00 4,85 5,30 5,25 5,00 5,05 5,20 5,20 5,15 5,35 5,45 5,70 5,75 5,45 5,55 45
4,80 4,85 4,95 4,85 4,75 5,05 4,90 5,35 5,25 5,05 5,10 5,30 5,30 5,25 5,45 5,50 5,75 5,80 5,50 5,60 50
4,85 4,90 5,00 4,95 4,80 5,10 4,95 5,40 5,30 5,10 5,15 5,35 5,35 5,30 5,50 5,55 5,80 5,90 5,55 5,65 55
4,95 4,95 5,05 50
4,85 5,20 5,00 5,40 5,35 5,15 5,25 5,40 5,40 5,40 5,55 5,65 5,85 5,95 5,60 5,70 60
5,00 5,05 5,10 5,05 4,90 5,25 5,05 5,45 5,40 5,20 5,35 5,45 5,45 5,55 5,60 5,70 5,90 6,00 5,65 5,80 65
5,05 5,10 5,15 5,10 4,95 5,30 5,10 5,50 5,45 5,25 5,45 5,50 5,50 5,60 5,65 5,80 5,95 6,05 5,70 5,85 70
5,10 5,15 5,20 5,15 5,00 5,30 5,15 5,50 5,50 5,30 5,55 5,55 5,55 5,60 5,70 5,85 6,00 6,10 5,75 5,95 75
5,15 5,15 5,25 5,15 5,05 5,40 5,20 5,50 5,50 5,45 5,60 5,60 5,65 5,60 5,70 5,90 6,05 6,15 5,80 6,00
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Berat Beban
g
Diameter Sebar cm F
F
1
F
2
F
3
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
80 5,20 5,15 5,30 5,25 5,15 5,40 5,30 5,50 5,50 5,45 5,60 5,60 5,65 5,60 5,70 5,95 6,05 6,15 5,90 6,05
85 5,20 5,15 5,30 5,25 5,20 5,40 5,40 5,50 5,50 5,45 5,60 5,60 5,65 5,60 5,70 6,00 6,05 6,15 6,00 6,05
90 5,20 5,15 5,30 5,25 5,20 5,40 5,40 5,50 5,50 5,45 5,60 5,60 5,65 5,60 5,70 6,00 6,05 6,15 6,00 6,05
Rata- rata ±
SD 5,22 ± 0,05
5,45 ± 0,04 5,63 ± 0,01
6,05 ± 0,05 RSD
0,98 0,82
0,71 0,91
C.3 Tabulasi hasil pengujian pH krim
Replikasi pH
F F
1
F
2
F
3
1 7,90
7,82 7,76
7,60 2
7,93 7,87
7,78 7,55
3 7,89
7,87 7,75
7,51 4
7,93 7,85
7,73 7,50
5 7,92
7,83 7,79
7,50 Rata-rata ± SD
7,91 ± 0,02
7,85 ± 0,02
7,76 ± 0,02
7,50 ± 0,04
RSD 0,20
0,26 0,27
0,51
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C.4 Tabulasi hasil pengujian rheologi krim
Menit ke-
Viskositas dPa.s F
F
1
F
2
F
3
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
Rep 1
Rep 2
Rep 3
Rep 4
Rep 5
180 180
180 175
185 160
160 160
170 160
150 150
155 155
155 140
140 145
145 140
5 150
150 170
140 150
135 130
150 140
140 130
140 130
125 140
130 130
105 125
105 10
140 125
150 130
125 120
120 120
125 120
120 125
120 120
120 120
110 100
105 100
15 130
110 140
120 120
110 110
115 120
120 115
115 110
115 110
115 105
95 100
100 20
125 110
130 105
110 105
105 110
110 115
115 110
110 105
105 115
100 95
100 95
25 110
105 125
100 100
105 100
105 105
110 110
105 105
105 100
110 95
90 95
90 30
105 100
110 100
95 100
100 95
100 105
100 100
100 100
100 100
95 90
90 90
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0,9 g 100 g
D. Penentuan KHM