Penentuan bahan konstruksi : Perhitungan Neraca Massa dan Energi a. Neraca Massa DC-301

A-180 Tabel C.13.6. Data hasil perhitungan trial T bubble feed Komponen xi Po mmhg Ki a xia yi C8H10 0.1945 284.6537 0.37455 0.5611 0.1091 0.0728 CH3COOH 0.0804 507.3537 0.6676 1 0.0804 0.0537 HBr 0.0039 507.3537 0.6676 1 0.0039 0.0026 CH3COO2Co 0.0006 507.3537 0.6676 1 0.0006 0.0004 CH3COO2Mn 0.0005 507.3537 0.6676 1 0.0005 0.0003 C8H6O4 6.41E- 07 3.481E-10 4.580E-13 6.861E-13 4.397E-19 2.935E-19 H2O 0.7201 918.6135 1.2087 1.8106 1.3039 0.8702 total 1 1.4984 1

b. Menentukan Temperatur DEW Point Distilat

Pada keadaan dew point, K Heavy key = 1  yia. Dengan cara trial T pada tekanan operasi 1 atm hingga K Heavy key = 1  yia, maka akan diperoleh temperatur dew point distilat. Dari perhitungan didapat kondisi produk distilat DC-401 : P = 1 atm = 760 mmHg T = 100.020902 o C 373.170902 K Tabel C.13.7. Data hasil perhitungan trial T Dew distilat komponen yi Po mmhg Ki a KiKhk yia xi C8H10 238.2395 0.3135 0.563 CH3COOH 1.117E- 05 423.1762 0.5568 1 1.117E-05 0,00002 HBr 423.1762 0.5568 1 CH3COO2Co 423.1762 0.5568 1 CH3COO2Mn 423.1762 0.5568 1 C8H6O4 1.097E-10 1.444E-13 2.593E-13 H2O 0.99999 760.656 1.0009 1.7975 0.5563 0.99998 total 1 0.5563 1 A-181

c. Menentukan Temperatur Bubble Point Bottom

Pada keadaan bubble point, K Heavy key = 1  xi x a. Dengan cara trial T pada tekanan operasi 1 atm hingga K Heavy key = 1  xi x a maka akan diperoleh temperatur bubble point bottom. Dari perhitungan didapat kondisi produk distilat MD-301 : P = 1 atm = 760 mmHg T = 130.36330101 o C 403.5131010 K Tabel.C.13.8. Data hasil perhitungan trial T bubble bottom produk komponen xi Po; mmHg Ki a xia yi C8H10 0.6948 609.0963 0.8014 0.5506 0.3826 0.5561 CH3COOH 0.2872 1106.2095 1.4555 1 0.2872 0.4175 HBr 0.0139 1106.2095 1.4555 1 0.0139 0.0202 CH3COO2Co 0.0021 1106.2095 1.4555 1 0.0021 0.00297 CH3COO2Mn 0.0018 1106.2095 1.4555 1 0.0018 0.0026 C8H6O4 2.289E-06 3.62E-08 4.77E-11 3.27E-11 7.49E-17 1.091E-16 H2O 0.0003 2060.9833 2.7118 1.8632 0.0005 0.0007 total 1 9.3354 6.4137 0.688 1

E. Neraca Energi DC-401 a. Menghitung panas umpan

Kondisi umpan masuk : T in = T bubble point feed = 105.37C 378.37 K Tref = 25 o Q = n x ∫Cp dT A-182 Perhitungan Q umpan dapat dilihat pada tabel berikut: Tabel C.13.9. Perhitungan Q umpan DC-401 komponen kmoljam ∫Cp.dT KJKg.K Q=n∫Cp dT KJjam C8H10 27.96 11563.32165 323314.3439 CH3COOH 11.56 5559.989154 64266.88044 HBr 0.56 5559.99 3103.31214 CH3COO2Co 0.08 5559.99 457.8135279 CH3COO2Mn 0.07 5559.99 407.5466044 C8H6O4 0.00 0.00 H2O 103.52 2717.318039 281302.7128 total 143.76 672852.6094

b. Menghitung panas distilat

T T dew distilat = 100.020902 o C 373.170902 K Tref = 25 o C 298,15 K Tabel C.13.10. Perhitungan Q distilat DC-401 komponen kmoljam ∫Cp.dT KJKg.K Q=n∫Cp dTKJjam C8H10 10738.24285 CH3COOH 0.00115588 1 5172.690846 5.979017134 HBr 5172.690846 CH3COO2Co 5172.690846 CH3COO2M n 5172.690846 C8H6O4 H2O 103.511837 2 2539.923553 262912.1534 total 262918.1324

c. Menghitung panas liquid refluks